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1. 2021 roadmap for sodium-ion batteries

Author

Tapia-Ruiz, N, Armstrong, AR, Alptekin, H, Amores, MA, Au, H, Barker, J, Boston, R, Brant, WR, Brittain, JM, Chen, Y, Chhowalla, M, Choi, YS, Costa, SIR, Ribadeneyra, MC, Cussen, SA, Cussen, EJ, David, WIF, Desai, AV, Dickson, SAM, Eweka, EI, Forero-Saboya, JD, Grey, CP, Griffin, JM, Gross, P, Hua, X, Irvine, JTS, Johansson, P, Jones, MO, Karlsmo, M, Kendrick, E, Kim, E, Kolosov, OV, Li, Z, Mertens, SFL, Mogensen, R, Monconduit, L, Morris, RE, Naylor, AJ, Nikman, S, O'Keefe, CA, Ould, DMC, Palgrave, RG, Poizot, P, Ponrouch, A, Renault, S, Reynolds, EM, Rudola, A, Sayers, R, Scanlon, DO, Sen, S, Seymour, VR, Silván, B, Sougrati, MT, Stievano, L, Stone, GS, Thomas, CI, Titirici, MM, Tong, J, Wood, TJ, Wright, DS, and Younesi, R

Subjects
energy materials, batteries, 13. Climate action, anodes, sodium ion, electrolytes, 7. Clean energy, cathodes
Abstract

Increasing concerns regarding the sustainability of lithium sources, due to their limited availability and consequent expected price increase, have raised awareness of the importance of developing alternative energy-storage candidates that can sustain the ever-growing energy demand. Furthermore, limitations on the availability of the transition metals used in the manufacturing of cathode materials, together with questionable mining practices, are driving development towards more sustainable elements. Given the uniformly high abundance and cost-effectiveness of sodium, as well as its very suitable redox potential (close to that of lithium), sodium-ion battery technology offers tremendous potential to be a counterpart to lithium-ion batteries (LIBs) in different application scenarios, such as stationary energy storage and low-cost vehicles. This potential is reflected by the major investments that are being made by industry in a wide variety of markets and in diverse material combinations. Despite the associated advantages of being a drop-in replacement for LIBs, there are remarkable differences in the physicochemical properties between sodium and lithium that give rise to different behaviours, for example, different coordination preferences in compounds, desolvation energies, or solubility of the solid–electrolyte interphase inorganic salt components. This demands a more detailed study of the underlying physical and chemical processes occurring in sodium-ion batteries and allows great scope for groundbreaking advances in the field, from lab-scale to scale-up. This roadmap provides an extensive review by experts in academia and industry of the current state of the art in 2021 and the different research directions and strategies currently underway to improve the performance of sodium-ion batteries. The aim is to provide an opinion with respect to the current challenges and opportunities, from the fundamental properties to the practical applications of this technology.

