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The Duolingo application offers foreign language learning, specifically Arabic, to learners worldwide. Although effective, the material within it must meet international language learning standards. This research aims to assess the suitability of Duolingo's material in accordance with the international standards set by ACTFL. This study employs a descriptive qualitative approach, with primary data consisting of Duolingo's materials and secondary data comprising relevant literature. Both data sets are analyzed using Milles and Hubberman's theory. The results indicate that Duolingo complies with the international standards established by ACTFL, covering proficiency levels from Distinguished, Superior, Advanced, Intermediate, to Novice. Each proficiency level ensures that learners can learn a foreign language gradually and systematically according to their language abilities.

Abstract Background This study focused on the aging mechanism and degradation of mechanical and structural features of elastodontic appliances (EA) under artificial and intraoral aging to achieve oral myofunctional therapy with particular removable silicone elastomer devices. Materials and methods EAs artificially aged in saliva with different pH values were investigated through cyclic compression testing along with characterization techniques (Scanning electron microscopy, X-ray diffraction, and Fourier transform infrared spectroscopy), and characterization analysis was also performed on clinically retrieved EAs. Results Artificial aging was found to have minimal effect on the structural properties of EAs, and intraorally aged samples showed perceptible micro-morphology. The Mullins index and peak stress decreased (P

Some wrong decisions and faulty practices applied during the repair and restoration of traditional buildings cause more damage to the structures due to the materials used in the repair. The aim of this study is to establish a scientific basis for material selection in the repair of traditional buildings in the Konuralp region through chemical and petrographic analyses. In this study, brick, mortar, plaster, and wood samples were taken from one registered building in the Konuralp neighborhood of Düzce Province that has survived to the present day by preserving its original structural features and reflecting the characteristics of traditional housing. Chemical and petrographic analyses were carried out on the samples. In line with these analyses, a scientific basis was created for selecting material properties in the repair and reuse processes of traditional buildings and suggestions are made for the analysis of materials specific to traditional buildings in Konuralp.

The research area of the interaction between religion, politics, and medieval Hispanic art has been pioneering and at the cutting edge of contemporary historiography in recent years. The deployment of iconographic and calligraphic motifs in medieval religious spaces has been identified as a key means of propagating legitimating messages of power and disseminating Christian doctrines. This interdisciplinary study proposes an analysis of the artistic vestiges present in the refectory of the Monastery of San Salvador de Oña (Burgos), with a view to establishing their decorative evolution during the 14th century and their symbolic significance. In order to establish a chronological proposal for the remains, the historical, artistic, and architectural contexts of the monastery are analyzed. This is complemented by a study of materials and techniques and a symbolic and iconographic analysis of the signs of power and evangelical concepts from the time of Pedro I until the transition to the Trastámara dynasty. In this way, a cross-disciplinary investigation is proposed, with the aim of elucidating how a sacred artistic work situated within a secular context can serve multiple purposes of political and religious legitimation through the adaptation of its iconography over time. [ABSTRACT FROM AUTHOR]

Access to research infrastructure for heritage science is the best way of narrowing the collections knowledge gap between resource-rich and resource-poor cultural institutions. Here we demonstrate a novel workflow that streamlines the use of a mobile laboratory for data collection (MOLAB) followed by a digital platform for data processing, analysis and interpretation (DIGILAB). The data collection and processing are taken care of by heritage science specialists, while the data analysis and interpretation can be performed collaboratively with conservators and curators. MOLAB with specialist personnel and mobile scientific instruments can sometimes be aided by in-house fixed laboratory (FIXLAB) equipment and personnel from resource-rich institutions to assist the resource-poor institutions if their collection can be hosted by the resource-rich institutions for analysis. The aim is to widen participation in the adoption of heritage science and material analysis in the understanding and conservation of collections, while ensuring high-quality, efficient and reliable data acquisition, processing, analysis and interpretation. The approach taken in this project combines access to various research infrastructure platforms to achieve extra benefit through adding further expert-assisted data analysis and interpretation capabilities, enabled by a new digital platform for data processing and visualisation. [ABSTRACT FROM AUTHOR]

Some wrong decisions and faulty practices applied during the repair and restoration of traditional buildings cause more damage to the structures due to the materials used in the repair. The aim of this study is to establish a scientific basis for material selection in the repair of traditional buildings in the Konuralp region through chemical and petrographic analyses. In this study, brick, mortar, plaster, and wood samples were taken from one registered building in the Konuralp neighborhood of Düzce Province that has survived to the present day by preserving its original structural features and reflecting the characteristics of traditional housing. Chemical and petrographic analyses were carried out on the samples. In line with these analyses, a scientific basis was created for selecting material properties in the repair and reuse processes of traditional buildings and suggestions are made for the analysis of materials specific to traditional buildings in Konuralp. [ABSTRACT FROM AUTHOR]

