86 results on '"S. I. Popkov"'
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2. An applied multi-agent system within the framework of a player-centered probabilistic computer game.
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Lev S. Kuravsky, S. I. Popkov, and Sergey L. Artemenkov
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- 2018
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3. Anisotropic Magnetization of an NbN Film
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D. M. Gokhfeld, N. E. Savitskaya, S. I. Popkov, N. D. Kuzmichev, M. A. Vasyutin, and D. A. Balaev
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General Physics and Astronomy - Published
- 2022
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4. Research of Interactive and Traditional Tasks Aimed at Studying Information Technologies among Students
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S I Popkov
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research ,Multimedia ,business.industry ,Computer science ,05 social sciences ,050301 education ,Information technology ,050109 social psychology ,General Medicine ,computer.software_genre ,Education ,programming education ,interactivity ,0501 psychology and cognitive sciences ,business ,0503 education ,computer ,jasp - Abstract
The results of a study conducted within the framework of an interactive approach to the task formation, which is an actual branch of computer methods in education, are presented. The author notes that the branch is currently not used for teaching information technologies practice in higher educational institutions due to the labor cost of forming, implementing and taking into account the impact of interactive tasks on the success of the educational process participants. The purpose of the study is to substantiate the introduction of relevant information technologies into the educational process, as well as approaches to the verification and formation of knowledge. It tested the main hypothesis: tasks aimed at interactive activity better help students in mastering the material, based on their own perception, than static tasks based on traditional approaches in the educational process with information technologies application. An intraindividual scheme of the experiment is used on the basis of traditional and interactive tasks, different types of tasks are presented to the same group of students. The sample for the participants of the experiment is recruited among the most capable students of the Information Technologies Faculty, bachelors, 2-4 year of experience according to the criterion of academic performance in the framework of specialized disciplines (28 people participated). The variables are empirically selected characteristics that reflect the useful qualities of the task in the context of the educational process. Methods of descriptive statistics are used to test hypotheses. It is noted that the results of the study make it possible to determine and formulate conditions that allow maximum use of the advantages of each of the studied types of tasks. The research confirms the demand for the development of teaching tools for students using interactive tasks, indicating the boundary conditions under which, according to the author, an interactive approach to the construction and implementation of tasks can demonstrate its effectiveness.
- Published
- 2021
5. Application of the Digital Adaptive Platform for Learning Programming with the Teamwork Skills Forming Function
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S I Popkov
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Teamwork ,Computer science ,Human–computer interaction ,media_common.quotation_subject ,General Medicine ,Function (engineering) ,Learning programming ,media_common - Abstract
Research is carried out on approaches for the digital adaptive platform for learning programming with the teamwork skills forming function application. The work environment interface and key components that make the platform adaptable are demonstrated. The platform services responsible for information security functions are detailed. An example of the presented task is given.
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- 2021
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6. General Regularities and Differences in the Behavior of the Dynamic Magnetization Switching of Ferrimagnetic (CoFe2O4) and Antiferromagnetic (NiO) Nanoparticles
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S. V. Semenov, A. A. Dubrovskii, S. I. Popkov, S. S. Yakushkin, D. A. Balaev, A. A. Krasikov, Oleg N. Martyanov, and V. L. Kirillov
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010302 applied physics ,Materials science ,Magnetic moment ,Condensed matter physics ,Coercivity ,Condensed Matter Physics ,Magnetic hysteresis ,01 natural sciences ,Electronic, Optical and Magnetic Materials ,Magnetization ,Hysteresis ,Ferromagnetism ,Ferrimagnetism ,0103 physical sciences ,Antiferromagnetism ,Condensed Matter::Strongly Correlated Electrons ,010306 general physics - Abstract
In antiferromagnetic (AFM) nanoparticles, an additional ferromagnetic phase forms and leads to the appearance in AFM nanoparticles of a noncompensated magnetic moment and the magnetic properties typical of common FM nanoparticles. In this work, to reveal the regularities and differences of the dynamic magnetization switching in FM and AFM nanoparticles, the typical representatives of such materials are studied: CoFe2O4 and NiO nanoparticles with average sizes 6 and 8 nm, respectively. The high fields of the irreversible behavior of the magnetizations of these samples determine the necessity of using strong pulsed fields (amplitude to 130 kOe) to eliminate the effect of the partial hysteresis loop when studying the dynamic magnetic hysteresis. For both types of the samples, coercive force HC at the dynamic magnetization switching is markedly higher than HC at quasi-static conditions. HC increases as the pulse duration τP decreases and the maximum applied field H0 increases. The dependence of HC on field variation rate dH/dt = H0/2τP is a unambiguous function for CoFe2O4 nanoparticles, and it is precisely such a behavior is expected from a system of single-domain FM nanoparticles. At the same time, for AFM NiO nanoparticles, the coercive force is no longer an unambiguous function of dH/dt, and the value of applied field H0 influences more substantially. Such a difference in the behaviors of FM and AFM nanoparticles is caused by the interaction of the FM subsystem and the AFM “core” inside AFM nanoparticles. This circumstance should be taken into account when developing the theory of dynamic hysteresis of the AFM nanoparticles and also to take into account their practical application.
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- 2020
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7. Features of the Pulsed Magnetization Switching in a High-Coercivity Material Based on ε-Fe2O3 Nanoparticles
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S. S. Yakushkin, A. A. Dubrovskii, S. V. Semenov, S. I. Popkov, Oleg N. Martyanov, D. A. Balaev, A. A. Krasikov, and V. L. Kirillov
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Condensed Matter::Materials Science ,Magnetization ,Materials science ,Magnetic moment ,Magnetic structure ,Condensed matter physics ,Ferrimagnetism ,Relaxation (NMR) ,Coercivity ,Condensed Matter Physics ,Magnetic hysteresis ,Electronic, Optical and Magnetic Materials ,Superparamagnetism - Abstract
The magnetic structure of the e-Fe2O3 iron oxide polymorphic modification is collinear ferrimagnetic in the range from room temperature to ~150 K. As the temperature decreases, e-Fe2O3 undergoes a magnetic transition accompanied by a significant decrease in the coercivity Hc and, in the low-temperature range, the compound has a complex incommensurate magnetic structure. We experimentally investigated the dynamic magnetization switching of the e-Fe2O3 nanoparticles with an average size of 8 nm in the temperature range of 80–300 K, which covers different types of the magnetic structure of this iron oxide. A bulk material consisting of xerogel SiO2 with the e-Fe2O3 nanoparticles embedded in its pores was examined. The magnetic hysteresis loops under dynamic magnetization switching were measured using pulsed magnetic fields Hmax of up to 130 kOe by discharging a capacitor bank through a solenoid. The coercivity Нс upon the dynamic magnetization switching noticeably exceeds the Нс value under the quasi-static conditions. This is caused by the superparamagnetic relaxation of magnetic moments of particles upon the pulsed magnetization switching. In the range from room temperature to ~ 150 K, the external field variation rate dH/dt is the main parameter that determines the behavior of the coercivity under the dynamic magnetization switching. It is the behavior that is expected for a system of single-domain ferro- and ferrimagnetic particles. Under external conditions (at a temperature of 80 K) when the e-Fe2O3 magnetic structure is incommensurate, the coercivity during the pulsed magnetization switching depends already on the parameter dH/dt and is determined, to a great extent, by the maximum applied field Hmax. Such a behavior atypical of systems of ferrimagnetic particles is caused already by the dynamic spin processes inside the e-Fe2O3 particles during fast magnetization switching.
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- 2020
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8. Synthesis and Magnetic Properties of the Core–Shell Fe3O4/CoFe2O4 Nanoparticles
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Oleg N. Martyanov, D. A. Balaev, V. L. Kirillov, A. A. Dubrovskii, A. A. Krasikov, S. V. Semenov, S. I. Popkov, and S. S. Yakushkin
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Chemical substance ,Materials science ,Solid-state physics ,Shell (structure) ,Nanoparticle ,Coercivity ,Condensed Matter Physics ,Electronic, Optical and Magnetic Materials ,law.invention ,Core (optical fiber) ,Magazine ,Chemical engineering ,law ,Science, technology and society - Abstract
The Fe3O4/CoFe2O4 nanoparticles with a core–shell structure with an average size of 5 nm have been obtained by codeposition from the iron and cobalt chloride solutions. An analysis of the magnetic properties of the obtained system and their comparison with the data for single-phase Fe3O4 (4 nm) and CoFe2O4 (6 nm) nanoparticles has led to the conclusion about a noticeable interaction between the soft magnetic (Fe3O4) and hard magnetic (CoFe2O4) phases forming the core and shell of hybrid particles.
