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Facile hydrothermal synthesis of Ag@AgCl@AlOOH hollow microspheres and their characterizations.
- Source :
-
Materials Letters . Oct2016, Vol. 181, p204-207. 4p. - Publication Year :
- 2016
-
Abstract
- In this paper, Ag@AgCl@AlOOH hollow microspheres were successfully synthesized with AgNO 3 and AlCl 3 ·6H 2 O in NaOH/urea solution by a facile hydrothermal method. NaOH/urea solution acted as structure-directing agent here. Scanning electron microscopy (SEM) and X-ray powder diffraction (XRD) were used to characterize the as-prepared samples. The effects of hydrothermal heating temperatures on the phases and morphologies of samples were investigated. The size distributions analysis showed that the samples were Ag@AgCl@AlOOH microspheres with a diameter of 5.48~6.77 µm. With higher reaction temperatures, more Ag@AgCl@AlOOH microspheres with hollow structures appeared, and the size of Ag@AgCl@AlOOH microspheres decreased. The formation process of Ag@AgCl@AlOOH hollow microspheres was explored and discussed in detail. [ABSTRACT FROM AUTHOR]
Details
- Language :
- English
- ISSN :
- 0167577X
- Volume :
- 181
- Database :
- Academic Search Index
- Journal :
- Materials Letters
- Publication Type :
- Academic Journal
- Accession number :
- 116927205
- Full Text :
- https://doi.org/10.1016/j.matlet.2016.06.027