Abstract Funerary masks played a crucial role in ancient Egyptian burial practices, as part of the rituals to ensure a successful afterlife. This study presents the first comprehensive analysis of a gilded mummy mask from the Roman period in Egypt from the collections of The Ny Carlsberg Glyptotek in Copenhagen. Portraying a young female, the mask belongs to a distinctive group of mummy masks, whose origins can be identified to be coming from the Dakhlah and Kharga oases. The construction of the mask (plaster, textiles) and the constituents of its polychromy (pigments, binding media) was analysed using various non- and micro-destructive methods: imaging, cross-section analysis, optical microscopy, Fourier transform infrared spectroscopy and scanning electron microscopy coupled to energy-dispersive X-ray spectroscopy. Additionally, samples were taken for palaeoproteomic analysis with liquid chromatography–tandem mass spectrometry. A wide range of pigments such as yellow and red ochre, carbon-based black, and Egyptian blue were identified, reflecting common materials in polychromy in Egypt during the Roman period. Notably, indigo was detected, suggesting its usage in mixtures to render purple hues. Analysis of adhesives and media identified plant gum and collagen-based animal glue. Proteomic analysis identified Equus asinus (donkey) as the predominant protein source for the collagen-based glue. The results shed light on the materials and techniques employed in ancient polychromy in Egypt in the Roman period, further enriching our understanding of artistic practices at the time.

Materials applied in nuclear environments such as fission or fusion power-plants face severe conditions. The irradiation by neutrons induces thermal loads and irradiation damage. Furthermore, coolants in contact with the materials induce corrosion, which is particularly challenging for liquid salts intended for the next generation of fission reactors. A new device (DICE) is installed at the 3.5 MV accelerator at DIFFER for the accelerated testing of such materials under combined irradiation and corrosion conditions. The DICE enables irradiation of samples at temperatures of up to 1050 K and in contact with liquid salts. An integrated shielding and a low power temperature control concept based on radiation cooling enables high-duty cycle application in a standard accelerator laboratory. Ion currents of up to 30 µA are possible with continuous irradiation. This work outlines the technical concept of the device and presents the first data. [ABSTRACT FROM AUTHOR]

In this study, mortar and plaster samples taken from a traditional house (1799 parcel) located in the neighborhood Konuralp, Düzce Province, were subjected to acid loss, ignition loss, loss of aggregates sieve analysis after acid, protein, and fat tests, tests of salt, as well as Petrographic and SEM-EDX analyses. Brick samples underwent physical examinations microscopic analyses and mechanical in addition to SEM-EDX analyses. For wood samples, macroscopic and microscopic analyses were conducted to determine their types. Based on these analyses, recommendations have been made to contribute to the repair and reuse of the material properties of the selection processes of traditional structures. [ABSTRACT FROM AUTHOR]

Funerary masks played a crucial role in ancient Egyptian burial practices, as part of the rituals to ensure a successful afterlife. This study presents the first comprehensive analysis of a gilded mummy mask from the Roman period in Egypt from the collections of The Ny Carlsberg Glyptotek in Copenhagen. Portraying a young female, the mask belongs to a distinctive group of mummy masks, whose origins can be identified to be coming from the Dakhlah and Kharga oases. The construction of the mask (plaster, textiles) and the constituents of its polychromy (pigments, binding media) was analysed using various non- and micro-destructive methods: imaging, cross-section analysis, optical microscopy, Fourier transform infrared spectroscopy and scanning electron microscopy coupled to energy-dispersive X-ray spectroscopy. Additionally, samples were taken for palaeoproteomic analysis with liquid chromatography–tandem mass spectrometry. A wide range of pigments such as yellow and red ochre, carbon-based black, and Egyptian blue were identified, reflecting common materials in polychromy in Egypt during the Roman period. Notably, indigo was detected, suggesting its usage in mixtures to render purple hues. Analysis of adhesives and media identified plant gum and collagen-based animal glue. Proteomic analysis identified Equus asinus (donkey) as the predominant protein source for the collagen-based glue. The results shed light on the materials and techniques employed in ancient polychromy in Egypt in the Roman period, further enriching our understanding of artistic practices at the time. [ABSTRACT FROM AUTHOR]

Copyright of Czech Journal of Historical Heritage Preservation / Zpravy Pamatkove Pece is the property of Narodni Pamatkovy Ustav and its content may not be copied or emailed to multiple sites or posted to a listserv without the copyright holder's express written permission. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract. (Copyright applies to all Abstracts.)

