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1. Selective Synthesis of Symmetrical Thiosulfonates via Oxidative Coupling of Thiols Catalyzed by Diorganyl Diselenide.

Author

Silva, Calebe H. L., Soares, Jéssica, Peixoto, Carlos R. M., Azeredo, Juliano B., de Souza, Bruno S., Rohers, Juliano A., and Godoi, Marcelo

Subjects
OXIDATIVE coupling, RADICALS (Chemistry), THIOLS
Abstract

A straightforward methodology for the synthesis of symmetrical thiosulfonates through direct oxidative coupling of thiols is reported. Dibutyl diselenide was suitably applied as a catalyst for the selective conversion of thiols into respective thiosulfonates in good yields. Moreover, mechanistic studies revealed a radical reaction pathway for the preparation of target products. [ABSTRACT FROM AUTHOR]

Published
2023
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