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The resistivity of a coarse grain steel against fatigue crack initiation in presence of micro-defects is discussed. Samples of material with martensitic microstructure were prepared by adequate thermal treatment. Microstructurally small Vickers indentations were used as artificial micro-defect. The compressive residual stresses are due to the irreversibility of plastic deformation. The moment of indenting enables to prepare samples with and without effects of residual stresses. The stress level for crack initiation depends on the actual indentation size. The location of initiated cracks is affected by the presence and character of residual stresses.

Structural components which are loaded in cyclic load mostly fail due to fatigue. The fatigue strength of metals as well as weld joint regions in metals depends on mechanical properties especially hardness, the size of defect and the size of grains. Resistivity of the fine grain HAZ prepared against fatigue crack initiation will be explained in this article. Samples of material with martensitic fine grain microstructure were prepared by laboratory furnace by proper thermal treatment. Mechanical properties of fine grain heat affected zone and its microstructure were investigated. Special attention was given to behavior of fine grain during the cycle loading under stress concentration. Stress concentration was similar to the one in real welds. The S-N curve and the fatigue limit were determined. The Paris curve and the threshold for crack propagating were also determined. [ABSTRACT FROM AUTHOR]

The analysis of the energy of fracture of specimens from steel OSL, which is widely used for the manufacture of railway axles under shock loading, is performed. The nature and quantitative parameters of the typical stages of the processes of plastic and brittle fracture, depending on the test temperature and stiffness of the stress state at the tip of the crack-like defect, are established. It is shown that impact loading at 20 °C leads to the formation of the local zone of plasticity and ductile-brittle fracture of the material. An increased stiffness of the stress state at the tip of the defect at −40 °C causes brittle fracture. An approach is developed, which is based on using the size of shear lips as a quantitative parameter of fracture under normal and low temperatures, similar in its physical essence to deformation approaches of nonlinear fracture mechanics. Based on this approach and the quantitative analysis of specimen fracture zones, the physical and mechanical scheme of specimen fracture is proposed in the presence of localized plasticity and in its absence near the tip of the concentrator. [ABSTRACT FROM AUTHOR]

This paper presents research experience related to implementation of vibrations on residual stress relief with the equipment for treatment by vibration method. The paper provides explanation of effects achieved by vibration method when implemented during welding, and elaborates advantages and disadvantages of that method applied after welding process. In order to present effects of vibration on solid structures, there was experimental analysis performed and compared with heat treatment. [ABSTRACT FROM AUTHOR]

This paper presents weld thermal cycle simulation of high strength steel S960QL, and describes influence of cooling time t8/5 on hardness and impact toughness of weld thermal cycle simulated specimens. Furthermore, it presents analysis of characteristic fractions done by electron scanning microscope which can contribute to determination of welding parameters for S960QL steel. [ABSTRACT FROM AUTHOR]

The paper presents impact energy results of thermal cycle simulated specimens of quenched and tempered fine grain structural steel S960QL. These results are obtained by examining notched Charpy specimens. Upon performed metallographic analysis and measured hardness, total impact energy is separated into ductile and brittle components. [ABSTRACT FROM AUTHOR]

Fatigue crack growth and fracture mechanics analysis of a working roll surface layer material is presented in this paper. The research is done on a hot strip mill working roll where High Chromium Steel is used for roll's shell material. To obtain corresponding parameters, a rectangular single edge notched bend specimens - SENB, according to standard BS 7448, were used. The fatigue crack growth analysis was done on a resonant testing machine with use of special crack gauges, while for fracture mechanics parameters the electro-mechanical testing machine was used. [ABSTRACT FROM AUTHOR]

The paper presents research of weldability of microalloyed high strength steels TStE 420 and S960QL after weld thermal cycle simulation. Beside mechanical properties hardness and impact strength, the microstructures of characteristic weld thermal cycled structures for both steels are given. The results will contribure to determination of weakest points in Heat Af ected Zone of both steels. [ABSTRACT FROM AUTHOR]

