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Mild and Efficient Synthesis of 1,8-Naphthalide and 1,8-Naphthalenedimethanol.
- Source :
-
Synthetic Communications . 2004, Vol. 34 Issue 12, p2269-2275. 7p. 1 Diagram, 1 Chart. - Publication Year :
- 2004
-
Abstract
- Mild and efficient procedures have been developed for synthesis of 1,8-naphthalide and 1,8-naphthalenedimethanol. In an ice-water bath, 1,8-naphthalide was prepared from 1,8-naphthlic anhydride using LiAlH4 as reducing agent. 1,8-Naphthalenedimethanol was obtained with good yield from reduction of 1,8-naphthalic anhydride by LiAlH4 and Lewis acids at room temperature. The effects of various factors on the reduction of 1,8-naphthalic anhydride with LiAlH4 were investigated. [ABSTRACT FROM AUTHOR]
- Subjects :
- *NAPHTHALENE
*METHANOL
*LEWIS acids
*ACID-base chemistry
*ANHYDRIDES
Subjects
Details
- Language :
- English
- ISSN :
- 00397911
- Volume :
- 34
- Issue :
- 12
- Database :
- Academic Search Index
- Journal :
- Synthetic Communications
- Publication Type :
- Academic Journal
- Accession number :
- 13538202
- Full Text :
- https://doi.org/10.1081/SCC-120038510