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1. Crystal structure of (diaqua-bis(phenanthroline-K 2 N,N′)-tetrakis(m 2-3,4,5,6-tetrafluorophthalato-K 4 O,O:O′:O″;K 2 O:O′)dierbium (III) phenanthroline (1/2), C80H38Er2F16N8O18

Author

Song Jun-Ya, Zhang Xiao-Yu, Zhang Chun-Li, Zhao Bei-Bei, Huang Shi-Jie, and Liu Xinfang

Subjects
2235105, Physics, QC1-999, Crystallography, QD901-999
Abstract

C80H38Er2F16N8O18, triclinic, P1‾ $P\overline{1}$ (no. 2), a = 11.4228(4) Å, b = 12.6712(3) Å, c = 13.2663(4) Å, α = 102.660(2)°, β = 98.047(3)°, γ = 105.509(3)°, V = 1764.54(10) Å3, Z = 1, R gt(F) = 0.0311, wR ref(F 2) = 0.0668, T = 293(2) K.

Published
2023
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2. Crystal structure of diaqua-diphenanthroline-κ2 N,N′-bis(μ2-2-carboxy-3,4,5,6-tetrafluorobenzoato-κ2 O:O′)-bis(μ2-tetrafluorophthalato-κ3 O,O′:O′)didysprosium(III) – phenanthroline (1/2), C80H38Dy2F16N8O18

Author

Zhang Xiao-Yu, Zhao Bei-Bei, Huang Shi-Jie, Song Jun-Ya, and Liu Xin-Fang

Subjects
2153477, Physics, QC1-999, Crystallography, QD901-999
Abstract

C80H38Dy2F16N8O18, triclinic, P1‾ $P\overline{1}$ (no. 2), a = 11.3924(5) Å, b = 12.7091(4) Å, c = 13.2583(5) Å, α = 102.496(3)°, β = 97.955(4)°, γ = 105.588(4)°, V = 1765.36(12) Å3, Z = 2, Rgt (F) = 0.0298, wRref (F 2) = 0.0606, T = 293(2) K.

Published
2022
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3. Crystal structure of acrinidinium tetrafluorohydrogenphthalate, C21H11F4NO4

Author

Liu Xin-Fang, Song Jun-Ya, Zhao Bei-Bei, and Huang Shi-Jie

Subjects
2151627, Physics, QC1-999, Crystallography, QD901-999
Abstract

C21H11F4NO4, triclinic, P1‾ $P\overline{1}$ (no. 2), a = 9.5000(4) Å, b = 13.9989(7) Å, c = 14.1423(5) Å, α = 91.355(4)°, β = 108.542(4)°, γ = 98.958(4)°, V = 1756.02(14) Å3, Z = 4, R gt(F) = 0.0494, wR ref(F 2) = 0.1157, T = 293(2) K.

Published
2022
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4. Crystal structure of (diaqua-bis(phenanthroline-K2N,N′)-tetrakis(m2-3,4,5,6-tetrafluorophthalato-K4O,O:O′:O″;K2O:O′)dierbium (III) phenanthroline (1/2), C80H38Er2F16N8O18

Author

Song, Jun-Ya, Zhang, Xiao-Yu, Zhang, Chun-Li, Zhao, Bei-Bei, Huang, Shi-Jie, and Liu, Xinfang

Subjects
CRYSTAL structure, PHENANTHROLINE, ERBIUM, MANGANESE porphyrins, ERBIUM compounds
Abstract

C80H38Er2F16N8O18, triclinic, P 1 ‾ (no. 2), a = 11.4228(4) Å, b = 12.6712(3) Å, c = 13.2663(4) Å, α = 102.660(2)°, β = 98.047(3)°, γ = 105.509(3)°, V = 1764.54(10) Å3, Z = 1, Rgt(F) = 0.0311, wRref(F2) = 0.0668, T = 293(2) K. [ABSTRACT FROM AUTHOR]