This paper presents results of a study on martensitic coarse grain heat affected zone that can appear in welded joints. Mechanical properties of martensitic coarse grain heat affected zone and its microstructure were investigated. Special attention was given to its behaviour during the cycle loading under stress concentration. Stress concentration was similar to the one in real welds. The S-N curve and the fatigue limit were determined. The Paris curve and the threshold for crack propagating were also determined. [ABSTRACT FROM AUTHOR]

This paper elaborates results of hardness and impact energy of thermal cycle simulated specimens of high-alloy steel P 91 and their dependence on cooling time from 800 to 500 °C. Results were obtained by measuring hardness HV 1 and by experimental testing of Charpy notched specimens. Metallographic analysis of samples was performed on scanning electronic microscope. [ABSTRACT FROM AUTHOR]

The paper deals with research into dependence of hardness and impact energy of thermal cycle simulated specimens of fine-grained structural steel S960QL on cooling time from 800 to 500 °C and on tested temperature. Results were obtained by measuring hardness of HV 10 and by experimental testing of Charpy notched tubes on instrumented Charpy hammer. Total impact energy, initiation energy and fracture propagation energy needed for occurrence of fracture is also elaborated. [ABSTRACT FROM AUTHOR]

The aim of this work is to study joining Al 2024-T3 alloy plates with different welding procedures. Aluminum alloy AA 2024-T351 is especially used in the aerospace industry. Aluminum plates are welded by the TIG and MIG fusion welding process, as well as by the solid-state welding process, friction stir welding (FSW), which has recently become very important in aluminum and alloy welding. For welding AA2024-T35 with MIG and TIG fusion processes, the filler material ER 4043-AlSi 5 was chosen because of reduced cracking. Different methods were used to evaluate the quality of the produced joints, including macro- and microstructure evaluation, in addition to hardness and tensile tests. The ultimate tensile strength (UTS) of the FSW sample was found to be 80% higher than that of MIG and TIG samples. The average hardness value of the weld zone of metal for the MIG- and TIG-produced AA2024-T3511 butt joints showed a significant decrease compared to the hardness of the base metal AA2024-T351 by 50%, while for FSW joints, in the nugget zone, the hardness is about 10% lower relative to the base metal AA2024-T3511.

Cladding with a stick electrode is one of the oldest arc processes for adding a deposit on a base material. The process is suitable for outdoor working, but the disadvantages are low productivity and large dilution rates. In this work, a simple solution is proposed, which would enable cladding of a larger area with one pass and decrease the dilution rate at the same time-a new type of electrode was developed, exhibiting a rectangular cross-section instead of a round one. Hardfacings, welded with E Fe8 electrodes according to EN 14 700 Standard were welded on mild steel S355 J2 base material with three different coated stick electrodes. The first one was a commercially available, standard, round hardfacing electrode, the second was the same, but with a thinner coating, and the third one was a newly developed rectangular electrode. All three types had equal cross-sections of the metallic core and the same type of coating. Manufacturing of the rectangular electrodes in the laboratory is explained briefly. One- and multi-layer deposits were welded with all three types. Differences were observed in the arc behavior between the round and rectangular electrodes. With the rectangular electrode, the microstructure of the deposit was finer, penetration was shallower, and dilution rates were lower, while the hardness was higher, residual stresses predominantly compressive, and the results of instrumented Charpy impact tests and fracture mechanics tests were better.

The production of personal protective equipment (PPE) has increased dramatically in recent years, not only because of the pandemic, but also because of stricter legislation in the field of Employee Protection. The increasing use of PPE, including disposable surgical masks (DSMs), is putting additional pressure on waste collectors. For this reason, it is necessary to find high-quality solutions for this type of waste. Mechanical recycling is still the most common type of recycling, but the recyclates are often classified as low-grade materials. For this reason, a detailed analysis of the recyclates is necessary. These data will help us to improve the properties and find the right end application that will increase the value of the materials. This work represents an extended analysis of the recyclates obtained from DSMs, manufactured from different polymers. Using surface and morphology tests, we have gained insights into the distribution of different polymers in polymer blends and their effects on mechanical and surface properties. It was found that the addition of ear loop material to the PP melt makes the material tougher. In the polymer blends obtained, PP and PA 6 form the surface (affects surface properties), while PU and PET are distributed mainly inside the injection-molded samples.

