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Noval Á.M., Gallach D., García-Tuñón M.A.G., Ferro-Llanos V., Herrero P., Fukami K., Ogata Y.H., Torres-Costa V., Martín-Palma R.J., Ciment-Font A., Silván M.M. and We acknowledge the European Synchrotron Radiation Facility for provision of synchrotron radiation facilities and the MEC and Consejo Superior de Investigaciones Científicas for financial support (PE-2010 6 0E 013). We would like to thank the BM25-SpLine staff for the technical support. This work has been supported by MICINN through projects FIS-2008-06249, MAT2009-14578-C03-02, MAT2008-06858-C02-01, and MAT2008-06858-C02-02, as well as Comunidad de Madrid, project NANOBIOMAGNET (S2009/MAT-1726) and European project MAGNIFYCO (Contract NMP4-SL-2009-228622). Technical support from ICTS Centro Nacional de Microscopia Electrónica (UCM, Madrid) is gratefully acknowleged.

Muñoz-Noval Á., Torres-Costa V., Martín-Palma R.J., Herrero-Fernández P., García M.Á., Fukami K., Ogata Y.H., Silván M.M. and Authors would like to thank the ESRF for time allocation and financial support through experiment MA-1168. The staff of Spline BM25 beamline is acknowledged for assistance and support with the XAS experiments. We also acknowledge funding provided by grant MAT2008-06858-C02-01-02 , FUNCOAT-CSD2008-00023 and FIS-2008-06249 from Ministerio de Ciencia e Innovación (Spain) , Comunidad de Madrid, Grant 'Microseres' and project NANOBIOMAGNET ( S2009/MAT-1726 ). The technical support from L García Pelayo, from Servicio de Microscopía (ICMM-CSIC) and from Esteban Urones at I.C.T.S. Centro Nacional de Microscopía Avanzada (UCM) is gratefully acknowledged.