Published
2023
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5. Crystal structure of (diaqua-bis(phenanthroline-K2N,N′)-tetrakis(m2-3,4,5,6-tetrafluorophthalato-K4O,O:O′:O″;K2O:O′)dierbium (III) phenanthroline (1/2), C80H38Er2F16N8O18

Author

Song, Jun-Ya, Zhang, Xiao-Yu, Zhang, Chun-Li, Zhao, Bei-Bei, Huang, Shi-Jie, and Liu, Xinfang

Abstract

C80H38Er2F16N8O18, triclinic, P1‾$P\overline{1}$ (no. 2), a= 11.4228(4) Å, b= 12.6712(3) Å, c= 13.2663(4) Å, α= 102.660(2)°, β= 98.047(3)°, γ= 105.509(3)°, V= 1764.54(10) Å3, Z= 1, Rgt(F) = 0.0311, wRref(F2) = 0.0668, T = 293(2) K.

Published
2023
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6. Crystal structure of diaqua-diphenanthroline-κ2N,N′-bis(μ2-2-carboxy-3,4,5,6-tetrafluorobenzoato-κ2O:O′)-bis(μ2-tetrafluorophthalato-κ3O,O′:O′)didysprosium(III) – phenanthroline (1/2), C80H38Dy2F16N8O18

Author

Zhang, Xiao-Yu, Zhao, Bei-Bei, Huang, Shi-Jie, Song, Jun-Ya, and Liu, Xin-Fang

Subjects
CRYSTAL structure, COORDINATION polymers, ATOMS, PHENANTHROLINE, PICRIC acid, HYDROGEN atom, RARE earth metals
Abstract

In the title complex, there are one Dy(III) ion, one phen ligand, two differently deprotonated tetrafluorophthalato ligands (HTFPA SP - sp and TFPA SP 2- sp , respectively), one coordinated water and one cocrystallized phen in the asymmetric unit. Dy-MOFs can be constructed from Dy(III) ion and carboxylate and nitrogen-containing ligands [[8]], [[9]], [[10]]. Dy1 is nine-coordinated by two N atoms (N1, N2) of the phen ligand, one O atom (O9) from coordinated water, two O atoms (O4, O3A) from two mono-deprotonated HTFPA SP - sp ligands and four O atoms (O6, O8, O5A and O6A) from two fully-deprotonated TFPA SP 2- sp ligands. [Extracted from the article]

Published
2022
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7. Crystal structure of acrinidinium tetrafluorohydrogenphthalate, C21H11F4NO4.

Author

Liu, Xin-Fang, Song, Jun-Ya, Zhao, Bei-Bei, and Huang, Shi-Jie

Subjects
CRYSTAL structure
Abstract

C21H11F4NO4, triclinic, P 1 ‾ (no. 2), a = 9.5000(4) Å, b = 13.9989(7) Å, c = 14.1423(5) Å, α = 91.355(4)°, β = 108.542(4)°, γ = 98.958(4)°, V = 1756.02(14) Å3, Z = 4, Rgt(F) = 0.0494, wRref(F2) = 0.1157, T = 293(2) K. [ABSTRACT FROM AUTHOR]

Published
2022
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8. Crystal structure of diaqua-diphenanthroline-κ2N,N′-bis(μ2-2-carboxy-3,4,5,6-tetrafluorobenzoato-κ2O:O′)-bis(μ2-tetrafluorophthalato-κ3O,O′:O′)didysprosium(III) – phenanthroline (1/2), C80H38Dy2F16N8O18

Author

Zhang, Xiao-Yu, Zhao, Bei-Bei, Huang, Shi-Jie, Song, Jun-Ya, and Liu, Xin-Fang

Abstract

C80H38Dy2F16N8O18, triclinic, P1‾$P\overline{1}$ (no. 2), a= 11.3924(5) Å, b= 12.7091(4) Å, c= 13.2583(5) Å, α= 102.496(3)°, β= 97.955(4)°, γ= 105.588(4)°, V= 1765.36(12) Å3, Z= 2, Rgt(F) = 0.0298, wRref(F2) = 0.0606, T = 293(2) K.

Published
2022
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