We studied the shear bond strength (SBS) of two PEEK composites (BioHPP, BioHPP plus) with three veneering composites: Visio.lign, SR Nexco and VITA VM LC, depending on the surface treatment: untreated, sandblasted with 110 μm Al 2 O 3 , sandblasted and cleaned ultrasonically in 80% ethanol, with or without adhesive Visio.link, with applied Visio.link and MKZ primer. For the BioHPP plus, differential scanning calorimetry (DSC) revealed a slightly lower glass transition temperature ( T g 150.4 ± 0.4 °C) and higher melting temperature ( T m 339.4 ± 0.6 °C) than those of BioHPP ( T g 151.3 ± 1.3 °C, T m 338.7 ± 0.2 °C). The dynamical mechanical analysis (DMA) revealed a slightly higher storage modulus of BioHPP ( E' 4.258 ± 0.093 GPa) than of BioHPP plus ( E ' 4.193 ± 0.09 GPa). The roughness was the highest for the untreated BioHPP plus, and the lowest for the polished BioHPP. The highest hydrophobicity was achieved on the sandblasted BioHPP plus, whereas the highest hydrophilicity was found on the untreated BioHPP. The highest SBSs were determined for BioHPP and Visio.lign, adhesive Visio.link (26.31 ± 4.17 MPa) or MKZ primer (25.59 ± 3.17 MPa), with VITA VM LC, MKZ primer and Visio.link (25.51 ± 1.94 MPa), and ultrasonically cleaned, with Visio.link (26.28 ± 2.94 MPa). For BioHPP plus, the highest SBS was determined for a sandblasted surface, cleaned ultrasonically, with the SR Nexco and Visio.link (23.39 ± 2.80 MPa).

This study presents a comprehensive experimental investigation of the high-cycle fatigue (HCF) behaviour of the ductile aluminium alloy AA 5083-H111. The analysed specimens were fabricated in the rolling direction (RD) and transverse direction (TD). The HCF tests were performed in a load control (load ratio R = 0.1) at different loading levels under the loading frequency of 66 Hz up to the final failure of the specimen. The experimental results have shown that the S-N curves of the analysed Al-alloy consist of two linear curves with different slopes. Furthermore, RD-specimens demonstrated longer fatigue life if compared to TD-specimens. This difference was about 25% at the amplitude stress 65 MPa, where the average fatigue lives 276,551 cycles for RD-specimens, and 206,727 cycles for TD-specimens were obtained. Similar behaviour was also found for the lower amplitude stresses and fatigue lives between 10 6 and 10 8 cycles. The difference can be caused by large Al 6 (Mn,Fe) particles which are elongated in the rolling direction and cause higher stress concentrations in the case of TD-specimens. The micrography of the fractured surfaces has shown that the fracture characteristics were typical for the ductile materials and were similar for both specimen orientations.

The impact and fracture toughness of a nanostructured, kinetically activated bainitic steel was determined using Standard methods. Prior to testing, the steel was quenched in oil and aged naturally for a period of 10 days in order to obtain a fully bainitic microstructure with a retained austenite content below 1%, resulting in a high hardness of 62HRC. The high hardness originated from the very fine microstructure of bainitic ferrite plates formed at low temperatures. It was determined that the impact toughness of the steel in the fully aged condition improved remarkably, whereas the fracture toughness was in line with expectations based on the extrapolated data available in the literature. This suggests that a very fine microstructure is most beneficial to rapid loading conditions, whereas material flaws such as coarse nitrides and non-metallic inclusions are the major limitation for obtaining a high fracture toughness.