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- 2020
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9. Physical Properties of a Frustrated Quasi-One-Dimensional NaCuFe2(VO4)3 Magnet and Effect of Chemical Pressure Induced by the Substitution of Sodium for Lithium
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G. A. Petrakovskii, A. M. Vorotynov, S. I. Popkov, T. V. Drokina, M. S. Molokeev, Oleg A. Bayukov, and D. A. Velikanov
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010302 applied physics ,Phase transition ,Materials science ,Condensed matter physics ,Magnetism ,Resonance ,chemistry.chemical_element ,Condensed Matter Physics ,01 natural sciences ,Electronic, Optical and Magnetic Materials ,law.invention ,Paramagnetism ,chemistry ,law ,0103 physical sciences ,Antiferromagnetism ,Condensed Matter::Strongly Correlated Electrons ,Lithium ,010306 general physics ,Electron paramagnetic resonance ,Néel temperature - Abstract
The structural, thermal, static magnetic, and resonance properties of the low-dimensional NaCuFe2(VO4)3 compound obtained by the solid-phase synthesis have been investigated. In the temperature range of 110–300 K, the electron spin resonance in the X band with a g factor of 2.008 has been detected. The magnetic properties of a sample with a high frustration level in the paramagnetic, antiferromagnetic, and disordered states have been examined. A shift of the Neel temperature to the high-temperature region in an external magnetic field has been observed. The origin of the disordered magnetism in NaCuFe2(VO4)3 are discussed. The features of substitution of sodium for lithium on the physical properties of the ACuFe2(VO4)3 (A = Na, Li) system have been established. It is shown that the chemical pressure changes the crystal lattice parameters, spacings between magnetic ions, and crystallite size, which is reflected in the physical properties of the material.
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- 2020
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10. Organization of Client-Server Interaction on a Single Computer
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S I Popkov
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Client–server model ,Computer science ,business.industry ,General Medicine ,business ,Computer network - Abstract
A research of existing approaches to the organization of client-server interaction is conducted. Special attention is paid to the practical application of client-server interaction on a single computer. An experiment was conducted with the implementation of minimal server code and the application of virtualization. The result of the experiment is presented, the technical features and the results obtained are described.
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- 2020
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11. Formation of the magnetic subsystems in antiferromagnetic NiO nanoparticles using the data of magnetic measurements in fields up to 250 kOe
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S. I. Popkov, A. A. Krasikov, D. A. Balaev, V. L. Kirillov, Oleg N. Martyanov, and D. A. Velikanov
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010302 applied physics ,Materials science ,Spins ,Magnetic moment ,Condensed matter physics ,02 engineering and technology ,021001 nanoscience & nanotechnology ,Condensed Matter Physics ,01 natural sciences ,Electronic, Optical and Magnetic Materials ,Magnetic field ,Magnetization ,Paramagnetism ,0103 physical sciences ,Antiferromagnetism ,Particle ,Condensed Matter::Strongly Correlated Electrons ,Particle size ,0210 nano-technology - Abstract
It is well-known that the fraction of surface atoms and the number of defects in an antiferromagnetic particle increase with a decrease in the particle size to tens of nanometers, which qualitatively changes the properties of the particle. Specifically, in antiferromagnetic nanoparticles, spins in the ferromagnetically ordered planes can partially decompensate; as a result, an antiferromagnetic particle acquires a magnetic moment. As a rule, uncompensated chemical bonds of the surface atoms significantly weaken the exchange coupling with the antiferromagnetic particle core, which can lead to the formation of an additional magnetic subsystem paramagnetic at high temperatures and spin-glass-like in the low-temperature region. The existence of several magnetic subsystems makes it difficult to interpret the magnetic properties of antiferromagnetic nanoparticles. It is shown by the example of NiO nanoparticles with an average size of 8 nm that the correct determination of the contributions of the magnetic subsystems forming in antiferromagnetic nanoparticles requires magnetic measurements in much stronger external magnetic fields than those commonly used in standard experiments (up to 60–90 kOe). An analysis of the magnetization curves obtained in pulsed magnetic fields up to 250 kOe allows one to establish the contributions of the uncompensated particle magnetic moment μun, paramagnetic subsystem, and antiferromagnetic particle core. The μun value obtained for the investigated NiO particles is consistent with the Neel model, in which μun ∼ N1/2 (N is the number of magnetically active atoms in a particle), and thereby points out the existence of defects on the surface and in the bulk of a particle. It is demonstrated that the anomalous behavior of the high-field susceptibility dM/dH of antiferromagnetic NiO nanoparticles, which was observed by many authors, is caused by the existence of a paramagnetic subsystem, rather than by the superantiferromagnetism effect.
- Published
- 2019
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12. Magnetic and thermodynamic properties and spin-flop-driven magnetodielectric response of the antiferromagnetic Pb2Fe2Ge2O9 single crystals
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S.E. Nikitin, A. D. Balaev, A.L. Freydman, M.I. Kolkov, S. I. Popkov, A. I. Pankrats, D. A. Balaev, and A. A. Krasikov
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010302 applied physics ,Materials science ,Condensed matter physics ,Exchange interaction ,02 engineering and technology ,021001 nanoscience & nanotechnology ,Condensed Matter Physics ,01 natural sciences ,Electronic, Optical and Magnetic Materials ,Magnetic field ,Magnetization ,Ferromagnetism ,0103 physical sciences ,Antiferromagnetism ,Condensed Matter::Strongly Correlated Electrons ,Orthorhombic crystal system ,0210 nano-technology ,Anisotropy ,Néel temperature - Abstract
Orthorhombic Pb2Fe2Ge2O9 antiferromagnetic single crystals have been synthesized by a modified pseudo-flux technique and their magnetic, thermodynamic, and magnetodielectric properties have been investigated. It has been found that, below the Neel temperature (45.2 K), iron moments are arranged in a canted antiferromagnetic structure with a weak ferromagnetic moment parallel to the a axis. According to the specific heat measurement data, the TN value remains invariable in applied magnetic fields of up to 50 kOe within the experimental accuracy. The magnetic entropy in the investigated crystals attains 2Rln(2S + 1) right above TN, which is indicative of a purely magnetic nature of the transition. It has been shown that the weak ferromagnetic moment is induced by the interplay between the single-ion anisotropy and antisymmetric Dzyaloshinskii–Moriya exchange interaction, with the latter contribution being dominant. It has been established from the angular dependences of the magnetization in three orthorhombic planes that the symmetries of the magnetic and crystal structure are identical. The magnetodielectric properties of the Pb2Fe2Ge2O9 single crystals have been studied at different mutual orientations of the electric and magnetic fields. The most prominent anomalies have been observed in the vicinity of the spin-flop transition in a magnetic field applied along the c axis.
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- 2019
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13. Peculiarities of a magnetic transition in a quasi-one-dimensional ferromagnet PbMnBO4
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A. A. Krasikov, M.I. Kolkov, S. Martynov, A. D. Balaev, A. I. Pankrats, Mikhail V. Gorev, and S. I. Popkov
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Magnetization ,Materials science ,Mean field theory ,Ferromagnetism ,Condensed matter physics ,Magnetic structure ,Curie temperature ,Condensed Matter::Strongly Correlated Electrons ,Atmospheric temperature range ,Condensed Matter Physics ,Heat capacity ,Electronic, Optical and Magnetic Materials ,Magnetic field - Abstract
Near the Curie temperature TC = 30.3 K, the temperature dependences of the magnetization and heat capacity of a single-crystal ferromagnet PbMnBO4 in the magnetic fields of 1, 3, 10 and 30 kOe are studied. In the strong magnetic fields, both the magnetic contribution to the specific heat and the nonlinearity of the field dependences of the magnetization are maintained up to the temperatures exceeding TC more than twice. It is assumed that in PbMnBO4 the difference between TC, the paramagnetic Curie temperature θ = 49 K and the broad temperature region above TC where the magnetic contribution to the specific heat is significant is due to the quasi-one-dimensional character of the magnetic structure of this ferromagnet. Using both the estimation of TC from the Ginzburg-Landau field theory and the θ value, the total exchange interaction parameters 2J ≈ 40.4 K (intrachain) and z′J′ ≈ 8.8 K (interchain) are determined, with z′ = 4 being the number of neighboring chains. The estimation shows that the Ginzburg-Landau field theory describing the quasi-one-dimensional behavior of PbMnBO4 is well applicable in the temperature range from to T = S2J ≈ 80 K. Above this temperature, the mean field approximation with the exchange parameter λθ based on the paramagnetic Curie temperature θ describes well the experimental temperature dependences of the magnetization in the strong magnetic field and the specific heat is determined by the lattice contribution.
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- 2019
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14. The Method of External Optimization for Methods of Markov Processes Identification
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Education, Moscow, Russian Federation and S. I. Popkov
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symbols.namesake ,Identification (information) ,Computer science ,symbols ,Markov process ,Data mining ,computer.software_genre ,computer - Published
- 2018
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15. Pulsed Field-Induced Magnetization Switching in Antiferromagnetic Ferrihydrite Nanoparticles
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N. V. Dubynin, R. N. Yaroslavtsev, V. P. Ladygina, S. I. Popkov, D. A. Velikanov, S. V. Stolyar, D. A. Balaev, and A. A. Krasikov
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010302 applied physics ,Materials science ,Condensed matter physics ,Magnetism ,Relaxation (NMR) ,Coercivity ,Condensed Matter Physics ,Magnetic hysteresis ,01 natural sciences ,Electronic, Optical and Magnetic Materials ,Condensed Matter::Materials Science ,Magnetization ,Hysteresis ,Ferrimagnetism ,0103 physical sciences ,Magnetic nanoparticles ,Condensed Matter::Strongly Correlated Electrons ,010306 general physics - Abstract
The dynamic magnetization switching of ferrihydrite nanoparticles has been investigated by a pulsed magnetometer technique in maximum fields Hmax of up to 130 kOe with pulse lengths of 4, 8, and 16 ms. Ferrihydrite exhibits antiferromagnetic ordering and defects cause the uncompensated magnetic moment in nanoparticles; therefore, the behavior typical of magnetic nanoparticles is observed. The dynamic hysteresis loops measured under the above-mentioned conditions show that the use of pulsed fields significantly broadens the temperature region of existence of the magnetic hysteresis and the coercivity can be governed by varying the maximum field and pulse length. This behavior is resulted from the relaxation effects typical of conventional ferro- and ferrimagnetic nanoparticles and the features typical of antiferromagnetic nanoparticles.
