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Due to variations in chemical composition and production processes, homonymous austenitic stainless steels can differ significantly regarding their initial microstructure, metastability, and thus, their fatigue behavior. Microstructural investigations and fatigue tests have been performed in order to evaluate this aspect. Three different batches and production forms of nominally one type of steel AISI 347 were investigated under monotonic tensile tests and cyclic loading under total strain and stress control in low and high cycle fatigue regimes, respectively. The deformation induced α'-martensite formation was investigated globally by means of in situ magnetic measurements and locally using optical light microscopy of color etching of micrographs. The investigation showed that the chemical composition and the different production processes influence the material behavior. In fatigue tests, a higher metastability and thus a higher level of deformation induced α'-martensite pronounced cyclic hardening, resulting in significantly greater endurable stresses in total strain-controlled tests and an increase in fatigue life in stress-controlled tests. For applications of non-destructive-testing, detailed knowledge of a component's metastability is required. In less metastable batches and for lower stress levels, α'-martensite primarily formed at the plasticization zone of a crack. Furthermore, the formation and nucleation points of α'-martensite were highly dependent on grain size and the presence of δ-ferrite. This study provides valuable insights into the different material behavior of three different batches with the same designation, i.e., AISI 347, due to different manufacturing processes and differences in the chemical composition, metastability, and microstructure. [ABSTRACT FROM AUTHOR]

The oxide layer development of X6CrNiNb18-10 (AISI 347) during exposure to high-temperature water has been investigated. Stainless steels are known to form a dual oxide layer in corrosive environments. The secondary Fe-rich oxide layer has no significant protective effect. In contrast, the primary Cr-rich oxide layer is known to reach a stabilized state, protecting the base metal from further oxidation. This study's purpose was to determine the development of oxide layer dimensions over exposure time using SEM, TEM and EDX line scans. While a parabolic development of Cr in the protective primary layer and Fe in the secondary layer was observed, the dimensions of the Ni layer remained constant. Ni required the presence of a pronounced Fe-rich secondary layer before being able to reside on the outer secondary layer. With increasing immersion time, the Ni element fraction surpassed the Cr element fraction in the secondary layer. Oxide growth on the secondary layer could be observed. After 480 h, nearly the entire surface was covered by the outer oxide layer. In the metal matrix, no depletion of Cr or Ni could be observed over time; however, an increased presence of Cr and Ni in the primary layer was found at the expense of Fe content. The Nb-stabilized stainless steel was subject to the formation of Niobium pentoxide (Nb2O5), with the quantity and magnitude of element fraction increasing over exposure time. [ABSTRACT FROM AUTHOR]

Friction stir welding, as a solid-state welding technique, is especially suitable for effectively joining high-strength aluminum alloys, as well as for multi-material welds. This research investigates the friction stir welding of thin aluminum and steel sheets, an essential process in the production of hybrid tailor-welded blanks employed in deep drawing applications. Despite its proven advantages, the welding process exhibits variable outcomes concerning formability and joint strength when utilizing an H13 welding tool. To better understand these inconsistencies, multiple welds were performed in this study, joining 1 mm thick steel to 2 mm thick aluminum sheets, with a cumulative length of 7.65 m. The accumulation of material on the welding tool was documented through 3D scanning and weighing. The integrity of the resulting weld seam was analyzed through metallographic sections and X-ray imaging. It was found that the adhering material built up continuously around the tool pin over several welds totaling between 1.5 m and 2.5 m before ultimately detaching. This accretion of material notably affected the welding process, resulting in increased intermixing of steel particles within the aluminum matrix. This research provides detailed insights into the dynamics of friction stir welding in multi-material welds, particularly in the context of tool material interaction and its impact on weld quality. [ABSTRACT FROM AUTHOR]

The aim of the paper is to investigate experimentally the fatigue and creep-fatigue material behaviour of improved materials and welded joints for the application in flexible future power plants. These materials promise a reduction in manufacturing costs as well as an increase in flexibility by providing enhanced creep strength thorugh a wall thickness reduction. At the temperature range between 500°C −550°C, the investigation focusses on the creep and low-cycle fatigue behaviour of dissimilar welded joints from conventional materials (bainitic and martensitic materials T24 and T92) to nickel-based alloys (A617B and HR6W) fabricated as tubes. At the temperature range between 700°C and 750°C, it focusses on the creep, low-cycle fatigue and creep-fatigue behaviour of similar and dissimilar welded joints from nickel-based alloys (A740H, A617B and A263) fabricated as tubes and as pipes. Metallographic investigations after testing provide support for understanding the influence of temperature, strain amplitude and dwell time on the microstructure change and the fatigue strength. [ABSTRACT FROM AUTHOR]

The microstructural anisotropy caused by the highly oriented solidification of the metal Laser Powder Bed Fusion (PBF-LB/M) process affects mechanical short- and long-term properties. Component build orientation influences grain morphology and orientation, and thus, mechanical properties. While the creep behaviour of samples manufactured parallel and perpendicular to the build direction are studied intensively, the 45° build orientation remains uncharacterised. In this study, IN738LC creep samples are manufactured via PBF-LB/M in three build orientations (0°, 45° and 90°). While the results of 90° and 0° are as expected, where 90° achieves the longest time to rupture and largest rupture strain, the 45° specimen shows the least fracture time. Differences in microstructure and twinning behaviour are identified as one of the root causes for this unexpected behaviour. This study discusses the correlation between microstructure, twinning and build orientation and their effect on creep behaviour, with special focus on the 45° build orientation. [ABSTRACT FROM AUTHOR]

The experimentally observed short fatigue crack growth rate of an uncharged specimen tested in air is compared with results obtained from specimens tested in 10 MPa hydrogen atmosphere and specimens previously charged with hydrogen. To further discuss the hydrogen related short propagation mechanisms, a simulation approach for predicting short fatigue crack growth is presented. The boundary element method is used for calculating stresses and displacements in an anisotropic elastic solid. The hydrogen concentration is assumed to be homogeneously distributed in the microstructure. Based on this modelling approach, it could be concluded that hydrogen leads to an increasing short fatigue crack growth rate due to increasing irreversible deformation processes at the crack tip and also promotes grain boundary cracking in specimens tested in 10 MPa hydrogen atmosphere.

The paper focuses on experimental and numerical fatigue assessment procedures to evaluate the influence of multi-axial stress state caused by high centrifugal forces superimposed with bending loads due to blade vibrations on the lifetime of end stage blades from steam turbines. The experimental investigations on original-sized end stage blades were carried out on a test rig specially developed for high forces and multicomponent force application. This was based on detailed numerical simulations by the MPA University of Stuttgart. During the fractographic postexaminations of the tested blades using magnetic particle inspection, light and scanning electron microscopes, two competing damage mechanisms were identified that occurred at different locations. Numerical investigations by means of elastic-plastic finite element analyses were carried out to estimate the local stress conditions acting in the blade root. The local stresses and strains were postprocessed using the critical plane approach and advanced multi-axial fatigue damage parameters. Due to the high stress gradients at the edge of contact, over-conservative predictions may result if their effects are not taken into account. Based on the critical plane method in conjunction with fatigue damage parameters, an approach taking the stress gradient into consideration was developed to predict the fatigue life of the end stage blades. The approach is verified by the component tests on original-sized blades. [ABSTRACT FROM AUTHOR]