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Structural and magnetic properties of superconductor NiBi3/α-Bi2O3 synthesized by mechanical alloying.
- Source :
-
Journal of Applied Physics . 9/7/2020, Vol. 128 Issue 9, p1-9. 9p. - Publication Year :
- 2020
-
Abstract
- A nanostructured NiBi3/α-Bi2O3 superconductor composite has been synthesized by the process of mechanical alloying through 19 h of high energy ball milling. The kinetics of formation is analyzed in detail by x-ray diffraction and the Rietveld method. A simple method is proposed to determine the crystallinity of the resulting sample by using the background Rietveld fitting that permits a quantitative analysis of the diffuse x-ray profile taking into account the air and Compton scattering. The diffuse scattering is attributed to the formation of a nanocluster of α-Bi2O3 which is confirmed by high-resolution transmission electron microscopy and Raman measurements. The magnetic measurements show superconducting transition at around 4 K and the existence of NiBi3/α-Bi2O3 nanophases with a low irreversibility field at around 1.01 T at 2 K. Analysis of magnetic susceptibility and isothermal magnetic hysteresis of the NiBi3/α-Bi2O3 nanocomposite indicates the simultaneous existence of bulk superconductivity and ferromagnetism below 4 K. [ABSTRACT FROM AUTHOR]
Details
- Language :
- English
- ISSN :
- 00218979
- Volume :
- 128
- Issue :
- 9
- Database :
- Academic Search Index
- Journal :
- Journal of Applied Physics
- Publication Type :
- Academic Journal
- Accession number :
- 145535368
- Full Text :
- https://doi.org/10.1063/5.0010489