2. 2021 roadmap for sodium-ion batteries

Author

John T. S. Irvine, Emma Kendrick, Valerie R. Seymour, Aamod V. Desai, Edmund J. Cussen, Peter Gross, Andrew J. Naylor, Maria-Magdalena Titirici, Jake M. Brittain, Rebecca Boston, Ruth Sayers, Stewart A. M. Dickson, Sudeshna Sen, Sara I. R. Costa, Zhuangnan Li, Ashish Rudola, Heather Au, Dominic S. Wright, Nuria Tapia-Ruiz, Yongseok Choi, Hande Alptekin, John M. Griffin, Martin O. Jones, Marco Amores, Shahin Nikman, Eun Jeong Kim, A. Robert Armstrong, Reza Younesi, Maria Crespo Ribadeneyra, Laure Monconduit, William I. F. David, Christopher I Thomas, Patrik Johansson, Serena A. Cussen, Grant S. Stone, Jincheng Tong, Russell E. Morris, Clare P. Grey, Alexandre Ponrouch, Oleg Kolosov, Emmanuel I. Eweka, Darren M. C. Ould, Robert G. Palgrave, Thomas J. Wood, Yue Chen, Jerry Barker, Ronnie Mogensen, Stijn F. L. Mertens, Philippe Poizot, Juan Forero-Saboya, David O. Scanlon, Manish Chhowalla, Lorenzo Stievano, Emily M. Reynolds, Xiao Hua, Moulay Tahar Sougrati, William R. Brant, Martin Karlsmo, Stéven Renault, Christopher A. O’Keefe, Begoña Silván, Lancaster University, Harwell Science and Innovation Campus, Imperial College London, University of Sheffield [Sheffield], Faradion Limited, University of Virginia [Charlottesville], University of Oxford [Oxford], University of Cambridge [UK] (CAM), University College of London [London] (UCL), University of St Andrews [Scotland], AUTRES, Institut de Ciència de Materials de Barcelona (ICMAB-CSIC), Chalmers University of Technology [Gothenburg, Sweden], Science and Technology Facilities Council (STFC), University of Birmingham [Birmingham], Uppsala University, Institut Charles Gerhardt Montpellier - Institut de Chimie Moléculaire et des Matériaux de Montpellier (ICGM ICMMM), Ecole Nationale Supérieure de Chimie de Montpellier (ENSCM)-Centre National de la Recherche Scientifique (CNRS)-Université de Montpellier (UM)-Université Montpellier 1 (UM1)-Université Montpellier 2 - Sciences et Techniques (UM2)-Institut de Chimie du CNRS (INC), Réseau sur le stockage électrochimique de l'énergie (RS2E), Université de Picardie Jules Verne (UPJV)-Institut de Chimie du CNRS (INC)-Aix Marseille Université (AMU)-Université de Pau et des Pays de l'Adour (UPPA)-Université de Nantes (UN)-Université de Montpellier (UM)-Centre National de la Recherche Scientifique (CNRS)-Sorbonne Université (SU)-Ecole Nationale Supérieure de Chimie de Paris - Chimie ParisTech-PSL (ENSCP), Université Paris sciences et lettres (PSL)-Université Paris sciences et lettres (PSL)-Université de Haute-Alsace (UHA) Mulhouse - Colmar (Université de Haute-Alsace (UHA))-Collège de France (CdF (institution))-Institut polytechnique de Grenoble - Grenoble Institute of Technology (Grenoble INP ), Université Grenoble Alpes (UGA)-Université Grenoble Alpes (UGA)-Institut National Polytechnique (Toulouse) (Toulouse INP), Université Fédérale Toulouse Midi-Pyrénées-Université Fédérale Toulouse Midi-Pyrénées-Ecole Nationale Supérieure de Chimie de Montpellier (ENSCM), Institut des Matériaux Jean Rouxel (IMN), Université de Nantes - UFR des Sciences et des Techniques (UN UFR ST), Université de Nantes (UN)-Université de Nantes (UN)-Centre National de la Recherche Scientifique (CNRS)-Institut de Chimie du CNRS (INC)-Ecole Polytechnique de l'Université de Nantes (EPUN), Université de Nantes (UN)-Université de Nantes (UN), Alistore, European Commission, Swedish Research Council, Swedish Energy Agency, Swedish Research Council for Environment, Agricultural Sciences and Spatial Planning, Ministerio de Economía, Industria y Competitividad (España), Faraday Institution, Austrian Science Fund, Innovate UK, Tapia-Ruiz, Nuria [0000-0002-5005-7043], Armstrong, A Robert [0000-0003-1937-0936], Alptekin, Hande [0000-0001-6065-0513], Au, Heather [0000-0002-1652-2204], Barker, Jerry [0000-0002-8791-1119], Brant, William R [0000-0002-8658-8938], Choi, Yong-Seok [0000-0002-3737-2989], Costa, Sara I R [0000-0001-8105-207X], Crespo Ribadeneyra, Maria [0000-0001-6455-4430], Cussen, Serena A [0000-0002-9303-4220], Desai, Aamod V [0000-0001-7219-3428], Forero-Saboya, Juan D [0000-0002-3403-6066], Griffin, John M [0000-0002-8943-3835], Irvine, John T S [0000-0002-8394-3359], Johansson, Patrik [0000-0002-9907-117X], Karlsmo, Martin [0000-0002-0437-6860], Kendrick, Emma [0000-0002-4219-964X], Kolosov, Oleg V [0000-0003-3278-9643], Mertens, Stijn F L [0000-0002-5715-0486], Monconduit, Laure [0000-0003-3698-856X], Naylor, Andrew J [0000-0001-5641-7778], Poizot, Philippe [0000-0003-1865-4902], Renault, Stéven [0000-0002-6500-0015], Rudola, Ashish [0000-0001-9368-0698], Sayers, Ruth [0000-0003-1289-0998], Seymour, Valerie R [0000-0003-3333-5512], Silván, Begoña [0000-0002-1273-3098], Sougrati, Moulay Tahar [0000-0003-3740-2807], Stievano, Lorenzo [0000-0001-8548-0231], Thomas, Chris I [0000-0001-8090-4541], Titirici, Maria-Magdalena [0000-0003-0773-2100], Tong, Jincheng [0000-0001-7762-1460], Wood, Thomas J [0000-0002-5893-5664], Younesi, Reza [0000-0003-2538-8104], Apollo - University of Cambridge Repository, Kim, Eunjeong [0000-0002-2941-068], Kim, Eunjeong [0000-0002-2941-0682], University of Virginia, University of Oxford, Institut Charles Gerhardt Montpellier - Institut de Chimie Moléculaire et des Matériaux de Montpellier (ICGM), Ecole Nationale Supérieure de Chimie de Montpellier (ENSCM)-Institut de Chimie du CNRS (INC)-Université de Montpellier (UM)-Centre National de la Recherche Scientifique (CNRS), Université de Nantes (UN)-Aix Marseille Université (AMU)-Université de Haute-Alsace (UHA) Mulhouse - Colmar (Université de Haute-Alsace (UHA))-Collège de France (CdF (institution))-Université de Picardie Jules Verne (UPJV)-Ecole Nationale Supérieure de Chimie de Montpellier (ENSCM)-Ecole Nationale Supérieure de Chimie de Paris - Chimie ParisTech-PSL (ENSCP), Université Paris sciences et lettres (PSL)-Université Paris sciences et lettres (PSL)-Université de Pau et des Pays de l'Adour (UPPA)-Institut de Chimie du CNRS (INC)-Université de Montpellier (UM)-Sorbonne Université (SU)-Centre National de la Recherche Scientifique (CNRS)-Institut National Polytechnique (Toulouse) (Toulouse INP), Université de Toulouse (UT)-Université de Toulouse (UT)-Institut polytechnique de Grenoble - Grenoble Institute of Technology (Grenoble INP ), Université Grenoble Alpes (UGA)-Université Grenoble Alpes (UGA), Université de Nantes (UN)-Université de Nantes (UN)-Ecole Polytechnique de l'Université de Nantes (EPUN), Université de Nantes (UN)-Université de Nantes (UN)-Institut de Chimie du CNRS (INC)-Centre National de la Recherche Scientifique (CNRS), Tapia-Ruiz, N [0000-0002-5005-7043], Armstrong, AR [0000-0003-1937-0936], Alptekin, H [0000-0001-6065-0513], Au, H [0000-0002-1652-2204], Barker, J [0000-0002-8791-1119], Brant, WR [0000-0002-8658-8938], Choi, YS [0000-0002-3737-2989], Costa, SIR [0000-0001-8105-207X], Ribadeneyra, MC [0000-0001-6455-4430], Cussen, SA [0000-0002-9303-4220], Desai, AV [0000-0001-7219-3428], Forero-Saboya, JD [0000-0002-3403-6066], Griffin, JM [0000-0002-8943-3835], Irvine, JTS [0000-0002-8394-3359], Johansson, P [0000-0002-9907-117X], Karlsmo, M [0000-0002-0437-6860], Kendrick, E [0000-0002-4219-964X], Kolosov, OV [0000-0003-3278-9643], Mertens, SFL [0000-0002-5715-0486], Monconduit, L [0000-0003-3698-856X], Naylor, AJ [0000-0001-5641-7778], Poizot, P [0000-0003-1865-4902], Renault, S [0000-0002-6500-0015], Rudola, A [0000-0001-9368-0698], Sayers, R [0000-0003-1289-0998], Seymour, VR [0000-0003-3333-5512], Silván, B [0000-0002-1273-3098], Sougrati, MT [0000-0003-3740-2807], Stievano, L [0000-0001-8548-0231], Thomas, CI [0000-0001-8090-4541], Titirici, MM [0000-0003-0773-2100], Tong, J [0000-0001-7762-1460], Wood, TJ [0000-0002-5893-5664], Younesi, R [0000-0003-2538-8104], The Faraday Institution, University of St Andrews. School of Chemistry, University of St Andrews. Centre for Energy Ethics, University of St Andrews. Centre for Designer Quantum Materials, and University of St Andrews. EaSTCHEM

