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A facile route for large-scale synthesis of molybdenum phosphide nanoparticles with high surface area.
- Source :
-
Phosphorus, Sulfur & Silicon & the Related Elements . 2017, Vol. 192 Issue 11, p1159-1164. 6p. - Publication Year :
- 2017
-
Abstract
- In this study, we report a novel, simple and large-scale (about 100 g) synthesis of MoP nanoparticles with a high surface area (439.3 m2g−1). The current approach uses a solid mixture of MoO3, (NH4)2HPO4and phenol-formaldehyde resin (PFR) as a precursor and employs an inert gas as a feed gas. The formation mechanism of MoP was proposed by various techniques, including thermogravimetry-mass spectrometry (TG-MS), X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), and carbon content analysis. [ABSTRACT FROM PUBLISHER]
Details
- Language :
- English
- ISSN :
- 10426507
- Volume :
- 192
- Issue :
- 11
- Database :
- Academic Search Index
- Journal :
- Phosphorus, Sulfur & Silicon & the Related Elements
- Publication Type :
- Academic Journal
- Accession number :
- 125601950
- Full Text :
- https://doi.org/10.1080/10426507.2017.1330829