Heat-affected zones (HAZs) in real welds are usually quite narrow, and consequently most standard mechanical tests are difficult or even impossible. Therefore, simulated microstructures are often used for mechanical tests. However, the most often used weld thermal cycle simulator produces only a few millimeters wide area of simulated microstructure in the middle of specimens. Consequently, these kind of simulated specimen are not suitable for standard tensile tests, and even for Charpy impact tests, the simulated area can be too narrow. Therefore, to investigate the mechanical properties of a fine-grain heat-affected zone in 18CrNiMo7-6 steel, two methods were used for simulation of as-welded microstructures: (a) a weld thermal cycle simulator, and (b) as an alternative, though not yet verified option, austenitizing in a laboratory furnace + water quenching. The microstructures were compared and mechanical properties investigated. The grain sizes of the simulated specimens were 10.9 μm (water-quenched) and 12.6 μm (simulator), whereby the deviations from the real weld were less than 10%. Both types of simulated specimen were used for hardness measurement, Charpy impact tests, and fatigue tests. Water-quenched specimens were large enough to enable standard tensile testing. A hardness of 425 HV, yield strength R p02 = 1121 MPa, tensile strength R m = 1475 MPa, impact energy KV = 73.11 J, and crack propagation threshold Δ K thR = 4.33 MPa m 0.5 were obtained with the water quenched specimens, and 419 HV, KV = 101.49 J, and Δ K thR = 3.4 MPa m 0.5 with the specimens prepared with the simulator. Comparison of the results confirmed that the annealed and quenched specimens were suitable for mechanical tests of FG HAZs, even for standard tensile tests. Due to the use of simulated test specimens, the mechanical properties determined can be linked to the FG HAZ microstructure in 18CrNiMo7-6 steel.

In order to ensure a quality welded joint, and thus safe operation and high reliability of the welded part or structure achieved by friction stir welding, it is necessary to select the optimal welding parameters. The parameters of friction stir welding significantly affect the structure of the welded joint, and thus the mechanical properties of the welded joint. Investigation of the influence of friction stir welding parameters was performed on 6-mm thick plates of aluminum alloy AA2024 T351. The quality of the welded joint is predominantly influenced by the tool rotation speed n and the welding speed v. In this research, constant tool rotation speed was adopted n = 750 rpm, and the welding speed was varied ( v = 73, 116 and 150 mm/min). By the visual method and radiographic examination, imperfections of the face and roots of the welded specimens were not found. This paper presents the performed experimental tests of the macro and microstructure of welded joints, followed by tests of micro hardness and fracture behavior of Friction Stir Welded AA2024-T351 joints. It can be concluded that the welding speed of v = 116 mm/min is favorable with regard to the fracture behavior of the analysed FSW-joint.

The nanocomposites were prepared by synthesizing (2,2,6,6-tetramethylpiperidin-1-yl)oxyl (TEMPO)-oxidized cellulose nanofibrils (TCNFs) or cellulose nanocrystals (CNCs) with hydroxyapatite (HA) in varying composition ratios in situ. These nanocomposites were first obtained from eggshell-derived calcium and phosphate of ammonium dihydrogen orthophosphate as precursors at a stoichiometric Ca/P ratio of 1.67 with ultrasonication and compressed further by a uniaxial high-pressure technique. Different spectroscopic, microscopic, and thermogravimetric analyses were used to evaluate their structural, crystalline, and morphological properties, while their mechanical properties were assessed by an indentation method. The contents of TCNF and CNC were shown to render the formation of the HA crystallites and thus influenced strongly on the composite nanostructure and further on the mechanical properties. In this sense, the TCNF-based composites with relatively higher contents (30 and 40 wt %) of semicrystalline and flexible TCNFs resulted in smoother and more uniformly distributed HA particles with good interconnectivity, a hardness range of 550-640 MPa, a compression strength range of 110-180 MPa, an elastic modulus of ~5 GPa, and a fracture toughness value of ~6 MPa 1/2 in the range of that of cortical bone. Furthermore, all the composites did not induce cytotoxicity to human bone-derived osteoblast cells but rather improved their viability, making them promising for bone tissue regeneration in load-bearing applications.