The lithography books of Iran, despite their historical importance, have received relatively little attention. This study aims to comprehensively examine an Iranian lithography book from the Qajar period titled Hayat al-Qolub, to identify its materials. The paper pulp, sizing, inks and leather of the bookbinding were analyzed through various methods, including staining tests for identifying paper pulp, light microscopy, FTIR, Raman spectroscopy, Micro-spectrophotometry, multi-band imaging, SEM-EDS and LC-MS. The findings suggest that the book was made of rag paper composed of linen and cotton fibers, while animal glue and gypsum were used for paper sizing and filling, respectively. Carbon black was used as black printing ink and cochineal was used for red ink. The leather cover of the book was made of goat skin that was tanned with gallotannins and unhaired with lime. Evidence of the use of liming in the unhairing process was also observed in this leather. This research enhances our understanding of paper and bookmaking techniques of the Qajar period in Iran. [ABSTRACT FROM AUTHOR]

The material manifestation of late medieval parchment manuscripts results from their history, which is shaped by owners, fragmentators or bookbinders. While certain characteristics, such as the dissection or palimpsesting of manuscripts, are clearly recognizable and analyzable, these objects contain further significant information about their past, which is, unfortunately, invisible to the human eye.Using three music manuscripts from the early fifteenth century, we demonstrate how processed multispectral data can provide digital images that contain new evidence about the manuscript's past, its production, and its use and interaction with other objects. Multispectral data have until now been generated – mostly at great expense – to make obscured writing visible. Our approach relies on a secondary use of these data to elucidate a manuscript's production and its afterlife, and some results consequently compelled us to undertake further codicological and material investigations. Our specific findings include the imprints of spectacles used by Florentine monks, the traces left by Viennese bookbinders and Nuremberg librarians, and a music scribe's unexpected change of inks.This paper is aimed at manuscript researchers and imaging scholars, as well as librarians and conservators, who are interested in the information on materiality that can be gleaned from manuscripts by applying MSI, and that can thus enrich our understanding of these unique objects. [ABSTRACT FROM AUTHOR]

The urgent need to preserve cultural heritage is starkly evident in contemporary society, particularly poignant in Morocco where its rich cultural legacy faces unprecedented threats. The rapid forces of urbanization and relentless economic development have converged, resulting in the alarming devaluation and irreversible degradation of a substantial portion of this invaluable heritage. Within this disconcerting backdrop, certain remarkable vestiges have managed to endure the ravages of time. One such exemplar is the Marinid Madrasa, an architectural marvel from the 4th century, nestled within the Chellah archaeological site in Rabat, Morocco. Beyond its physical grandeur, the Madrasa plays a pivotal role as a conduit between the past and the future, facilitating the transmission of cultural heritage to generations yet unborn. This paper embarks on a multidisciplinary journey, employing advanced techniques such as terrestrial photogrammetry, numerical modeling, and specialized archaeological characterization, to undertake comprehensive diagnostic study processes. The convergence of these diverse methodologies lays a robust foundation for a holistic diagnostic study. This endeavor serves not only academic curiosity but becomes the cornerstone upon which strategies for compatible conservation and restoration interventions are erected. In the intricate interplay between historical preservation and the imperatives of progress, these methodologies form a bridge. This bridge links the architectural magnificence of the Madrasa with the imperatives of safeguarding it in a rapidly changing world. The ultimate aspiration of this multidisciplinary approach is twofold: to ensure the enduring protection of the Marinid Madrasa and other archaeological remnants against the erosive forces of time and urban development, and to forge a narrative that sensitively navigates the challenges posed by preserving cultural heritage in the face of modernity. In this endeavor, advanced technologies are interwoven with a profound recognition of the historical, social, and cultural significance of these sites, ultimately charting a course that not only conserves architectural brilliance but also honors the profound stories they encapsulate across the epochs.

Unitized regenerative proton exchange membrane fuel cell (URPEMFC) as a self-sufficient hydrogen energy system offers a unique proposition for achieving a net zero emissions future. The system combines the operation of water. Due to the design parameters and operating conditions of URPEMFC, the potential cycling from the mode switching, high temperature, humidified environment and the long exposure of metallic components to hydrogen are the primary factors causing degradation to the system. Consequently, the conventional graphite bipolar plate (BP) suffers heavily under such an environment while giving rise to alternative metallic base materials, such as titanium, stainless steel, and aluminum. Various surface treatment and coating methods are currently under investigation to provide the required corrosion resistance while maintaining feasible manufacturing process and cost. This paper presents an overview into the degradation phenomena of URPEMFC that contributes to the corrosion of BP that is affecting the performance and future commercialization of the system. The operating condition of the system is summarized in terms of fuel cells and water electrolyzers respectively, along with the integration of both operations as a system. Next, the paper outlines the degradation phenomena observed on BP and the behavior of various materials under such conditions. The performances of various base and coating materials have been compiled as have characterization methods that are useful in measuring corrosion resistance. This paper aims to provide a better understanding on the overall degradation of BP in URPEMFC and overview of various material choices to identify the optimal corrosion mitigation solution. [Display omitted] • Breakdown of the URPEMFC operating parameters from the respective operation modes. • System design approaches allowing integration of fuel cell and electrolyzer modes. • Identification of the main degradation mechanism on the BP. • Tabulated data of various base materials and coatings performance. • Discussion of current experimental and modeling methods for corrosion resistance characterization. [ABSTRACT FROM AUTHOR]