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- 2018
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16. Dynamic Magnetization Switching in NiO Nanoparticles: Pulsed Field Magnetometry Study
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A. A. Dubrovskiy, S. I. Popkov, Oleg N. Martyanov, A. D. Balaev, A. A. Krasikov, D. A. Balaev, and V. L. Kirillov
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010302 applied physics ,Materials science ,Spins ,Magnetic moment ,Condensed matter physics ,Magnetometer ,Relaxation (NMR) ,02 engineering and technology ,Coercivity ,021001 nanoscience & nanotechnology ,Condensed Matter Physics ,Magnetic hysteresis ,01 natural sciences ,Electronic, Optical and Magnetic Materials ,law.invention ,Condensed Matter::Materials Science ,Magnetization ,law ,0103 physical sciences ,Antiferromagnetism ,Condensed Matter::Strongly Correlated Electrons ,0210 nano-technology - Abstract
The dynamic magnetization switching of antiferromagnetic nickel oxide nanoparticles with a characteristic size of 8 nm has been experimentally investigated by pulsed field magnetometry. It is shown that, due to the presence of defects in NiO nanoparticles, as in other antiferromagnetic particles, the uncompensated magnetic moment is induced by the incomplete compensation of spins at the antiferromagnetic ordering. The dynamic magnetic hysteresis loops have been studied in pulsed fields with the maximum field ( $H_{{\max }}$ ) of up to 130 kOe and pulse lengths (τP) of 4, 8, and 16 ms. According to the results obtained, the coercivity (HC) depends on both the τP and $H_{{\max }}$ values. The observed increase in the $H_{\mathrm {C}}$ value with decreasing pulse length (i.e., with increasing switching field frequency) is unambiguously related with the relaxation processes typical of single-domain ferromagnetic nanoparticles. However, the observed effect of the maximum applied field ( $H_{{\max }})$ on the $H_{\mathrm {C}}$ value is assumed to be a feature of antiferromagnetic nanoparticles.
- Published
- 2018
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17. Bacterial Ferrihydrite Nanoparticles: Preparation, Magnetic Properties, and Application in Medicine
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S. V. Stolyar, V. P. Ladygina, Dobretsov Kg, D. A. Balaev, Oksana A. Kolenchukova, Rauf S. Iskhakov, Mikhail N. Volochaev, Yu. V. Knyazev, R. N. Yaroslavtsev, S. I. Popkov, E. V. Morozov, E. V. Inzhevatkin, Oleg A. Bayukov, A. A. Dubrovskiy, I. A. Chizhova, A. A. Krasikov, and O. V. Falaleev
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010302 applied physics ,Materials science ,Magnetic moment ,Nanoparticle ,Nanotechnology ,02 engineering and technology ,021001 nanoscience & nanotechnology ,Condensed Matter Physics ,01 natural sciences ,Electronic equipment ,Electronic, Optical and Magnetic Materials ,Ferrihydrite ,Targeted drug delivery ,0103 physical sciences ,Drug delivery ,Particle ,0210 nano-technology - Abstract
Nanoparticles of antiferromagnetically ordered materials acquire the uncompensated magnetic moment caused by defects and surface effects. A bright example of such a nano-antiferromagnet is nanoferrihydrite consisting of particles 2–5 nm in size, the magnetic moment of which amounts to hundreds of Bohr magnetons per particle. We present a brief review of the studies on magnetic properties of ferrihydrite produced by bacteria. Special attention is focused on the aspects of possible biomedical applications of this material, i.e., the particle elimination, toxicity, and possible use for targeted drug delivery.
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- 2018
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18. Superconductivity on Interfaces of Nonsuperconducting Granules La2CuO4 and La1.56Sr0.44CuO4
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Mihail Petrov, A. A. Bykov, K. Yu Terent’ev, Denis Gokhfeld, S. I. Popkov, and N. E. Savitskaya
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010302 applied physics ,Superconductivity ,Materials science ,Condensed matter physics ,Annealing (metallurgy) ,Condensed Matter Physics ,01 natural sciences ,Electronic, Optical and Magnetic Materials ,Magnetic field ,Condensed Matter::Materials Science ,Magnetization ,Electrical resistivity and conductivity ,Condensed Matter::Superconductivity ,visual_art ,0103 physical sciences ,Volume fraction ,visual_art.visual_art_medium ,Cuprate ,Ceramic ,010306 general physics - Abstract
Composite materials fabricated by annealing of nonsuperconducting ceramics La2CuO4 and La1.56Sr0.44CuO4 at 910 °C during various time are investigated. Areas of superconducting La1.85Sr0.15CuO4 phase arises at boundaries of contacting nonsuperconducting granules. The volume fraction of the superconducting phase increases with increasing annealing time. A model describing the magnetic and transport properties of the samples at low magnetic fields is constructed. The magnetotransport characteristics of obtained samples at low magnetic fields (∼ 100 Oe) are defined by weak links network formed by superconducting areas. At high fields, behavior of the system is defined by a magnetization of the disconnected superconducting islands. The average size of the superconducting areas has been estimated from an extended critical state model.
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- 2018
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19. Magnetic properties of NiO nano particles: Contributions of the antiferromagnetic and ferromagnetic subsystems in different magnetic field ranges up to 250 kOe
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V. L. Kirillov, S. I. Popkov, A. A. Krasikov, K. A. Shaikhutdinov, D. A. Balaev, A. D. Balaev, Oleg N. Martyanov, and A. A. Dubrovskiy
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010302 applied physics ,Materials science ,Condensed matter physics ,Magnetic moment ,Solid-state physics ,02 engineering and technology ,021001 nanoscience & nanotechnology ,Condensed Matter Physics ,01 natural sciences ,Electronic, Optical and Magnetic Materials ,Magnetic field ,Magnetization ,Ferromagnetism ,0103 physical sciences ,Antiferromagnetism ,Condensed Matter::Strongly Correlated Electrons ,0210 nano-technology ,Spin (physics) ,Superparamagnetism - Abstract
The magnetic properties of antiferromagnetic NiO nanoparticles prepared by thermal decomposition of nickel hydroxocarbonate are investigated. According to the data of magnetization measurements in fields of up to 250 kOe, the magnetic moment linearly grows in strong fields, which is caused by the contribution of the antiferromagnetically ordered nanoparticle core, and the antiferromagnetic susceptibility corresponds to that of bulk polycrystalline NiO. This allowed the antiferromagnetic and ferromagnetic contributions to the total magnetic response of a sample to be quantitatively determined. The latter occurs due to the incomplete spin compensation in an antiferromagnetic nanoparticle caused by defects on its surface. It is demonstrated that to correctly determine the superparamagnetic blocking temperature, it is necessary to take into account the antiferromagnetic susceptibility of the particle core.
- Published
- 2017
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20. Magnetic properties of heat treated bacterial ferrihydrite nanoparticles
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D. A. Balaev, Oleg A. Bayukov, S. I. Popkov, V. P. Ladygina, A. A. Krasikov, R. N. Yaroslavtsev, Rauf S. Iskhakov, S. V. Stolyar, and A. A. Dubrovskiy
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010302 applied physics ,Materials science ,Magnetic moment ,Nanoparticle ,02 engineering and technology ,equipment and supplies ,021001 nanoscience & nanotechnology ,Condensed Matter Physics ,Magnetic hysteresis ,01 natural sciences ,Electronic, Optical and Magnetic Materials ,Ferrihydrite ,Magnetic anisotropy ,Magnetization ,Nuclear magnetic resonance ,Chemical physics ,0103 physical sciences ,Particle ,0210 nano-technology ,human activities ,Superparamagnetism - Abstract
The magnetic properties of ferrihydrite nanoparticles, which are products of vital functions of Klebsiella oxitoca bacteria, have been studied. The initial powder containing the nanoparticles in an organic shell was subjected to low-temperature (T=160 °C) heat treatment for up to 240 h. The bacterial ferrihydrite particles exhibit a superparamagnetic behavior. Their characteristic blocking temperature increases from 26 to 80 K with the heat treatment. Analysis of the magnetization curves with regard to the magnetic moment distribution function and antiferromagnetic contribution shows that the low-temperature heat treatment enhances the average magnetic moment of a particle; i.e., the nanoparticles coarsen, probably due to their partial agglomeration during heat treatment. It was established that the blocking temperature nonlinearly depends on the particle volume. Therefore, a model was proposed that takes into account both the bulk and surface magnetic anisotropy. Using this model, the bulk and surface magnetic anisotropy constants KV≈1.7×105 erg/cm3 and KS≈0.055 erg/cm2 have been determined. The effect of the surface magnetic anisotropy of ferrihydrite nanoparticles on the observed magnetic hysteresis loops is discussed.
