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4. Hydrothermal synthesis, structure and properties of a new 3D two-fold Co-based coordination framework

Author

Sheng Liangbing, Xiao-Jie Li, Chun-Hua Zhang, Man-Sheng Chen, Lu Weihong, and Yi-Fang Deng

Subjects
Coordination polymer, Hydrothermal reaction, 02 engineering and technology, 010402 general chemistry, 021001 nanoscience & nanotechnology, Electrochemistry, 01 natural sciences, 0104 chemical sciences, Inorganic Chemistry, Pentane, chemistry.chemical_compound, Crystallography, chemistry, Hydrothermal synthesis, Physical and Theoretical Chemistry, 0210 nano-technology, Single crystal
Abstract

A new 3D coordination polymer, [Co2(MIP)2(BMIP)]n (1), [H2MIP = 5-methyl-isophthalic acid, BMIP = 1,5-bis-(2-methyl-imidazol)pentane] has been synthesized and characterized by single crystal X-ray ...

Published
2020
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5. Synthesis, structure, and properties of two coordination polymers constructed from 5-(isonicotinamido)isophthalic acid

Author

Yi-Fang Deng, Man-Sheng Chen, Chun-Hua Zhang, Sheng Liangbing, Xiao-Li Chen, and Pan Zhu

Subjects
chemistry.chemical_classification, Metals and Alloys, Polymer, 010403 inorganic & nuclear chemistry, 01 natural sciences, Hydrothermal circulation, 0104 chemical sciences, Catalysis, Inorganic Chemistry, Isophthalic acid, chemistry.chemical_compound, Crystallography, Adsorption, chemistry, Materials Chemistry, Thermal stability, Organometallic chemistry, Topology (chemistry)
Abstract

Two three-dimensional (3D) coordination polymers, viz. [Ni(INAIP)(Him)(H2O)]·H2O (1) and [Fe(INAIP)(H2O)2]·H2O (2), were synthesized by reaction of 5-(isonicotinamido)isophthalic acid (H2INAIP), NiSO4·6H2O/FeSO4·7H2O, and N-donor ligands, namely 1H-imidazole or 4,4′-bipyridine, under hydrothermal conditions. Single-crystal X-ray diffraction analysis indicated that [Ni(INAIP)(Him)(H2O)]·H2O has a two-dimensional (2D) layer network structure with (6, 3) topology, while 2 shows a 3D fourfold interpenetrating framework with (103-b) topology. The thermal stability and magnetic and adsorption behavior in solid state of the complexes were investigated in detail. Moreover, the photocatalytic degradation of methylene blue (MB) over complex 1 was studied.

Published
2020
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