This research explores the enhancement of mechanical properties in material architectures, such as strength-to-weight ratio and resilience, through the inspiration of natural systems. Historically, designs for additive manufacturing have relied on simple, repetitive structures like honeycombs, often leading to unnecessary material expenditure. This study aims to examine the compressive mechanical attributes of designs inspired by natural systems, including bird nests, cocoons, and the layered structure of skull bones. Through a comparative analysis, we assessed peak load capacity, strength-to-weight ratio, and resilience between these bioinspired architectures and a standard 3D infill pattern utilized in additive manufacturing. Findings indicate that structures inspired by sandwiched bone layers excel in resilience and peak load, whereas those based on bird nests are notably lighter and, in some cases, exhibit the highest strength-to-weight ratio. The insights provided here will help design engineers with empirically backed mechanical properties of bioinspired architectures, offering a novel methodology for the development of material systems influenced by biological paradigms. [ABSTRACT FROM AUTHOR]

Several medieval mural cycles in Austria were studied from the material and technical point of view, aiming to confirm (or reject) the art-historical hypothesis of their stylistic and workshop connection. These paintings can be found in the churches of Rust (“Fischerkirche”), Marz (Virgin’s Coronation parish church), Kobenz (St. Ruprecht parish church), Ofenbach (St. Veid parish church), and St. Johann am Steinfelde (St. John parish church). They were carried out around 1400 in the International Gothic style. Their workshop connections based on the style are doubtful, therefore, a material and technical study was carried out. Results showed different plaster composition, similar pigment palette, and diverse painting procedures. The murals in Marz, St. Johann, and the older register in Rust reveal important similarities such as plaster composition, predominant a fresco painting technique, the use of natural inorganic pigments, as well as many aspects of the painting procedure and modeling. On the contrary, those in Kobenz, Ofenbach, and the younger register in Rust differ considerably. The second group reveals lower quality in plaster composition, larger a secco parts, addition of synthetic pigments (Kobenz), and a rougher color modeling, indicating less skilled artists. The lower quality also results in a worse conservation state of these murals. The obtained results confirm the same workshop, but different artists in the first group, while in the second group no clear workshop/artist connection could be established.

Biodegradable material is a kind of polymer material which has no pollution to the environment. It has been used in food packaging, medical treatment, agriculture and other industries. However, the production cost of biodegradable materials is high and the physical properties are defective, which affects their wide application in various fields. The types and properties of biodegradable materials are reviewed. The advantages and disadvantages of spectroscopy, nuclear magnetic resonance and chromatography and mass spectrometry in the identification of biodegradable materials are compared. It is pointed out that the material characterization of biodegradable materials and the analysis methods of impurities are the key research contents, so as to provide reference for the material analysis of biodegradable materials. [ABSTRACT FROM AUTHOR]

Several medieval mural cycles in Austria were studied from the material and technical point of view, aiming to confirm (or reject) the art-historical hypothesis of their stylistic and workshop connection. These paintings can be found in the churches of Rust ("Fischerkirche"), Marz (Virgin's Coronation parish church), Kobenz (St. Ruprecht parish church), Ofenbach (St. Veid parish church), and St. Johann am Steinfelde (St. John parish church). They were carried out around 1400 in the International Gothic style. Their workshop connections based on the style are doubtful, therefore, a material and technical study was carried out. Results showed different plaster composition, similar pigment palette, and diverse painting procedures. The murals in Marz, St. Johann, and the older register in Rust reveal important similarities such as plaster composition, predominant a fresco painting technique, the use of natural inorganic pigments, as well as many aspects of the painting procedure and modeling. On the contrary, those in Kobenz, Ofenbach, and the younger register in Rust differ considerably. The second group reveals lower quality in plaster composition, larger a secco parts, addition of synthetic pigments (Kobenz), and a rougher color modeling, indicating less skilled artists. The lower quality also results in a worse conservation state of these murals. The obtained results confirm the same workshop, but different artists in the first group, while in the second group no clear workshop/artist connection could be established. [ABSTRACT FROM AUTHOR]

