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This work describes a glassy carbon electrode (GCE) modified by 4-((E)-(2-methyl-4-nitrophenylimino) methyl) benzene-1,2-diol (abbreviated as MBD) and multiwall carbon nanotubes (MWNT) as an electrochemical sensor for monitoring of levodopa (LD) concentration. Different electrochemical parameters of MBD were obtained at MWCNT-GCE by cyclic voltammetry. Also the electrocatalytic behavior of LD was investigated at the MBD-MWNT-GCE by cyclic voltammetry, chronoamperometry and differential pulse voltammetry. Using the electrocatalysis of LD V in phosphate buffer solution pH 7.0 on this modified electrode it is possible to obtain a linear calibration curve from 5.0 10 – 7 to 9.0 10 – 4 M and a detection limit of 0.37 μM for LD by differential pulse voltammetry. The electrode was successfully applied for determination of LD in real sample. When you are citing the document, use the following link http://essuir.sumdu.edu.ua/handle/123456789/34938