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- 2016
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21. A Capacitive Dilatometer for Measuring the Magnetostriction, Piezoelectric Effect, and Linear Thermal-Expansion Coefficient
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A. L. Freidman, S. V. Semenov, S. I. Popkov, and P. P. Turchin
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010302 applied physics ,Materials science ,Physics and Astronomy (miscellaneous) ,Capacitive sensing ,Magnetostriction ,Atmospheric temperature range ,01 natural sciences ,Capacitance ,Piezoelectricity ,Thermal expansion ,Magnetic field ,0103 physical sciences ,Dilatometer ,Composite material ,010306 general physics - Abstract
We describe a capacitive dilatometer for measuring the magnetostriction, piezoelectric effect, and linear thermal-expansion coefficient in the temperature range from 1.85 to 350 K in external magnetic fields of up to 90 kOe under a voltage of 1 kV, which operates on the basis of a Quantum Design PPMS commercial facility for studying the properties of solids.
- Published
- 2018
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22. Features of the quasi-static and dynamic magnetization switching in NiO nanoparticles: Manifestation of the interaction between magnetic subsystems in antiferromagnetic nanoparticles
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A. A. Krasikov, S. I. Popkov, S. V. Semenov, Oleg N. Martyanov, D. A. Balaev, V. L. Kirillov, D. A. Velikanov, and A. A. Dubrovskiy
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010302 applied physics ,Materials science ,Magnetic moment ,Field (physics) ,Condensed matter physics ,02 engineering and technology ,Coercivity ,021001 nanoscience & nanotechnology ,Condensed Matter Physics ,Magnetic hysteresis ,01 natural sciences ,Electronic, Optical and Magnetic Materials ,Magnetic field ,Magnetization ,Ferrimagnetism ,0103 physical sciences ,Antiferromagnetism ,0210 nano-technology - Abstract
We report on the investigations of a system of 8-nm NiO particles representing antiferromagnetic (AFM) materials, which are weak magnetic in the form of submicron particles, but can be considered to be magnetoactive in the form of nanoparticles due to the formation of the uncompensated magnetic moment in them. The regularities of the behavior of magnetization switching in AFM nanoparticles are established by studying the magnetic hysteresis loops under standard quasi-static conditions and in a quasi-sinusoidal pulsed field of up to 130 kOe with pulse lengths of 4–16 ms. The magnetic hysteresis loops are characterized by the strong fields of the irreversible magnetization behavior, which is especially pronounced upon pulsed field-induced magnetization switching. Under the pulsed field-induced magnetization switching conditions, which are analogous to the dynamic magnetic hysteresis, the coercivity increases with an increase in the maximum applied field H0 and a decrease in the pulse length. This behavior is explained by considering the flipping of magnetic moments of particles in an external ac magnetic field; however, in contrast to the case of single-domain ferro- and ferrimagnetic particles, the external field variation rate dH/dt is not a universal parameter uniquely determining the coercivity. At the dynamic magnetization switching in AFM nanoparticles, the H0 value plays a much more important role. The results obtained are indicative of the complex dynamics of the interaction between magnetic subsystems formed in AFM nanoparticles.
- Published
- 2020
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23. Specific features of magnetic properties of ferrihydrite nanoparticles of bacterial origin: A shift of the hysteresis loop
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D. A. Balaev, S. V. Semenov, S. I. Popkov, R. N. Yaroslavtsev, V. P. Ladygina, A. A. Dubrovskiy, Rauf S. Iskhakov, A. A. Krasikov, S. V. Stolyar, Институт инженерной физики и радиоэлектроники, Научно-исследовательская часть, Базовая кафедра физики твердого тела и нанотехнологий, and Кафедра общей физики
- Subjects
010302 applied physics ,Materials science ,Magnetic moment ,Condensed matter physics ,Coercivity ,Condensed Matter Physics ,Magnetic hysteresis ,01 natural sciences ,Electronic, Optical and Magnetic Materials ,Magnetic field ,Condensed Matter::Materials Science ,Ferrihydrite ,Hysteresis ,0103 physical sciences ,29.19.43 ,010306 general physics ,Anisotropy ,Superparamagnetism - Abstract
The results of the experimental investigation into the magnetic hysteresis of systems of superparamagnetic ferrihydrite nanoparticles of bacterial origin have been presented. The hysteresis properties of these objects are determined by the presence of an uncompensated magnetic moment in antiferromagnetic nanoparticles. It has been revealed that, under the conditions of cooling in an external magnetic field, there is a shift of the hysteresis loop with respect to the origin of the coordinates. These features are associated with the exchange coupling of the uncompensated magnetic moment and the antiferromagnetic “core” of the particles, as well as with processes similar to those responsible for the behavior of minor hysteresis loops due to strong local anisotropy fields of the ferrihydrite nanoparticles.
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- 2016
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24. Pulsed solenoid with nanostructured Cu-Nb wire winding
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A. A. Krasikov, A. M. Parshin, A. A. Bykov, and S. I. Popkov
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Operability ,Nuclear magnetic resonance ,Materials science ,Amplitude ,Condensed matter physics ,Thermal ,Physics::Accelerator Physics ,Pulse duration ,Solenoid ,Thin film ,Finite element method ,Surfaces, Coatings and Films ,Magnetic field - Abstract
The construction of a solenoid with nanostructured Cu-Nb wire winding is studied and its electromagnetic, mechanical, and thermal parameters are analytically and numerically calculated. Comparing the results of the calculation and testing, the solenoid operability at an amplitude strength of the generated magnetic field of 40 T and a pulse length of 20 ms is established. The obtained parameters make the solenoid applicable in experimental research aimed at solving topical fundamental problems.
- Published
- 2015
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25. Magnetoresistance of porous polycrystalline HTSC: Effect of the transport current on magnetic flux compression in intergranular medium
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S. I. Popkov, K. A. Shaikhutdinov, M. I. Petrov, D. A. Balaev, and Denis Gokhfeld
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Superconductivity ,Hysteresis ,Materials science ,Magnetic moment ,Condensed matter physics ,Magnetoresistance ,Condensed Matter::Superconductivity ,Grain boundary ,Crystallite ,Intergranular corrosion ,Condensed Matter Physics ,Magnetic flux ,Electronic, Optical and Magnetic Materials - Abstract
The hysteretic dependences of the magnetoresistance of porous (38% of the theoretical density) granular high-temperature superconductor (HTSC) Bi1.8Pb0.3Sr1.9Ca2Cu3Ox have been analyzed in the model of the effective intergranular field. This effective field has been defined by the superposition of the external field and the field induced by magnetic moments of superconducting grains. The magnetic flux compression in an intergranular medium, characterized by the effective field, controls the hysteretic behavior of the magnetoresistance. It has been found that the magnetoresistance hysteresis width for the studied porous HTSC depends on the transport current, in contrast to the superconductor of the same composition with high physical density (more than 90% of the theoretical value). For a porous superconductor, a significant current concentration occurs in the region of the grain boundaries, which is caused by features of its microstructure. A current-induced increase in the effective boundary length results in a decrease in the flux compression, a decrease in the effective field in the intergranular medium, and a magnetoresistance hysteresis narrowing with increasing current.
- Published
- 2014
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26. The Stratified Superconductivity in Ba0.6K0.4BiO3 Single Crystal: Direct Measurement of Energy Gap between Homo-, and Inhomogeneous States
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A. M. Tskhovrebov, L. N. Zherikhina, D. A. Balaev, S. I. Popkov, L. A. Klinkova, D. A. Velikanov, and K. A. Shaikhutdinov
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Physics ,Superconductivity ,Condensed matter physics ,Band gap ,Fermi surface ,Crystallite ,Single crystal ,Quantum tunnelling ,Voltage ,Magnetic field - Abstract
The existence of space inhomogeneous superconductor insulator state (SISIS) found out earlier in polycrystalline samples of high- TC system Ba0.6K0.4BiO3 (TC≈30 K) is confirmed on Ba0.6K0.4BiO3 single crystal. At T* (T*
- Published
- 2014
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27. Magnetic and dielectric properties of the PbFeBO4 single crystal
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Maxim S. Molokeev, A. A. Krasikov, A. Eremin, A. M. Vorotynov, K. A. Sablina, A. I. Pankrats, S. I. Popkov, D. A. Velikanov, and Oleg A. Bayukov
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Materials science ,Condensed matter physics ,Physics::Optics ,Dielectric ,Condensed Matter Physics ,Magnetic susceptibility ,Electronic, Optical and Magnetic Materials ,law.invention ,Crystal ,law ,Condensed Matter::Superconductivity ,Antiferromagnetism ,Condensed Matter::Strongly Correlated Electrons ,Orthorhombic crystal system ,Crystallization ,Néel temperature ,Single crystal - Abstract
PbFeBO 4 single crystals up to 4×2.5×0.5 mm 3 in size were grown by spontaneous crystallization from a solution in a melt and their magnetic and dielectric properties were investigated. The high Neel temperature T N =114 K and the absence of the broad maximum of susceptibility above the Neel temperature suggest that the PbFeBO 4 crystal is a three-dimensional antiferromagnet. The magnetic susceptibility anisotropy in the ordered state indicates that the antiferromagnetic vector is directed along the orthorhombic c axis. The anomalies of dielectric permittivities e ' and e ″ were observed in both polycrystalline and single-crystal samples within the temperature ranges where the short- and long-range magnetic orders are established. This confirms the correlation between the magnetic and electric subsystems in the crystal.