Not many manuscript maps have been the object of material analysis so far. A portolan chart, signed and dated by Juan Vespucci in 1520, was studied in this research, conserved at the Archivo General de Indias in Seville (Spain). It is made on parchment and depicts the coasts and islands of Europe and Africa. It is the oldest portolan chart made in Seville, being unusual in applying hand stamp for decorative figures. The map was analysed by different non-invasive techniques: infra-red and ultraviolet light, digital microscope and X-ray fluorescence (XRF). The main goals of this study were to identify the materials used, as well as to detect retouching or restoration work. Results showed that the entire parchment was first covered with a white layer made of lead white (Pb), calcite or gypsum (Ca). The principal pigments used were vermilion (Hg), yellow ochre (Fe), azurite (Cu) and a copper-based green pigment (Cu) and carbon black. The letters were probably written with an iron-gall ink (Fe, Cu). Very thin golden leaves were applied on a mixtion glue for gilded wind roses. Several retouches from the 19th/20th centuries were found using zinc and titanium whites and probably cobalt blue.

P.Cair.Zen. IV 59538 (TM 1174), dated to 16 January of 257 BCE, is a fragmentary papyrus from the Zenon Archive that preserves the final part of a letter. Along with a significant part of its content, the identity of both its sender and addressee has been lost. However, a careful analysis of the material aspects of the letter reveals that its author and scribe can be identified with Amyntas (TM Per 769), the administrator of the Alexandrine household of Apollonios. [ABSTRACT FROM AUTHOR]

The aim of this study was to develop bio-based adhesives that can be used for various packaging papers. In addition to commercial paper samples, papers produced from harmful plant species in Europe, such as Japanese Knotweed and Canadian Goldenrod, were used. In this research, methods were developed to produce bio-based adhesive solutions in combinations of tannic acid, chitosan, and shellac. The results showed that the viscosity and adhesive strength of the adhesives were best in solutions with added tannic acid and shellac. The tensile strength with adhesives of tannic acid and chitosan was 30% better than with commercial adhesives and 23% for combinations of shellac and chitosan. For paper from Japanese Knotweed and Canadian Goldenrod, the most durable adhesive was pure shellac. Because the surface morphology of the invasive plant papers was more open and had numerous pores compared to the commercial papers, the adhesives penetrated the paper structure and filled the voids. There was less adhesive on the surface and the commercial papers achieved better adhesive properties. As expected, the bio-based adhesives also showed an increase in peel strength and exhibited favorable thermal stability. In summary, these physical properties support the use of bio-based adhesives use in different packaging applications. [ABSTRACT FROM AUTHOR]

This research explores the enhancement of mechanical properties in material architectures, such as strength-to-weight ratio and resilience, through the inspiration of natural systems. Historically, designs for additive manufacturing have relied on simple, repetitive structures like honeycombs, often leading to unnecessary material expenditure. This study aims to examine the compressive mechanical attributes of designs inspired by natural systems, including bird nests, cocoons, and the layered structure of skull bones. Through a comparative analysis, we assessed peak load capacity, strength-to-weight ratio, and resilience between these bioinspired architectures and a standard 3D infill pattern utilized in additive manufacturing. Findings indicate that structures inspired by sandwiched bone layers excel in resilience and peak load, whereas those based on bird nests are notably lighter and, in some cases, exhibit the highest strength-to-weight ratio. The insights provided here will help design engineers with empirically backed mechanical properties of bioinspired architectures, offering a novel methodology for the development of material systems influenced by biological paradigms.

Environmental concerns push for a reduction in greenhouse gas emissions and technologies with a low carbon footprint. In the transportation sector, this drives the transition toward electric vehicles (EVs), which are nowadays mainly based on lithium-ion batteries (LIBs). As the number of produced EVs is rapidly growing, a large amount of waste batteries is expected in the future. Recycling seems to be one of the most promising end-of-life (EOL) methods; it reduces raw material consumption in battery production and the environmental burden. Thus, this work introduces a comprehensive pre-recycling material characterization of waste nickel-manganese-cobalt (NMC) LIB cells from a fully electric battery electric vehicle (BEV), which represents a basis for cost-effective and environmentally friendly recycling focusing on the efficiency of the implemented technique. The composition of the NCM 622 battery cell was determined; it included a LiNi0.6Co0.2Mn0.2O2 spinel on a 15 μm Al-based current collector (cathode), a graphite layer on 60 μm copper foil (anode), 25 μm PE/PVDF polymer separator, and a LiPF6 salt electrolyte with a 1:3 ratio in primary solvents DMC and DEC. The performed research was based on a series of X-ray, infrared (IR) measurements, gas chromatography–mass spectrometry (GC-MS), and inductively coupled plasma–optical emission spectrometry (ICP-OES) characterization of an aqueous solution with dissolved electrolytes. These results will be used in subsequent works devoted to optimizing the most suitable recycling technique considering the environmental and economic perspectives. [ABSTRACT FROM AUTHOR]

