Optimization of obtaining of translucent luminescent ceramics YNbO4 by uniaxial hot pressing from crystal powders synthesized by sol-gel.

We have established optimized parameters of technological process for obtaining of translucent luminescent YNbO 4 ceramics by uniaxial hot pressing (UHP). Ultrafine crystalline powders used for this have been synthesized by sol-gel and sintered at three different temperatures. Series of ceramic YNbO 4 samples were obtained from the powders by UHP at three different sintering conditions. Morphological features of the microstructure, mechanical and photoluminescent characteristics in the visible wavelength range have been compared for YNbO 4 ceramic samples obtained at different UHP conditions and controlled with sample prepared by conventional sintering (CS). The most optimal UHP regime for translucent YNbO 4 ceramics obtaining have been chosen. • Ultrafine YNbO 4 powders were prepared by sol-gel and sintered at 3 temperatures. • An optimal regime was chosen for uniaxial hot pressing (UHP) of YNbO 4 ceramics. • The optimal regime is: T sint = 1180 °C, P 1 = 220 kg/cm2, τ sint = 60 min. • Microstructure, mechanical characteristics and photoluminescence were studied. [ABSTRACT FROM AUTHOR]