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The design, simulation, fabrication and characterization of a new integrated optical accelerometer is presented in this paper. The reduction of fabrication, packaging and thermomechanical stresses are considered by keeping the weak mechanical parts free of stresses. The mechanical sensor consists on a quad beam structure with one single mass. In addition, there are two waveguides on the frame of the chip self-aligned to one on the mass of the accelerometer. Four lateral beams increase the mechanical sensitivity and allow the fiat displacement of the optical waveguides on the mass. The working principle is based on the variation of the output light intensity versus the acceleration due to the misalignment of the waveguides. The devices have been optimized by the finite-element method to obtain a mechanical sensitivity of 1 µm/g. The fabrication technology is based on BESOI wafers combining bulk an surface micromachining. Moreover, machined glass wafers with cavities are bonded to the silicon wafer for packaging and damping control. Special packaging considerations as dicing, polishing and alignment are also presented. Optical measurements at 633 nm shown an optical sensitivity of 2.3 dB/g for negative and 1.7 dB/g for positive acceleration. This difference in the sensitivity has been demonstrated as a consequence of the passivation layer located over the core of the waveguides. [ABSTRACT FROM AUTHOR]

Examines the use of an integrated waveguide absorbance optodes for ion-selective sensing. Development of ion-selective membranes in combination with a selective ionophore; Advantages of the flow injection system; Toxic effects of heavy metals.

Details the optical and analytical characteristics of ketocyanine dyes, neutral hydrogen-selective chromoionophores, in polyvinyl chloride. Spectral properties; Acid-base properties; Chemical stability; solubility in the membrane phase; Response characteristics tested in a conventional absorbance/transmittance flow cell.

In this paper, a computer controlled microreactor to synthesize water soluble CdS and CdS/ZnS nanocrystals with in situ monitoring of the reaction progress is developed. It is based on ceramic tapes and the Low-Temperature Co-fired Ceramics technology (LTCC). As well the microsystem set-up, the microreactor fluidic design has also been thoroughly optimized. The final device is based on a hydrodynamic focusing of the reagents followed by a three-dimensional micromixer. This generates monodispersed and stable CdS and core-shell CdS/ZnS nanocrystals of 4.5 and 4.2 nm, respectively, with reproducible optical properties in terms of fluorescence emission wavelengths, bandwidth, and quantum yields, which is a key requirement for their future analytical applications. The synthetic process is also controlled in real time with the integration of an optical detection system for absorbance and fluorescence measurements based on commercial miniaturized optical components. This makes possible the efficient managing of the hydrodynamic variables to obtain the desired colloidal suspension. As a result, a simple, economic, robust and portable microsystem for the well controlled synthesis of CdS and CdS/ZnS nanocrystals is presented. Moreover, the reaction takes place in aqueous medium, thus allowing the direct modular integration of this microreactor in specific analytical microsystems, which require the use of such quantum dots as labels., (This journal is © The Royal Society of Chemistry 2012)

We report on results from the characterization of Stimulated Brillouin Scattering (SBS) spectra for standard single-mode fiber produced by the interaction between two counter-propagating tunable laser sources (TLS) using one as the probe signal to measure and the other as the pump, sweeping a wide span around the signal. Assuming TLS linewidth negligible against SBS gain bandwidth, we measure SBS spectrum for a wide range of pump and probe signal power levels and study the evolution of relevant SBS parameters such as linewidth and gain profile. High signal to noise ratio measurements allows analyzing the evolution of the SBS gain profile from Lorentzian to Gaussian as predicted by current theory of SBS and the use of SBS response for filtering applications.

The optical and analytical characteristics of a series of neutral H+-selective chromoionophores in PVC membranes are described. Such indicators have been synthesized so that they can operate in bulk optode membranes as the chemically active region of integrated waveguide absorbance optodes (IWAOs), lambdamax near 780 nm. Their spectral characteristics, acid-base properties, chemical stability, and solubility in the membrane phase are given and discussed. The response characteristics are first tested in a conventional absorbance/transmittance flow cell. They offer a wide range of pKa's in PVC membranes, good sensitivity as a result of their high molar absortivities, excellent solubility in the plasticizer, and quick response times. They present good chemical stability in common laboratory conditions when stored in the dark, and the absence of leaching guarantees a long lifetime. Membranes have been finally applied as the sensing region of an integrated waveguide optode, demonstrating the extraordinary sensitivity improvement while preserving the remaining analytical features. Calibration curve slopes are multiplied by 3-28, and response times lower than 2 min are obtained.