- Published
- 2014
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28. Size effects in the formation of an uncompensated ferromagnetic moment in NiO nanoparticles
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Mikhail N. Volochaev, S. I. Popkov, D. A. Balaev, Oleg N. Martyanov, V. L. Kirillov, A. A. Krasikov, and A. A. Dubrovskiy
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010302 applied physics ,Materials science ,Condensed matter physics ,Spins ,Non-blocking I/O ,General Physics and Astronomy ,Nanoparticle ,02 engineering and technology ,021001 nanoscience & nanotechnology ,01 natural sciences ,Magnetic field ,Condensed Matter::Materials Science ,Magnetization ,Ferromagnetism ,0103 physical sciences ,Antiferromagnetism ,Condensed Matter::Strongly Correlated Electrons ,Particle size ,0210 nano-technology - Abstract
The magnetic properties of samples of NiO nanoparticles with average sizes of 23, 8.5, and 4.5 nm were investigated. Using the magnetization curves measured in strong (up to 250 kOe) pulsed magnetic fields, the contributions of the free spin and ferromagnetic subsystems were extracted. It has been found that the ferromagnetic contribution increases with a decrease in the nanoparticle size and is proportional to the fraction of uncompensated exchange-coupled spins. It is demonstrated that the uncompensated spins form in the antiferromagnetic NiO oxide due to an increase in the fraction of surface atoms in the nanoparticles with decreasing particle size and defects in the bulk of particles.
- Published
- 2019
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29. Increase in the magnetization loop width in the Ba0.6K0.4BiO3 superconductor: Possible manifestation of phase separation
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K. A. Shaikhutdinov, L. N. Zherikhina, A. M. Tsvokhrebov, D. A. Balaev, S. I. Popkov, Denis Gokhfeld, and L. A. Klinkova
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Superconductivity ,Loop (topology) ,Magnetization ,Materials science ,Condensed matter physics ,Solid-state physics ,Remanence ,Condensed Matter::Superconductivity ,Phase (matter) ,General Physics and Astronomy ,Atmospheric temperature range ,Magnetic field - Abstract
The magnetization of Ba0.6K0.4BiO3 samples in fields up to 90 kOe in the temperature range from 2 to 30 K is investigated. It is shown that the observed increase in the width of the magnetization loop can be explained by a decrease in the phase nonuniformity upon an increase in the magnetic field. The asymmetric hysteretic dependence of magnetization with the secondary peak was successfully described by the extended critical state model taking into account the phase separation in the superconductor.
- Published
- 2014
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30. Current-conducting properties of paper consisting of multiwall carbon nanotubes
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T. I. Buryakov, Vladimir L. Kuznetsov, I. N. Mazov, E. N. Tkachev, K. A. Shaikhutdinov, S. I. Popkov, and Sergey I. Moseenkov
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Materials science ,Condensed matter physics ,Solid-state physics ,law ,Electrical resistivity and conductivity ,Phase (matter) ,General Physics and Astronomy ,Carbon nanotube ,Electron ,Atmospheric temperature range ,Conductivity ,Thermal conduction ,law.invention - Abstract
Electrical conductivity σ(T) of the paper consisting of multiwalled carbon nanotubes (MWCNTs) is studied in the temperature range 4.2-295 K, and its magnetoresistivity ρ(B) at various temperatures in magnetic fields up to 9 T is analyzed. The temperature dependence of the paper electrical conductivity σ(T) exhibits two-dimensional quantum corrections to the conductivity below 10 K. The dependences of negative magnetoresistivity ρ(B) measured at various temperatures are used to estimate the wavefunction phase breakdown length Lφ of conduction electrons and to obtain the temperature dependence Lφ = constT−p/2, where p ≈ 1/3. Similar dependences of electrical conductivity σ(T), magnetoresistivity ρ(B), and phase breakdown length Lφ(T) are detected for the initial MWCNTs used to prepare the paper.
- Published
- 2013
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31. Current-voltage characteristics of polycrystalline (La0.5Eu0.5)0.7Pb0.3MnO3 at low temperatures
- Author
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N. V. Volkov, S. I. Popkov, N. V. Sapronova, S. V. Semenov, K. A. Shaikhutdinov, and D. A. Balaev
- Subjects
Materials science ,Solid-state physics ,Condensed matter physics ,Transition temperature ,Condensed Matter Physics ,Electronic, Optical and Magnetic Materials ,Magnetic field ,Condensed Matter::Materials Science ,chemistry.chemical_compound ,Lanthanum manganite ,chemistry ,Condensed Matter::Superconductivity ,Phase (matter) ,Condensed Matter::Strongly Correlated Electrons ,Crystallite ,Layering ,Quantum tunnelling - Abstract
The current-voltage characteristics of the polycrystalline substituted lanthanum manganite (La0.5Eu0.5)0.7Pb0.3MnO3 have been measured at temperatures close to the metal-insulator transition temperature and at low temperatures. In both cases, the current-voltage characteristics exhibit nonlinear properties that are strongly dependent on the strength of an applied magnetic field. The mechanisms responsible for the nonlinear properties at these temperatures are found to be different: near the metal-insulator transition, the current-voltage characteristics are determined by the phase layering inside granules, while at low temperatures, they are determined by tunneling of carriers through insulating interlayers of the granules.
- Published
- 2011
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- View/download PDF
32. Pinning in a porous high-temperature superconductor Bi2223
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Denis Gokhfeld, K. Yu. Terent’ev, K. A. Shaikhutdinov, S. I. Popkov, and M. I. Petrov
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Superconductivity ,High-temperature superconductivity ,Materials science ,Solid-state physics ,Condensed matter physics ,Condensed Matter Physics ,Curvature ,Electronic, Optical and Magnetic Materials ,law.invention ,Vortex ,Magnetic field ,Electrical resistance and conductance ,law ,Condensed Matter::Superconductivity ,Phase (matter) - Abstract
The current-voltage characteristics of a porous superconductor Bi2Sr2Ca2Cu3Ox (Bi2223) have been measured at temperatures in the range from 10 to 90 K in magnetic fields of 0–80 kOe. The experimental dependences have been analyzed within the model allowing for pinning by clusters of a normal phase with fractal boundaries, as well as the model taking into account phase transformations of vortex matter. It has been found that the electrical resistance of the superconductor material significantly increases at temperatures of 60–70 K over the entire range of magnetic fields under consideration without changing in the sign of the curvature of the dependence R(I). It has been assumed that this behavior is associated with the specific feature of the pinning in a highly porous high-temperature superconductor, which lies in the fractality of the distribution of pinning centers in a wide range of self-similarity scales. The studied material at the aforementioned temperatures is characterized by the melting of the vortex structure.
- Published
- 2011
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33. General regularities of magnetoresistive effects in the polycrystalline yttrium and bismuth high-temperature superconductor systems
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M. I. Petrov, S. I. Popkov, A. A. Dubrovskii, A. A. Bykov, K. A. Shaikhutdinov, S. V. Semenov, and D. A. Balaev
- Subjects
Superconductivity ,High-temperature superconductivity ,Materials science ,Condensed matter physics ,Magnetoresistance ,chemistry.chemical_element ,Thermomagnetic convection ,Condensed Matter Physics ,Electronic, Optical and Magnetic Materials ,law.invention ,Bismuth ,chemistry ,law ,Grain boundary ,Texture (crystalline) ,Crystallite - Abstract
The influence of thermomagnetic prehistory on the behavior of a resistive transition R(T) in external magnetic fields of polycrystalline YBa2Cu3O7 and Bi1.8Pb0.3Sr1.9Ca2Cu3Ox high-temperature supercon-ductors and the Bi1.8Pb0.3Sr1.9Ca2Cu3Ox + Ag texture has been investigated. It has been found that, for YBa2Cu3O7, the thermomagnetic prehistory exerts a substantial influence on the dissipation in the subsystem of grain boundaries in magnetic fields up to ∼103 Oe, and this effect becomes insignificant in fields higher than ∼104 Oe. This behavior has been explained by the influence of magnetic moments of high-temperature superconductor grains on the effective magnetic field in the intergranular medium. For bismuth high-temperature superconductors, no influence of thermomagnetic prehistory on the resistive transition has been observed; however, this effect manifests itself in current-voltage characteristics at high transport current densities. There is also a radical difference in the behavior of isotherms of the magnetoresistance R(H) for the yttrium and bismuth systems. For YBa2Cu3O7, there is a clear separation between the dissipation regimes in the intergranular medium and in grains, which manifests itself even at low transport current densities as a change of sign in the curvature of the dependence R(H). For a texture based on the bismuth high-temperature superconductor, this feature has been observed only at high current densities (comparable to the critical current density at H = 0). This difference in the behavior of magnetoresistive properties of the classical high-temperature superconductor systems under investigation has been explained by relatively low irreversibility fields of the bismuth high-temperature superconductors. In these materials, simultaneous processes of dissipation can occur in an external magnetic field both in the subsystem of grain boundaries between crystallites and in the crystallites themselves.