Subjects
Chemical process, Technology, Computer science, PAIR DISTRIBUTION FUNCTION, HIGH-ENERGY DENSITY, ELECTROCHEMICAL PROPERTIES, Materialkemi, 02 engineering and technology, 01 natural sciences, 7. Clean energy, Materials Chemistry, QD, LITHIUM-ION, Energy demand, Scope (project management), anodes, NA2TI3O7 NANOSHEETS, [CHIM.MATE]Chemical Sciences/Material chemistry, sodium ion, 021001 nanoscience & nanotechnology, Variety (cybernetics), General Energy, Roadmap, T-DAS, Lithium, 0210 nano-technology, Battery (electricity), energy materials, Energy & Fuels, HIGH-CAPACITY ANODE, batteries, Materials Science (miscellaneous), Materials Science, chemistry.chemical_element, Materials Science, Multidisciplinary, electrolytes, 010402 general chemistry, Energy storage, MECHANISTIC INSIGHTS, SDG 7 - Affordable and Clean Energy, STRUCTURAL EVOLUTION, SOLID-ELECTROLYTE INTERPHASE, Science & Technology, QD Chemistry, 0104 chemical sciences, chemistry, 13. Climate action, Sustainability, HIGH-PERFORMANCE CATHODE, Biochemical engineering, cathodes
Abstract

