The effect of agglomerate integrity and blending formulation on the mechanical properties of whey protein concentrate powder tablets.

Abstract In this work, the strength of tablets made from mixtures of whey protein concentrate (WPC) powder and different types of sugar was investigated. The agglomerated WPC powder was pneumatically conveyed (lean phase) at three different air speeds of 10, 20 or 30 m/s to simulate the effects of industrial powder transport, resulting in agglomerates with reduced integrity. Conveyed and control WPC powder, and sugar of three different particle size distributions (i.e., granulated, GS; caster, CS and icing sugar, IS) were analysed for microstructure, particle size, moisture, and flowability. Tensile strength of tablets from WPC powder alone or blended with 0.5–10% sugar was tested. Conveying of WPC powder led to a significant increase in tablet strength, (i.e., from failure strength of 1.67 N/mm2 for control tablets to 2.33, 2.11 and 2.11 N/mm2 after conveying at 10, 20 or 30 m/s, respectively), suggesting that the generation of smaller powder particles led to increased mechanical strength of tablets. The addition of sugar also resulted in a significant increase in tablet strength (e.g., failure strength of 2.34, 2.12 and 2.47 N/mm2 at 1.5% addition level of GS, CS and IS, respectively) and strongest tablets were obtained at 1.5–3% sugar addition and by blending with icing sugar. This study demonstrated, for the first time, that conveying and dry blending of whey protein and sugar powders significantly influenced the rheological properties of resultant tablets. Highlights •Lean phase conveying reduced mechanical integrity of powder agglomerates. •Bulk flow behavior was enhanced post lean phase conveying. •Tablets prepared using conveyed powders had higher fracture load. •Incorporation of sugar in blends with whey powder resulted in stronger tablets. •Brazilian disc test can detect variations in tablet composition as little as 0.5%. [ABSTRACT FROM AUTHOR]