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27. Investigation of the Dissolution Behavior of AlN in CaO–Al2O3–MgO Refining Slag and CaO–Al2O3–F–Li2O–BaO Mold Flux.

Author

Wang, Jinlong, Xue, Zhengliang, and Song, Shengqiang

Subjects
*LIGHTWEIGHT materials, *STEEL, *STEEL manufacture, *ALUMINUM oxide, *ABSORPTION
Abstract

Low‐density steels have garnered widespread attention as novel lightweight materials. Owing to its high Mn and Al content, brittle AlN inclusions, detrimental to both steelmaking and steel properties, can precipitate directly from the molten steel. Employing slag absorption effectively removes these floating AlN inclusions from the molten steel. Herein, a series of analytical methods are utilized to investigate the dissolution behavior of AlN in CaO–Al2O3–MgO refining slag and CaO–Al2O3–F–Li2O–BaO mold flux. The results indicate that the initial dissolution temperatures of AlN in the slag and mold flux are 1361 and 1080 °C, respectively. The dissolution in the refining slag is attributed to the high‐temperature self‐decomposition of AlN, producing N2(g). In the mold flux, the dissolution reaction involves both the high‐temperature self‐decomposition of AlN and its reaction with Li2O in mold flux, generating N2(g) and Li(g). No reaction interface is observed at the AlN‐slag/mold flux boundary. As the dissolution mass of AlN in the slag/mold flux increases, the Al2O3 content in the slag/mold flux rises. The main phases in slag transition from Ca9(Al6O18) to Ca12Al14O33 and Ca3Al2O6. In the mold flux, the LiBaF3 phase disappears, and the 11CaO·7Al2O3·CaF2 phase, which can degrade the flux's physicochemical properties, becomes the dominant phase. [ABSTRACT FROM AUTHOR]

Published
2024
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38. Evolution of physicochemical properties of quick lime at converter-smelting temperature

Author

Zhang Mengxu, Li Jianli, Xue Zhengliang, Zhu Renlin, Mou Qiqiang, and Zhu Hangyu

Subjects
quick lime, reactivity, cao crystal, porosity, f-cao, Technology, Chemical technology, TP1-1185, Chemicals: Manufacture, use, etc., TP200-248
Abstract

The volume stability caused by the hydration of f-CaO is one of the main obstacles to the comprehensive utilization of steel-making slag. In view of the f-CaO produced by incomplete dissolution of lime, it is necessary to strengthen the dissolution behavior of lime in the converter process. The reactivity of lime determines the dissolution efficiency and is closely related to its microstructure. The experimental results show that the reactivity and porosity of quick lime decrease and the average diameter of pore increases with an increase in temperature. The CaO crystals gradually grow up under the action of grain boundary migration. When the temperature increased from 1,350 to 1,600°C, the lime reactivity decreased from 237.60 to 40.60 mL, the porosity decreased from 30.55 to 15.91%, the average pore diameter increased from 159.10 to 1471.80 nm, and the average CaO particle size increased from 0.33 to 9.61 µm. The results indicate that reactivity is decreased because of the deformation and growth of CaO crystals and the decrease in porosity in reactive lime. This will cause an obstacle to the dissolution of lime and is not conducive to the control of f-CaO in slag.

Published
2021
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