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For this paper, studies of the microstructure as well as the mechanical and biological properties of bioinert titanium, zirconium, and niobium alloys in their nanostructured (NS) and ultrafine-grained (UFG) states have been completed. The NS and UFG states were formed by a combined two-step method of severe plastic deformation (SPD), first with multidirectional forging (MDF) or pressing into a symmetrical channel (PSC) at a given temperature regime, and then subsequent multi-pass groove rolling (MPGR) at room temperature, with pre-recrystallization annealing. Annealing increased the plasticity of the alloys in the NS and UFG states without changing the grain size. The UFG structure, with an average size of structural elements of no more than 0.3 μm, was formed as a result of applying two-step SPD and annealing. This structure presented significant improvement in the mechanical characteristics of the alloys, in comparison with the alloys in the coarse-grained (CG) or small-grained (SG) states. At the same time, although the formation of the UFG structure leads to a significant increase in the yield strength and tensile strength of the alloys, their elastic modulus did not change. In terms of biocompatibility, the cultivation of MG-63 osteosarcoma cells on the polished and sandblasted substrates demonstrated high cell viability after 10 days and good cell adhesion to the surface. more...

Bioinert metals are used for medical implants and in some industrial applications. This study was performed to detect and analyze peculiarities that appear in the temperature distributions during quasi-static tensile testing of bioinert alloys. These alloys include VT1-0 titanium, Zr-1%Nb and Ti-45%Nb in both coarse-grain (CG) and ultrafine-grain (UFG) states. The crystal structure, as well as the crystal domain and grain sizes of these alloys in the UFG state, may be different from the CG versions and identifying the thermal signatures that occur during their deformation and fracture is of interest, as it may lead to an understanding of physical processes that occur during loading. By comparing the surface temperature distributions of specimens undergoing deformation under tensile loading to the distributions at maximum temperatures it was found that the observed differences depend on the alloy type, the alloy structural state and the thermal properties of structural defects in the specimen. Macro-defects were found in some specimens of VT1-0 titanium, Zr-1Nb and Ti-45Nb alloys in both the CG and UFG states. The average tensile strength of specimens containing defects was lower than that of specimens with no defects. Infrared thermography documents change in the thermal patterns of specimens as they are deformed under tensile loading and when the load stops changing or the specimen breaks. more...