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Cohesive horizons are widespread along the Brazilian coastal tablelands and, despite their importance to soil management under intensive cultivation, their genesis remains, in many aspects, controversial. Studies diverge and indicate the participation of different mechanisms in the formation of these soil horizons. Although clay illuviation has been considered as one of the processes determining the formation of this soil attribute, recent studies suggest a limited participation of this soil process. The aim of the present study was to evaluate the relative contribution of argilluviation and sorting of sand to the genesis of cohesive horizons in an Ultisol toposequence from a toposequence from north-east Brazil. Soil samples were collected from cohesive and non-cohesive horizons from four soil profiles. We determined bulk soil density (BD), penetration resistance (PR), particle size distribution and the percentage of different sand fractions. The sand fractionation data were treated statistically to obtain different grain size parameters, such as mean grain size, sorting and kurtosis. An additional micromorphological study was performed on cohesive and non-cohesive horizons. The lowest BD and PR were recorded in non-cohesive horizons (1.53 Mg [m.sup.-3] and 0.74 MPa, respectively), whereas significantly higher values of BD (1.66-1.80 Mg [m.sup.-3]) and PR (2.61-7.71 MPa) were observed in cohesive horizons. Thin sections of cohesive soil horizons showed a significant reduction in void sizes and interconnecting pores compared with non-cohesive soil horizons. The higher values of BD and PR observed in the cohesive horizons are apparently related to this poorly interconnected void network. Textural pedofeatures observable with optical microscopy, which indicate argilluviation, were only found in one cohesive horizon. Sand fractionation showed a predominance of medium and fine sand fractions and indicated the dominance of poorly selected sand in cohesive horizons, probably causing the higher BD and PR values. However, the presence of textural pedofeatures (clay coatings) in one of the cohesive horizons studied may indicate a combined contribution of sand heterogeneity and argilluviation in the genesis of these horizons. Overall, the results of the present study showed that subtle variations in the distribution of basic soil components (i.e. particle size fractions) may determine the formation of cohesive horizons and thus must be taken into account in future studies aiming to predict their spatial distribution and to establish more efficient management strategies. Additional keywords: hard-setting soils, micromorphology, pedogenesis, soil physical properties, tropical soils. Received 27 June 2013, accepted 10 September 2014, published online 1 December 2014, Introduction The Coastal Tablelands represent a geomorphological unit of great social and economic importance in Brazil, extending from Rio de Janeiro to the Amazon (Amapa state) of Brazil. These coastal [...]

Wetland soils, especially those under a semi-arid climate, are among the least studied soils in the tropics. The hypersaline tidal flats on the north-eastern Brazilian coast, locally named apicum, are coastal wetland ecosystems in the peripheral portions of semi-arid estuaries. Despite their great ecological importance, they have been highly impacted by anthropogenic activities. Morphological and analytical data of six soil profiles, representative of the different coastal compartments (mangroves, apicum and coastal tablelands) of the north-eastern Brazilian coast, were examined to better understand the pedogenesis of apicum soils. The hypersaline tidal flat soils were classified as Typic Fluvaquents and Typic Sulfaquents with the following main characteristics: predominance of sand fraction (62-77%); presence of high- activity clays (> 24 [cmol.sub.c] [kg.sup.-1] clay); clay fraction comprising kaolinite, illite, smectite and an interstratified smectite/illite; exchangeable complex dominated by [Na.sup.+] (ESP [greater than or equal to] 15%); elevated levels of salinity (electrical conductivity, EC 25-44 dS [m.sup.-1]); alkaline pH values (7.5-9.5). The sandy texture and quartz-dominated composition of the hypersaline, tidal flat soils indicate a pedogenesis associated with the superficial addition of mineral material. This upbuilding process would have lowered the watertable (relatively to the ground level) and decreased the flooding frequency by the tides, favouring salinisation and solonisation processes at the hypersaline tidal flats. Furthermore, the still-existing hydromorphism would have promoted the maintenance of gleisation and sulfidisation. The presence of pyrite on the hyper-saline tidal flat soils further corroborates the formation of apicum soils from/over buried mangroves. Additional keywords: coastal wetlands, mineralogy, soil genesis. Received 16 October 2012, accepted 22 October 2013, published online 13 March 2014, Introduction The terms salt flats (Ridd and Stieglitz 2002), supratidal flats, hypersaline tidal flats and unvegetated flats (Hadlich et al. 2009) are used to refer to coastal ecosystems on the [...]

In Oaxaca, México, Haplophyton cimicidum is used in combination with other plants as part of a folk strategy against arthropod pests of crops and cattle. Methanolic and crude alkaloid (acid–base extraction) extracts of H. cimicidum leaves were analysed by thin-layer chromatography (TLC) and assayed in vitro for acetylcholinesterase (AChE) inhibitory activity using Spodoptera frugiperda homogenates as source of enzyme. Derivatised chromatographic plates indicated the presence of indoles and alkaloids in the extracts. The crude alkaloid extract exhibited a higher number of compounds than the methanolic extract as judged by the number of spots on TLC plates. The crude alkaloid extract had a weak inhibition potential of AChE with a lower IC50 (93 μg mL− 1) than the methanolic extract (159 μg mL− 1). Indole alkaloids may be responsible for the activity, though a subsequent analysis of the extract components is necessary to determine the active alkaloid(s). [ABSTRACT FROM AUTHOR]