- Published
- 2011
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34. Contributions from Inter-grain Boundaries to the Magneto-resistive Effect in Polycrystalline High-T C Superconductors. The Underlying Reason of Different Behavior for YBCO and BSCCO Systems
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A. A. Dubrovskiy, M. I. Petrov, E. I. Sabitova, K. A. Shaikhutdinov, S. I. Popkov, A. A. Bykov, S. V. Semenov, and D. A. Balaev
- Subjects
Superconductivity ,Materials science ,Magnetoresistance ,Condensed matter physics ,Field (physics) ,Grain boundary ,Crystallite ,Dissipation ,Condensed Matter Physics ,Current density ,Electronic, Optical and Magnetic Materials ,Magnetic field - Abstract
In order to clarify the mechanisms in charge of broadening of resistive transition R(T) in magnetic fields of bismuth-based polycrystalline high-T C superconductor (HTSC), a comparative study of Bi1.8Pb0.3Sr1.9Ca2Cu3O x (BSCCO) and YBa2Cu3O7−δ (YBCO) have been performed. Magnetoresistive effects and irreversibility line obtained from magnetic measurements have been studied. It was established that (1) for YBCO, the smooth part of R(T) dependence unambiguously corresponds to dissipation in the intergrain boundaries for arbitrary magnetic fields; (2) for polycrystalline BSCCO, the smooth part of R(T) dependences correspond to dissipation within intergrain boundary subsystem in the field range H 102 Oe reflect the dissipation processes occurring both in intergrain boundary and HTSC grain subsystems; (3) for the high-field range, the contribution from intergrain boundaries of BSCCO can be distinguished from magnetoresistance R(H) dependences obtained at high enough current density on textured samples. It is proposed that various magneto-resistive properties of these classical HTSC systems are due comparatively weak pinning in BSCCO.
- Published
- 2011
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35. Non-linear current–voltage characteristics of (La0.5Eu0.5)0.7Pb0.3MnO3 single crystals: Possible manifestation of the internal heating of chargecarriers
- Author
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S. I. Popkov, K. A. Shaykhutdinov, A. A. Dubrovskiy, S. V. Semenov, N. V. Sapronova, A. A. Bykov, N. V. Volkov, and D. A. Balaev
- Subjects
Materials science ,Condensed matter physics ,Dielectric ,Condensed Matter Physics ,Manganite ,Electronic, Optical and Magnetic Materials ,Charge ordering ,chemistry.chemical_compound ,Hysteresis ,Thermal conductivity ,Lanthanum manganite ,chemistry ,Electric field ,Electrical and Electronic Engineering ,Internal heating - Abstract
Temperature evolution of the current–voltage characteristics (CVCs) of a single-crystal lanthanum manganite (La 0.5 Eu 0.5 ) 0.7 Pb 0.3 MnO 3 is investigated in a wide (up to 1 А) range of instrumental currents. Effects of a transport current and an applied electric field on the resistance of the material are studied in view of possible implementation of the charge ordering break in dielectric regions occurring due to phase separation in manganites. A negative differential resistance portion observed in the CVCs suggests the presence of a current switching effect. Below the temperature of the metal–dielectric transition in (La 0.5 Eu 0.5 ) 0.7 Pb 0.3 MnO 3 , the hysteresis is observed in the CVC. The detailed analysis of the internal sample heating on the basis of experimental data on thermal conductivity showed, however, that these CVC features can be explained within the concept of non-equilibrium heating of electron gas.
- Published
- 2010
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36. Features of the low-temperature specific heat in underdoped YBa2Cu3O6 + x single crystals
- Author
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A. N. Lavrov, V. V. Val’kov, M. Yu. Kameneva, K. A. Shaykhutdinov, L. P. Kozeeva, S. I. Popkov, A. D. Fedoseev, and D. M. Dzebisashvili
- Subjects
Work (thermodynamics) ,Materials science ,Physics and Astronomy (miscellaneous) ,Condensed matter physics ,Solid-state physics ,Drop (liquid) ,Doping ,Anomaly (physics) ,Atmospheric temperature range ,Magnetic field ,Spin-½ - Abstract
The behavior of the low-temperature specific heat C(T) for YBa2Cu3O6 + x single crystals with the doping level corresponding to the normal phase has been studied by the relaxation technique at different values of the applied magnetic field. It has been found that the C(T)/T plot exhibits such an anomaly as a steep increase with decreasing temperature from T about 4 K down to T ≤ 2 K (the minimum temperature value accessible in the experiment). The applied magnetic field as high as 9 T inverts this anomaly and leads to a sharp drop in C(T)/T during cooling within the same temperature range. A model involving the Schottky-type centers formulated in this work and the data on spin correlation functions has allowed us to calculate the temperature dependence of the specific heat, which fits the experimental curves quite well.
- Published
- 2010
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37. Nonmonotonic behavior of magnetoresistance, R(H) hysteresis, and low-temperature heat capacity of the BaPb0.75Bi0.25O3 superconductor in a magnetic field: Possible manifestations of phase separation
- Author
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A. A. Dubrovskiy, K. A. Shaikhutdinov, Oleg N. Martyanov, M. I. Petrov, D. A. Balaev, and S. I. Popkov
- Subjects
Superconductivity ,Josephson effect ,Hysteresis ,Materials science ,Condensed matter physics ,Magnetoresistance ,Condensed Matter::Superconductivity ,General Physics and Astronomy ,Diamagnetism ,Type-II superconductor ,Magnetic flux ,Magnetic field - Abstract
The transport properties (R(T) and R(H) dependences at various values of the transport current in magnetic fields up to 65 kOe) and low-temperature heat capacity in magnetic fields up to 90 kOe of the BaPb0.75Bi0.25O3 superconductor (TC ≈ 11.3 K) are investigated with the goal of clarifying the mechanisms determining the nonmonotonic behavior and hysteresis of its magnetoresistance R(H). The type of R(H) hysteretic dependences for BaPb0.75Bi0.25O3 is analogous to that observed in granular high-Tc superconductors (HTSCs); however, unlike classical HTSC systems, the field width of the magnetoresistance hysteresis loop for polycrystalline BaPb0.75Bi0.25O3 depends on the transport current. This means that although the mechanisms responsible for the magnetoresistance hysteresis (the influence of the magnetic flux trapped in superconducting regions on the effective field in Josephson interlayers) are identical in these objects, the transport current in BaPb0.75Bi0.25O3 may considerably affect the diamagnetic response of the superconductor. A considerable effect of transport current on the field in which the R(H) dependences have a peak and exhibit hysterestic properties is observed. Such a behavior can be adequately interpreted using the model of the spatially inhomogeneous superconductor-insulator state proposed by Gorbatsevich et al. [JETP Lett. 52, 95 (1990)]. The nonmonotonic dependence of quantity C/T (C is the heat capacity) on the magnetic field discovered in the present study also agrees with the conclusions based on this model.
- Published
- 2010
- Full Text
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38. Magnetoresistance hysteresis of bulk textured Bi1.8Pb0.3Sr1.9Ca2Cu3Ox+Ag ceramics and its anisotropy
- Author
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Denis Gokhfeld, M. I. Petrov, D. A. Balaev, S. I. Popkov, K. A. Shaykhutdinov, A. A. Bykov, and S. V. Semenov
- Subjects
Superconductivity ,Materials science ,Condensed matter physics ,Magnetoresistance ,Magnetic moment ,Energy Engineering and Power Technology ,Condensed Matter Physics ,Electronic, Optical and Magnetic Materials ,Magnetic field ,Condensed Matter::Materials Science ,Dipole ,Magnetization ,Hysteresis ,Condensed Matter::Superconductivity ,Electrical and Electronic Engineering ,Anisotropy - Abstract
Magnetoresistance of bulk textured Bi1.8Pb0.3Sr1.9Ca2Cu3Ox + Ag ceramics has been studied in the magnetic fields applied parallel and perpendicular to a–b planes of Bi2223 crystallites. Besides well known anisotropy of magnetoresistance of textured superconductors (RH || c > RH || a–b), anisotropic hysteresis of R(H) dependences was investigated. Parameters characterizing hysteretic R(H) curves differ for the cases H || c and H || a–b. This behavior is explained within the model of a granular superconductor where the total magnetic induction in the intercrystallite boundaries is superposition of the external field and the magnetic field induced by dipole magnetic moments of neighbor crystallites.