This paper presents an investigation of wooden artworks from the collection of the National Gallery Prague created by Monogrammist IP–one of the top carvers of the Salzburg-Passau region at the beginning of the 16th century. His wood reliefs were examined to gain a better understanding of the historical techniques used in medieval art workshops. The internal structure of the small relief Visitation was analysed using computed tomography. Tomographic reconstruction made it possible to distinguish wood species, observe the internal structure of the artwork in detail, study the technological procedures and identify earlier repairs, additions and damages. Tomographic investigation proved the use of four types of wood on the relief Visitation, most likely pear, lime, unspecified softwood and other different species used for joining dowels. A combination of non-invasive and micro-destructive analytical techniques was employed for the chemical characterisation of the materials in the surface layers of the artworks. Photomicrographs of the surface were taken to provide material for the initial investigation. Non-invasive material research was conducted using a portable X-ray fluorescence analyser and, in selected cases, an external reflection infrared spectrometer. The detailed analyses on the micro-samples was carried out by optical microscopy, micro-Raman spectroscopy, Fourier transform infrared spectroscopy, scanning electron microscopy coupled with energy dispersive X-ray spectrometry and gas chromatography with mass spectrometry. A glaze layer based on protein with earth pigment was identified on the relief Christ the Saviour from Death. [ABSTRACT FROM AUTHOR]

Copyright of Fórum pro Konzervátory-Restaurátory is the property of Technical Museum in Brno and its content may not be copied or emailed to multiple sites or posted to a listserv without the copyright holder's express written permission. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract. (Copyright applies to all Abstracts.)

Not many manuscript maps have been the object of material analysis so far. A portolan chart, signed and dated by Juan Vespucci in 1520, was studied in this research, conserved at the Archivo General de Indias in Seville (Spain). It is made on parchment and depicts the coasts and islands of Europe and Africa. It is the oldest portolan chart made in Seville, being unusual in applying hand stamp for decorative figures. The map was analysed by different non-invasive techniques: infra-red and ultraviolet light, digital microscope and X-ray fluorescence (XRF). The main goals of this study were to identify the materials used, as well as to detect retouching or restoration work. Results showed that the entire parchment was first covered with a white layer made of lead white (Pb), calcite or gypsum (Ca). The principal pigments used were vermilion (Hg), yellow ochre (Fe), azurite (Cu) and a copper-based green pigment (Cu) and carbon black. The letters were probably written with an iron-gall ink (Fe, Cu). Very thin golden leaves were applied on a mixtion glue for gilded wind roses. Several retouches from the 19th/20th centuries were found using zinc and titanium whites and probably cobalt blue. [ABSTRACT FROM AUTHOR]

Abstract Copper indium gallium diselenide (CIGS) based technology is actively competing in the global photovoltaic market with high conversion efficiency. Commercial CIGS modules are anticipated to perform on rated output in the field condition for 20 years. Potential induced degradation (PID) is considered as one of the critical concerns among all the current reliability assessment issues. PID accelerated tests have been performed on pre‐commercial CIGS modules to investigate reduction in electrical performance. We report the severe reduction in electrical performance after PID is correlated to the microstructural and chemical properties of the constituent materials. Under extreme PID stress, the cell surface reveals various defects including crater formation. The aim of this article is to explore the consequences of PID induced craters on the efficiency of CIGS solar cells by investigating material degradation kinetics. In this perspective, we present the root cause of PID in CIGS thin‐film modules in relation to microstructural defects by detailed investigation using J‐V analysis, field emission scanning electron microscope (FESEM), Raman spectroscopy, X‐Ray diffraction (XRD), X‐ray photoelectron spectroscopy (XPS) and photoluminescence spectroscopy (PL). This analysis can provide more effective and sustainable research strategies to cultivate more efficient and reliable CIGS technologies in the long run.

Research interest in ceramic materials increased due to their extensive environmental, biomedical, and electronic applications. Increased demand for ceramics with specialized experimental conditions and limited resources has resulted in a higher cost for scientific practices and applications. Enormous material data is accumulated from traditional and high‐tech experimentation, but the manual recording process has shown inconsistencies in the analysis results. Recently, application based on artificial intelligence (AI) and machine learning has been able to address the issues of traditional scientific experiments in material science. However, no machine learning mechanisms are proposed for sophisticated data preparation and AI‐based discovery application of ceramics. This paper proposed an intelligent material data preparation mechanism based on ensemble learning for AI‐assisted material screening and discovery. The current method can potentially resolve the problems of missing and inconsistent material data. As a case study, a material data preparation platform for ceramic material data pre‐processing is developed. For performance evaluation of the proposed mechanism, machine learning regression models are trained before and after the imputation techniques applied to the data. Performance analysis shows that the ensemble model of deep learning network (DNN) and automated machine learning (autoML) performed better as compared to previously reported imputation approaches. [ABSTRACT FROM AUTHOR]

