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Because the physical properties of carbon fiber and glass fiber are very different, the fiber volume fraction in carbon/glass hybrid fiber composites cannot be tested by burning method or digestion method, respectively. Furthermore, these methods partially consume the fiber, especially for carbon fibers. To investigate the fiber volume fraction in carbon/glass hybrid fiber composites correctly, the test method is put forward. The burning method and the digestion method were combined to calculate the volume fraction of carbon fiber and glass fiber, respectively. The results show that the relative error between the measured value and the theoretical value is very small. The result of the present work implies that the feasibility and accuracy of this method through experimental verification. [ABSTRACT FROM AUTHOR]