- Published
- 2010
- Full Text
- View/download PDF
39. Increase in the diamagnetic response from low-density Bi1.8Pb0.3Sr1.9Ca2Cu3O x high-temperature superconductors and Bi1.8Pb0.3Sr1.9Ca2Cu3O x + Ag composites
- Author
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S. I. Popkov, K. A. Shaykhutdinov, D. A. Balaev, Oleg N. Martyanov, A. A. Dubrovskii, I. L. Belozerova, and M. I. Petrov
- Subjects
Superconductivity ,High-temperature superconductivity ,Materials science ,Physics and Astronomy (miscellaneous) ,Condensed matter physics ,Microstructure ,Magnetic flux ,law.invention ,Magnetization ,law ,Diamagnetism ,Crystallite ,Composite material ,Porous medium - Abstract
Low-density polycrystalline Bi1.8Pb0.3Sr1.9Ca2Cu3Ox high-temperature superconductors with a foamlike microstructure and composites consisting of this superconductor and silver in an amount of 20, 25, and 30 vol % are synthesized. The microstructure, as well as the temperature and field dependences of the magnetization, M(T) and M(H), are studied. It is found that, in Bi1.8Pb0.3Sr1.9Ca2Cu3Ox high-temperature superconductors and Bi1.8Pb0.3Sr1.9Ca2Cu3Ox + Ag composites, the diamagnetic response is enhanced and the screening properties are improved compared with high-temperature polycrystalline superconductors with the same composition that are prepared by the standard technology. The observed effect is explained by the features of magnetic flux penetration into a porous medium.
- Published
- 2009
- Full Text
- View/download PDF
40. Mechanism of formation of a negative magnetoresistance region in granular high-temperature superconductors
- Author
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K. A. Shaikhutdinov, D. A. Balaev, S. I. Popkov, and M. I. Petrov
- Subjects
Superconductivity ,High-temperature superconductivity ,Materials science ,Colossal magnetoresistance ,Condensed matter physics ,Field (physics) ,Magnetoresistance ,Condensed Matter Physics ,Microstructure ,Electronic, Optical and Magnetic Materials ,law.invention ,Dipole ,law ,Diamagnetism - Abstract
The field dependences of the magnetoresistance of Bi1.8Pb0.3Sr1.9Ca2Cu3Ox samples with different densities, which have a foam microstructure and exhibit different diamagnetic responses, were studied at 77.4 K to identify the mechanism responsible for the formation of a negative magnetoresistance region in granular high-temperature superconductors. A region with negative magnetoresistance was found to exist in samples with magnetizations highest in absolute magnitude. This behavior finds a reasonable interpretation as due to the effect exerted by dipole moments of high-temperature superconductor grains on the effective intergranular field. The strength of this effective field has been estimated.
- Published
- 2009
- Full Text
- View/download PDF
41. Mechanism of the hysteretic behavior of the magnetoresistance of granular HTSCs: The universal nature of the width of the magnetoresistance hysteresis loop
- Author
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D. A. Balaev, K. A. Shaikhutdinov, S. I. Popkov, Yu. S. Gokhfeld, A. A. Dubrovskiĭ, M. I. Petrov, and Denis Gokhfeld
- Subjects
Superconductivity ,Hysteresis ,Materials science ,Colossal magnetoresistance ,Magnetoresistance ,Condensed matter physics ,Condensed Matter::Superconductivity ,Relaxation (NMR) ,General Physics and Astronomy ,Current density ,Type-II superconductor ,Magnetic field - Abstract
The hysteretic behavior of the magnetoresistance R(H) of granular high-temperature superconductors (HTSCs) of the Y-Ba-Cu-O, Bi-Ca-Sr-Cu-O, and La-Sr-Cu-O classical systems is investigated for transport current densities lower and higher than the critical density (at H = 0). All systems exhibit universal behavior of the width of the magnetoresistance hysteresis loop: independence of transport current under identical external conditions. This means that flux trapping in HTSC grains is the main mechanism controlling the hysteretic behavior of the magnetoresistance of granular HTSCs, while pinning of Josephson vortices in the intragranular medium makes no appreciable contribution to the formation of magnetoresistance hysteresis (when transport current flows through the sample). Experimental data on relaxation of residual resistance after the action of a magnetic field also confirm this conclusion.
- Published
- 2009
- Full Text
- View/download PDF
42. Peculiarities of the time evolution of magnetoresistance of granular HTSC in a constant applied magnetic field
- Author
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M. I. Petrov, D. A. Balaev, A. A. Dubrovskiy, K. A. Shaykhutdinov, and S. I. Popkov
- Subjects
Superconductivity ,Materials science ,Magnetoresistance ,Field (physics) ,Condensed matter physics ,Relaxation (NMR) ,Time evolution ,General Chemistry ,Condensed Matter Physics ,Magnetic field ,Magnetization ,Condensed Matter::Superconductivity ,Materials Chemistry ,Crystallite - Abstract
The time evolution of the magnetoresistance of bulk YBCO + CuO composites at T = 4.2 K in constant applied magnetic fields was studied to clarify the mechanism of hysteretic behavior of magnetoresistance R ( H ) of granular HTSC. The composites represent “model” granular HTSC with weakened Josephson coupling between superconducting (YBCO) crystallites. It was found for the first time that on the ascending branch of R ( H ) dependence, the resistance at H = const decreased with time while on the descending branch, the resistance increased with time in an applied constant magnetic field. In the range of low magnetic fields (below the minimum point of the descending branch of the R(H) dependence), the resistance at H = const decreased again. Similar measurements performed on pure polycrystalline YBCO at T = 77.4 K have shown that the behavior of evolution of resistance with time is similar to that observed for the composite. This proves the peculiarity of time evolution of magnetoresistance to be a common feature of granular HTSCs. The behavior revealed is well described by the model of granular HTSC, where the intergrain media is in an effective magnetic field which is the superposition of the external field and the field induced by superconducting grains. The time evolution of resistance reflects the time relaxation of magnetization of HTSC grains due to the intragrain flux creep processes.
- Published
- 2008
- Full Text
- View/download PDF
43. Relaxation of the remanent resistance of granular HTSC Y-Ba-Cu-O + CuO composites after magnetic field treatment
- Author
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M. I. Petrov, K. A. Shaĭkhutdinov, S. I. Popkov, A. A. Dubrovskiĭ, and D. A. Balaev
- Subjects
Josephson effect ,Magnetization ,Hysteresis ,Materials science ,Solid-state physics ,Magnetoresistance ,Condensed matter physics ,Composite number ,Relaxation (NMR) ,Composite material ,Condensed Matter Physics ,Electronic, Optical and Magnetic Materials ,Magnetic field - Abstract
The hysteresis of magnetoresistance R(H) and relaxation of the remanent resistance R rem with time after magnetic field treatment of HTSC (Y-Ba-Cu-O) + CuO composites are studied. Such a composite constitutes a network of Josephson junctions wherein the nonsuperconducting component (CuO) forms Josephson barriers between HTSC grains. By comparing the experimental R rem(t) and R(H) dependences, it is shown that the relaxation of the remanent resistance is caused by the decreased magnetic field in the intergrain medium due to relaxation of magnetization. The reason is uncovered for the differences between the published values of pinning potentials determined by measuring the relaxation of magnetization or resistance and fitting them by the Anderson law.
- Published
- 2008
- Full Text
- View/download PDF
44. Magnetic Field Dependence of Intergrain Pinning Potential in Bulk Granular Composites YBCO + CuO Demonstrating Large Magneto-Resistive Effect
- Author
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M. I. Petrov, S. I. Popkov, D. A. Balaev, K. A. Shaykhutdinov, and A. A. Dubrovskiy
- Subjects
Josephson effect ,Resistive touchscreen ,Flux pinning ,Materials science ,Magnetoresistance ,Condensed matter physics ,Flux ,Atmospheric temperature range ,Condensed Matter::Mesoscopic Systems and Quantum Hall Effect ,Condensed Matter Physics ,Electronic, Optical and Magnetic Materials ,Magnetic field ,Condensed Matter::Superconductivity ,Composite material ,Magneto - Abstract
The broadening of the resistive transition in magnetic field and isotherms of magnetoresistance of bulk composites Y–Ba–Cu–O + CuO have been studied. These composites exhibit large magneto-resistive effect in a wide temperature range below TC due to weakening of Josephson coupling in this system. The broadening of the resistive transition and magnetoresistance are explained well by the Ambegaokar–Halperin (AH) model for phase slip in Josephson junctions. The magnetic field dependence of pinning potential in the intergrain boundaries deduced from AH model found out to be similar to that of critical current of an array of Josephson junctions. The values of pinning energy point out that the large magneto-resistive effect observed in the composites results from flux flow-like processes at the intergrain boundaries.
