1. Microstructure, hardness, and tribological properties of Ni-Co/ SiO2 nanocomposite coating produced through pulsed current electrodeposition.
- Author
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Akbarpour, M.R., Hosseini, S.F., and Kim, H.S.
- Subjects
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COMPOSITE coating , *FACE centered cubic structure , *SLIDING wear , *TRIBOLOGY , *MICROHARDNESS testing - Abstract
This study investigates the development of Ni-Co/SiO 2 nanocomposite coatings on mild steel surface using pulsed-current electrodeposition method. The effects of incorporating SiO 2 nanoparticle and varying its concentration on the coatings' microstructure, microhardness, wear resistance, and frictional properties were assessed using field-emission electron microscopy, X-ray diffraction, Vickers microhardness testing, and dry sliding wear tests. The results indicated that the coatings exhibited two-phases of Ni-Co solid solution (α) with a face-centered cubic (FCC) crystal structure and hexagonal Co, a refined crystallite size of approximately 31 nm for Ni-Co and about 25 nm for Ni-Co/SiO 2 , along with a colony-like morphology that did not show any preferred growth direction. The amount of Ni-Co solid solution increased with the addition of SiO 2 nanoparticles. The composite coatings demonstrated enhanced microhardness of 581 HV, which is 52 % greater than that of the Ni-Co coating, as well as improved wear resistance and a reduced friction coefficient compared to the unreinforced alloy coating. However, higher SiO 2 content adversely impacted the tribological properties due to nanoparticle agglomeration. Analysis of the worn surfaces revealed a transition from abrasive wear to oxidative wear with increasing applied force for the coatings. [ABSTRACT FROM AUTHOR]
- Published
- 2024
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