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This paper presents the results of optimizing the physicochemical properties of microsilica-based composite briquettes for metallurgical-grade silicon production. Microsilica, a waste product of silicon production, contains a sufficiently high amount of silicon dioxide (96–97%). This fact makes microsilica a promising composite material for metallurgical processing. However, its granulometric composition limits its direct use. The method of briquetting on an industrial briquetting press was used. The influence of the granulometric composition of the composite mixture on the heat tolerance and reactivity of the finished briquettes was studied. The methods of obtaining and testing the briquettes, their composition, and the briquetting and drying process were described. The obtained briquettes were tested for the smelting of metallurgical silicon. The silicon recovery rate in the metal with the standard charge was 71%, while the recovery rate with the briquetted monocharge was 85%. The results of silicon smelting from the briquettes demonstrated the high quality of the obtained metal, corresponding to the standards of metallurgical-grade silicon. The implementation of these technologies improves the quality of the finished product and addresses environmental issues related to the disposal of microsilica, reducing its accumulation and minimizing its impact on the environment. [ABSTRACT FROM AUTHOR]