- Published
- 2008
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45. Magnetoresistance hysteresis in granular HTSCs as a manifestation of the magnetic flux trapped by superconducting grains in YBCO + CuO composites
- Author
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D. A. Balaev, Denis Gokhfeld, S. I. Popkov, A. A. Dubrovskiĭ, K. A. Shaikhutdinov, and M. I. Petrov
- Subjects
Josephson effect ,Superconductivity ,Hysteresis ,Materials science ,Condensed matter physics ,Magnetoresistance ,Condensed Matter::Superconductivity ,General Physics and Astronomy ,Composite material ,Magnetic hysteresis ,Type-II superconductor ,Current density ,Magnetic flux - Abstract
Hysterestic behavior of the magnetoresistance of granular HTSCs and its interaction with the magnetic hysteresis are studied by measuring magnetoresistance R(H) and critical current Ic(H) of composites formed by HTSC Y0.75Lu0.25Ba2Cu3O7 and CuO. A network of Josephson junctions is formed in such composites, in which the nonsuperconducting component plays the role of barriers between HTSC grains. Hysteretic dependences R(H) of magnetoresistance are studied in a wide range of transport current density j and are analyzed in the framework of the two-level model of a granular superconductor, in which dissipation takes place in the Josephson medium and the magnetic flux can be pinned both in grains and in the Josephson medium. The interrelation between the hysteresis of critical current Ic(H) and the evolution of the hysterestic dependence R(H) of the magnetoresistance upon transport current variation is demonstrated experimentally. The effect of the magnetic past history on the hysteretic behavior of R(H) and the emergence of a segment with a negative magnetoresistance are analyzed. It is shown for the first time that the R(H) dependences are characterized by a parameter that is independent of the transport current, viz., the width of the R(H) hysteresis loop.
- Published
- 2007
- Full Text
- View/download PDF
46. Highly textured bismuth-containing high-temperature superconductor ceramics obtained by uniaxial pressing in liquid medium: Fabrication and properties
- Author
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I. L. Belozerova, M. I. Petrov, Oleg N. Martyanov, A. D. Vasil’ev, K.A. Shaihutdinov, Denis Gokhfeld, D. A. Balaev, and S. I. Popkov
- Subjects
Superconductivity ,Materials science ,Fabrication ,High-temperature superconductivity ,Physics and Astronomy (miscellaneous) ,Annealing (metallurgy) ,Scanning electron microscope ,chemistry.chemical_element ,Bismuth ,law.invention ,Nuclear magnetic resonance ,chemistry ,law ,visual_art ,visual_art.visual_art_medium ,Diamagnetism ,Ceramic ,Composite material - Abstract
A new method of fabricating textured ceramics with a composition of Bi1.8Pb0.3Sr1.9Ca2Cu3Ox is described, according to which the initial low-density ceramics is subjected to uniaxial pressing in a liquid medium followed by drying and annealing. Analysis of the X-ray diffraction and scanning electron microscopy data show evidence for a high degree of texture in high-temperature superconductor ceramics fabricated using the proposed method. The results of magnetic measurements indicate that the obtained material possesses anisotropy of the magnetic moment for the magnetic field H oriented parallel and perpendicular to the direction of uniaxial pressing. The textured ceramics also show high diamagnetic response for H parallel to the c axis of grains, which makes these ceramics promising materials for practical applications.
- Published
- 2007
- Full Text
- View/download PDF
47. Thermally activated dissipation in a novel foamed Bi-based oxide superconductor in magnetic fields
- Author
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M. I. Petrov, A.D. Vasilyev, D. A. Balaev, K. A. Shaykhutdinov, S. I. Popkov, and Oleg N. Martyanov
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Josephson effect ,Superconductivity ,Flux pumping ,Materials science ,Flux pinning ,Condensed matter physics ,Metals and Alloys ,Oxide ,Dissipation ,Condensed Matter Physics ,Magnetic field ,Pi Josephson junction ,chemistry.chemical_compound ,chemistry ,Condensed Matter::Superconductivity ,Materials Chemistry ,Ceramics and Composites ,Electrical and Electronic Engineering - Abstract
The transport properties of a novel foamed superconductor Bi1.8Pb0.3Sr1.9Ca2Cu3Ox have been studied. As the analysis of resistive transitions in a magnetic field shows, the dissipation follows a thermally activated flux creep model with the temperature-independent pinning potential in S–N–S-type Josephson junctions.
- Published
- 2007
- Full Text
- View/download PDF
48. Investigation of the Josephson coupling through a magnetoactive barrier (ferrimagnet, paramagnet) in Y3/4Lu1/4Ba2Cu3O7 + Y3(Al1 − x Fe x )5O12 composites
- Author
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S. I. Popkov, Mihail Petrov, K. A. Shaĭkhutdinov, and D. A. Balaev
- Subjects
Josephson effect ,Superconductivity ,Paramagnetism ,Materials science ,Electrical resistance and conductance ,Magnetic moment ,Magnetoresistance ,Condensed matter physics ,Ferrimagnetism ,Atmospheric temperature range ,Composite material ,Condensed Matter Physics ,Electronic, Optical and Magnetic Materials - Abstract
The transport properties of two-phase composites consisting of a high-temperature superconductor and a nonsuperconducting component with magnetic ordering are analyzed. These composites are considered as a network of “superconductor-magnetoactive insulator-superconductor” weak links of the Josephson type. Substituted garnets Y3(Al1 − xFex)5O12 (x = 0, ..., 1.0) are used as a magnetoactive component. The composites under investigation contain 92.5 vol % Y3/4Lu1/4Ba2Cu3O7 (the high-temperature superconductor) and 7.5 vol % Y3(Al1 − xFex)5O12 (x = 0, ..., 1.0). It is shown that an increase in the iron content in the Y3(Al1 − xFex)5O12 garnet leads to a reduction of the Josephson coupling strength: the temperature range in which the electrical resistance of the composites is equal to zero is reduced, and the critical current density at a temperature of 4.2 K decreases exponentially. For composites in which the iron content in the Y3(Al1 − xFex)5O12 garnet is higher than 0.1, the temperature dependence of the electrical resistance R(T) at temperatures below the transition point TC of high-temperature superconductor crystallites has a portion in the range Tm-TC where the resistance R(T) is independent of the transport current and the magnetic field strength. Below the temperature Tm, the dependences of the electrical resistance R(T) of the composites are nonlinear functions of the current and involve a considerable contribution from magnetoresistance. This behavior is characteristic of a network of Josephson junctions. The temperature Tm decreases with an increase in the iron content in the Y3(Al1 − xFex)5O12 garnet. The appearance of the above feature in the temperature dependences of the electrical resistance R(T) is interpreted as complete suppression of the Josephson coupling in the temperature range above Tm due to the interaction of supercurrent carrier pairs with magnetic moments of iron atoms in the dielectric barriers separating high-temperature superconductor grains.
- Published
- 2006
- Full Text
- View/download PDF
49. Magnetic properties of a low-density Bi-based HTSC
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M. I. Petrov, S. A. Satzuk, K. A. Shaikhutdinov, D. A. Balaev, Denis Gokhfeld, and S. I. Popkov
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Superconductivity ,Physics ,Magnetization ,Condensed matter physics ,Superconducting material ,Permeability (electromagnetism) ,Condensed Matter::Superconductivity ,Metallic materials ,Materials Chemistry ,Low density ,Condensed Matter Physics ,Magnetic field - Abstract
The preliminary results of the investigation of magnetic properties of a novel low-density superconducting material Bi1.8Pb0.3Sr2Ca2Cu3Ox with a low density and microfoam structure are presented. The temperature, magnetic field, and time dependences of magnetization M have been measured. The experimental hysteresis loops M(H) are well described in the framework of the Val’kov-Khrustalev theory developed for type II granular superconductors.
- Published
- 2006
- Full Text
- View/download PDF
50. Mechanisms of dissipation in a Josephson medium based on a high-temperature superconductor in a magnetic field
- Author
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K. A. Shaĭkhutdinov, M. I. Petrov, S. I. Popkov, and D. A. Balaev
- Subjects
Superconductivity ,Josephson effect ,Arrhenius equation ,Flux pumping ,Flux pinning ,Materials science ,Condensed matter physics ,Thermal fluctuations ,Condensed Matter Physics ,Electronic, Optical and Magnetic Materials ,Magnetic field ,Pi Josephson junction ,symbols.namesake ,Condensed Matter::Superconductivity ,symbols - Abstract
This paper reports on the results of an investigation into the influence of magnetic fields (0–60 kOe) on the temperature dependences of the electrical resistance R(T) of the Y3/4Lu1/4Ba2Cu3O7 + CuO composites. The structure of these composites is considered to be a network of tunnel-type Josephson junctions in which a nonsuperconducting component (CuO) forms boundaries (barriers) between high-temperature superconducting crystallites. The temperature dependence R(T) of the composites has two steps characteristic of granular superconductors: (i) an abrupt change in the electrical resistance at the critical temperature of high-temperature superconducting crystallites and (ii) a smooth transition to the superconducting state under the influence of the boundaries between the crystallites. The experimental dependences R(T) are analyzed within the Ambegaokar-Halperin model of thermal fluctuations in Josephson junctions and the flux creep model. An increase in the magnetic field leads to a crossover from the Ambegaokar-Halperin mechanism to the flux creep mechanism. The temperature dependences R(T) in the range of weak magnetic fields (from 0 to 102 Oe) are adequately described by the relationship following from the Ambegaokar-Halperin model. In the range of strong magnetic fields (from 103 to 6 × 104 Oe), the dissipation obeys the Arrhenius law R ∼ exp(−U(H)/T)], which is characteristic of the flux creep model with a temperature-independent pinning energy U(H). The effective Josephson coupling energies and the pinning energies corresponding to the Ambegaokar-Halperin and flux creep mechanisms are determined.
- Published
- 2006
- Full Text
- View/download PDF
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