Tapia-Ruiz, Nuria et al., Increasing concerns regarding the sustainability of lithium sources, due to their limited availability and consequent expected price increase, have raised awareness of the importance of developing alternative energy-storage candidates that can sustain the ever-growing energy demand. Furthermore, limitations on the availability of the transition metals used in the manufacturing of cathode materials, together with questionable mining practices, are driving development towards more sustainable elements. Given the uniformly high abundance and cost-effectiveness of sodium, as well as its very suitable redox potential (close to that of lithium), sodium-ion battery technology offers tremendous potential to be a counterpart to lithium-ion batteries (LIBs) in different application scenarios, such as stationary energy storage and low-cost vehicles. This potential is reflected by the major investments that are being made by industry in a wide variety of markets and in diverse material combinations. Despite the associated advantages of being a drop-in replacement for LIBs, there are remarkable differences in the physicochemical properties between sodium and lithium that give rise to different behaviours, for example, different coordination preferences in compounds, desolvation energies, or solubility of the solid–electrolyte interphase inorganic salt components. This demands a more detailed study of the underlying physical and chemical processes occurring in sodium-ion batteries and allows great scope for groundbreaking advances in the field, from lab-scale to scale-up. This roadmap provides an extensive review by experts in academia and industry of the current state of the art in 2021 and the different research directions and strategies currently underway to improve the performance of sodium-ion batteries. The aim is to provide an opinion with respect to the current challenges and opportunities, from the fundamental properties to the practical applications of this technology., The authors gratefully acknowledge RS2E and Alistore-ERI for funding their research into Na-ion batteries. The funding received from the European Union’s Horizon 2020 research and innovation programme under Grant Agreement No. 646433 (NAIADES), the Swedish Research Council, the Swedish Energy Agency (#37671-1), and the Swedish Research Council for Environment, Agricultural Sciences and Spatial Planning (FORMAS), are all gratefully acknowledged. The many fruitful discussions within ALISTORE-ERI, and especially with M Rosa Palacín, have been most valuable. P J is also grateful for the continuous support from several of the Chalmers Areas of Advance: Materials Science and Energy. Funding from the European Union’s innovation program H2020 is acknowledged: H2020-MSCA-COFUND-2016 (DOC-FAM, Grant Agreement No. 754397). A Ponrouch is grateful to the Spanish Ministry for Economy, Industry and Competitiveness Severo Ochoa Programme for Centres of Excellence in R&D (SEV-2015-0496).