Polymer insulators using silicone rubber materials as sheds and sheaths are widely used in power systems to replace traditional porcelain and glass insulators which are heavy, inconvenient to install, and prone to pollution flashover. However, in recent years, polymer insulators that have been operating in harsh outdoor environments for many years have experienced different degrees of aging. The aging degree and aging products of silicone rubber are the focus of research. Fourier transform infrared spectroscopy (FTIR) is a technical method to analyze the internal molecular bonds and functional groups of materials, and it is often used to study the aging degree and aging products of silicone rubber. In this paper, the aging characteristics of silicone rubber samples in a high altitude area, salt fog environment, and acid environment were studied by FTIR. The results showed that the silicone rubber in a harsh environment, such as strong radiation, salt fog, and acid fog was degraded to some extent, and its main chain was cut off, the degree of polymerization was reduced, and the content of hydrophobic functional groups was reduced. Infrared spectroscopy can be used to analyze the aging phenomenon of polymers. [ABSTRACT FROM AUTHOR]

Invasive plant species can impede the establishment and growth of native plants and affect several ecosystem properties. These properties include soil cover, nutrient cycling, fire regimes, and hydrology. Controlling invasive plants is therefore a necessary, but usually expensive, step in restoring an ecosystem. The sustainability of materials with an emphasis on the use of local resources plays an important role in the circular economy. The use of alternative fibers from invasive plants promotes local production in smaller paper mills that offer the protection of local species and the reduction of waste and invasive plants. A synthesis of the literature is needed to understand the various impacts of invasive plants and their practical control in the context of papermaking applications and to identify associated knowledge gaps. To improve our understanding of the practical application of invasive species in the paper industry, we reviewed the existing literature on invasive plant species in the area of fiber production, printability, coating solution production, dyes, and extracts, and collected information on the major invasive plant species in Europe and the methods used for various applications. [ABSTRACT FROM AUTHOR]

Copyright of Conservar Património is the property of Associacao Profissional de Conservadores-Restauradores de Portugal and its content may not be copied or emailed to multiple sites or posted to a listserv without the copyright holder's express written permission. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract. (Copyright applies to all Abstracts.)

Mural cycles in the churches of Plešivec, Čhyžné, and Štitnik from around 1400 were studied from the material and technical point of view. Stylistically, they show a mixture of Northern and Southern European stylistic currents, which were characteristic for the time around 1400 in East Central Europe. After a precise study in situ, an analysis of extracted samples was conducted by OM, SEM-EDX, and XRD. The plasters used for these murals were all made of lime and sand with different impurities; importantly, they different among each other in terms of their quality and stability. The pigments that were used in these murals were natural and organic: lime white, yellow and red earths, malachite, and azurite were identified, and some pigment degradations were also pointed out. The principal technique is a fresco, but all murals were finished a secco in different proportions, using an organic binder. Painting procedures and modelling were also studied, revealing a strong difference among all three cycles. The painting technique does not always correspond to the style.

In recent years, varying degrees of surface pulverization had been found on composite insulators running for years in severe outdoor environment such as dry, high altitude, salt fog and intensive ultraviolet radiation. Research on the basic characteristics of powdered substance is essential to maintain a high reliability of the power grid. In this study, the characteristics of the powdered layer of the composite insulator sheds aged for more than 10 years under three different environmental stresses are analyzed. The results show that powdered substance of each composite insulator sample contains two parts: the organic silicon which is oxidative degradation product of the original material polydimethylsiloxane (PDMS), and the partially dehydrated and deteriorated flame retardant filler aluminum hydroxide (ATH). However, the thickness of the powdered layer, the particle size distribution of the powdered substance and the composition ratio between the two components are different. The average particle size of powdered substance is between 2–7 μm. The content of Al element is 31.8–34.5%, the content of Si element is 12.7–17.5%, and the mass fraction ratio of two types of powdered substance is about 1/2–1/3. The essence of pulverization is finally concluded that the composite insulator is severely oxidized and degraded under the effect of various aging factors. The organic component silicone rubber is decomposed to fragments, and the bonding between inorganic flame retardant filler and polymer become weak. They will be detached from the main body skeleton and lost partly, then build up at the surface, forming powdered layer.

Dust has been collected and characterized by various methods during the 2021 first experimental campaign in EAST tokamak. It was found that the weight of the in-vessel dust collected at the mid-plane port varied from about 265 mg to about 966 mg. And the dust appeared mainly in the shape of spheroids, flakes, stripes and irregular-shaped particles with the sizes ranging from micrometers to several millimeters. The dust consisted of different elements, which was from the wall-conditioning, erosion of plasma-facing materials (PFMs) as well as the flaking of deposits. The dust collected from the lower port K contained different elements from those collected from the in-vessel port K, with more Fe in the lower port and more Li in the vacuum vessel. The ferromagnetic dust with different shape has been found, and different shape has different O content and size. By using the diagnostic observation window, dust was firstly collected during the campaign and the local dust production rate is calculated, which is found to decrease as the plasma operation goes.

