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This study investigated the simulated body fluid-assisted stress corrosion cracking (SCC) of an Al-free magnesium alloy (RS66) and a common Al-containing magnesium alloy (AZ91), the former being more suitable for temporary implant applications (however, we used AZ91 for comparison since there are considerable reports on SCC in this alloy). The investigation includes SCC tests under simultaneous conditions of mechanical loading and imposed electrochemical potential that established a combined effect of hydrogen and anodic dissolution as the embrittlement mechanism. Though the RS66 alloy possesses impressive mechanical properties in non-corrosive environments (as a result of its fine grain size), both alloys suffered significant embrittlement when tested in simulated body fluid. The susceptibility of the RS66 alloy to SCC was ~25% greater than that of AZ91, which is attributed to the greater resistance of AZ91 to corrosion/localised corrosion because of its Al content. [ABSTRACT FROM AUTHOR]

This paper forms part of an ongoing investigation into the tools required in linear elastic fracture mechanics (LEFM) for evaluating the durability of components designed for limited life replacement. In this study, we demonstrate that the USAF 'Characteristic K' method, when combined with the Hartman–Schijve adaptation of the NASGRO crack growth formula, can predict the impact of underloads on the propagation of small cracks in aluminum alloy AA7050-T7451 with reasonable accuracy. The published da/dN versus ΔK small crack growth curves associated with five specific underload spectra are examined. It is found that, in each case, there is reasonably good agreement between the predicted and the measured curves. To the best of the author's knowledge, this paper is the first to highlight the ability of the USAF Characteristic K approach, when coupled with the Hartman–Schijve equation, to reasonably accurately predict the growth of small cracks subjected to a range of underload spectra. [ABSTRACT FROM AUTHOR]

The present study examines the high-temperature (500–800 °C) oxidation behavior of Fe-10Cr-(3,5) Al alloys and studies the effect of nanocrystalline structure and Al content on their resistance to oxidation. The nanocrystalline (NC) alloy powder was synthesized via planetary ball milling. The prepared NC alloy powder was consolidated using spark plasma sintering to form NC alloys. Subsequently, an annealing of the NC alloys was performed to transform them into microcrystalline (MC) alloys. It was observed that the NC alloys exhibit superior resistance to oxidation compared to their MC counterparts at high temperatures. The superior resistance to oxidation of the NC alloys is attributed to their considerably finer grain size, which enhances the diffusion of those elements to the metal–oxide interface that forms the protective oxide layer. Conversely, the coarser grain size in MC alloys limits the diffusion of the oxide-forming components. Furthermore, the Fe-10Cr-5Al alloy showed greater resistance to oxidation than the Fe-10Cr-3Al alloy. [ABSTRACT FROM AUTHOR]