Published
2021

3. A facile and sustainable one-pot approach to the aqueous and low-temperature PET-to-UiO-66(Zr) upcycling.

Author

Ribadeneyra MC, King J, Titirici MM, and Szilágyi PÁ

Abstract

Accelerating waste management requires the conversion of polymer waste to value-added materials through sustainable approaches. While depolymerised PET has been used as feedstock to produce metal-organic frameworks, this is the first report of the successful one-pot hydrothermal synthesis of the desirable UiO-66 topology through the judicious choice of reactants, modulators and reaction conditions.

Published
2022
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4. High-Density Lignin-Derived Carbon Nanofiber Supercapacitors with Enhanced Volumetric Energy Density.

Author

Hérou S, Bailey JJ, Kok M, Schlee P, Jervis R, Brett DJL, Shearing PR, Ribadeneyra MC, and Titirici M

Abstract

Supercapacitors are increasingly used in short-distance electric transportation due to their long lifetime (≈15 years) and fast charging capability (>10 A g -1 ). To improve their market penetration, while minimizing onboard weight and maximizing space-efficiency, materials costs must be reduced (<10 $ kg -1 ) and the volumetric energy-density increased (>8 Wh L -1 ). Carbon nanofibers display good gravimetric capacitance, yet their marketability is hindered by their low density (0.05-0.1 g cm -3 ). Here, the authors increase the packing density of low-cost, free-standing carbon nanofiber mats (from 0.1 to 0.6 g cm -3 ) through uniaxial compression. X-ray computed tomography reveals that densification occurs by reducing the inter-fiber pore size (from 1-5 µm to 0.2-0.5 µm), which are not involved in double-layer capacitance. The improved packing density is directly proportional to the volumetric performances of the device, which reaches a volumetric capacitance of 130 F cm -3 and energy density of 6 Wh L -1 at 0.1 A g -1 using a loading of 3 mg cm -2 . The results outperform most commercial and lab-scale porous carbons synthesized from bioresources (50-100 F cm -3 , 1-3 Wh L -1 using 10 mg cm -2 ) and contribute to the scalable design of sustainable electrodes with minimal 'dead volume' for efficient supercapacitors., (© 2021 The Authors. Advanced Science published by Wiley-VCH GmbH.)

Published
2021
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5. Core-independent approach for polymer brush-functionalised nanomaterials with a fluorescent tag for RNA delivery.

Author

Li D, Wu L, Qu F, Ribadeneyra MC, Tu G, and Gautrot J

Subjects
Cell Line, Tumor, Cell Survival drug effects, Drug Carriers chemistry, Humans, Particle Size, Polyelectrolytes chemistry, Polymers pharmacology, Fluorescence, Nanostructures chemistry, Polymers chemistry, RNA administration & dosage
Abstract

Here we describe a core-independent approach enabling the grafting of polymer brushes from the surface of nanomaterials and microparticles for oligonucleotide delivery. This method is based on the adsorption of a polyelectrolyte macroinitiator (MI) combined with a fluorescent conjugated polymer for efficient and stable labelling. This allows dense brushes to be generated, with growth kinetics comparable to those observed from mono-functional initiators, for the imaging of nanomaterial cellular localisation and uptake. We also study the impact of brush chemistry on interactions with cell membranes and on transfection efficiency. The method we report offers a unique freedom of design of the core size and shape as well as surface chemistry, whilst enabling tagging, for the study of transfection processes or theragnostic applications.

Published
2019
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