In prosthetic joint surgery, Ag coating of implant areas in direct contact with bone has been met with hesitation for fear of compromising osseointegration. The physicochemical, antibacterial and osteoconductive properties of three different Ti samples were studied: Ti6Al4V alloy that was grit-blasted (GB), Ti6Al4V alloy with an experimental Ti-Ag-nitride layer (SN) applied by physical vapour deposition (PVD) and commercially available PVD-coated Ti6Al4V alloy with a base Ag layer and a surface Ti-Ag-nitride layer (SSN, clinically known as PorAg®). Ag content on the surface of experimental SN and SSN discs was 27.7 %wt and 68.5 % wt, respectively. At 28 d, Ag release was 4 ppm from SN and 26.9 ppm from SSN substrates. Colonisation of discs by Staphylococcus aureus was the highest on GB [944 (± 91) × 104 CFU/mL], distinctly lower on experimental SN discs [414 (± 117) × 104 CFU/mL] and the lowest on SSN discs [307 (± 126) × 104 CFU/mL]. Primary human osteoblasts were abundant 28 d after seeding on GB discs but their adhesion and differentiation, measured by alkaline-phosphatase production, was suppressed by 73 % on SN and by 96 % on SSN discs, in comparison to GB discs. Thus, the PVD-applied Ag coatings differed considerably in their antibacterial effects and osteoconductivity. The experimental SN coating had similar antibacterial effects to the commercially available SSN coating while providing slightly improved osteoconductivity. Balancing the Ag content of Ti implants will be vital for future developments of implants designed for cementless fixation into bone.

Analytical techniques play a fundamental role in heritage science. Among them, Particle Induced X-ray Emission (PIXE) and X-ray Fluorescence (XRF) techniques are widely used in many laboratories for elemental composition analysis. Although they are well-established, a strong effort is put on their upgrade, making them suitable for more and more applications. Over the years, at the INFN-LABEC (the laboratory of nuclear techniques for the environment and cultural heritage of the Italian National Institute of Nuclear Physics), the INFN-CHNet group, the network devoted to cultural heritage, has carried out many technological improvements to the PIXE and XRF set-ups for the analysis of works of art and archaeological finds. Among the many, we recall here the scanning external microbeam facility at the TANDEM accelerator and the MA-XRF scanner. The two instruments have shown complementary features: the former permits quantitative analysis of elements heavier than sodium, which is not possible with the latter in most of the case studies. On the contrary, the scanner has the undeniable advantage of portability, allowing it to work in situ. In this framework of technological developments in heritage science, INFN, CERN, and OPD are jointly carrying on the MACHINA (Movable Accelerator for Cultural Heritage In-situ Non-destructive Analysis) project for on-site Ion Beam Analysis (IBA) studies on cultural heritage. [ABSTRACT FROM AUTHOR]

The wear analysis is a basic step for assessment of the functioning of mechanical systems and helps to the products improvement. The service life of the assemblies is approximate depending on the level of wear of their components. Starting from the product prototype phase, all components are tested and very carefully analyzed. This kind of analysis depends on the fault type and also the analysis devices are chosen in view of this. The Scanning Electron Microscope is one of the most used equipment which provides images with very good resolution at nanometers sizes. The classic microscopes are very often used for surface analysis or measurements. Hardness tester and adhesion measurements devices help to evaluate the material hardness and coatings adhesion. The improvement of the wear analysis methods is necessary due to continuing evolution of the materials and production processes. This paper presents the most common wear types from the injection high-pressure pumps and their analysis methods. [ABSTRACT FROM AUTHOR]

This research interprets the marginalized neighborhood of Serrinha as a place in the city of Florianópolis, Brazil, by examining the relations between the physical neighborhood and internal social networks. I use concepts from the anthropology of materiality and an interdisciplinary understanding of place attachment to examine how the social and physical dimensions of place coalesce within Serrinha. I employ data from eight weeks of ethnographic research and Scannell and Gifford’s tripartite model of place attachment to frame the everyday experiences and affects of Serrinha residents, especially to illustrate Serrinha outside of the typical stereotypes of favelas. In doing so, the study analyzes the symbolic significance of brick as the material of choice for Serrinha’s self-built houses and asserts that the brick is a metaphor for local and global relationships. Ultimately, this research argues that autoconstruction of the house with brick constitutes a significant social and emotional process of attachment in Serrinha.