Search

Abstract This study aims to enhance the tribological properties of automotive applications by examining the effects of TiC content on the microstructure, mechanical properties, and wear behavior. This study investigates the production of Al–TiC composite strips using a novel multi-step densification process combining mechanical alloying and hot rolling with TiC concentrations ranging from 0 to 12 vol%. The novelty of this work lies in its comprehensive approach to developing and analyzing Al–TiC composite strips using a multistep densification method. This study integrates microstructural analysis, mechanical property evaluation, and detailed tribological behavior assessment under different wear loads (5–25 N). A key innovation is the application of the Abbott Firestone method to analyze worn surfaces, providing insights into optimal wear conditions. The study reveals that increasing the TiC content to 12 vol% significantly improves densification, hardness (up to 268.8% increase), and wear resistance (up to 95% improvement at a 5N load). Dry ball-on-flat sliding wear tests at loads of 5–25N demonstrate that TiC particles hindered complete delamination wear in the composite strips. The Abbott Firestone method analysis of worn surfaces indicated an optimal exploitation zone in the Al-6 vol% TiC composite at both low and high wear loads. This comprehensive approach provides valuable insights into optimizing Al–TiC composites for enhanced performance in automotive components that require improved wear resistance.

Abstract Owing to their exceptional mechanical properties, the various welding wires used to combine aluminum can meet the needs of many engineering applications that call for components with both good mechanical and lightweight capabilities. This study aims to produce high-quality welds made of AA7075 aluminum alloy using the GTAW technique and various welding wires, such as ER5356, ER4043, and ER4047. The microstructure, macrohardness, and other mechanical characteristics, such as tensile strength and impact toughness, were analyzed experimentally. To check the fracture surface of the AA7075 welded joints, the specimens were examined using optical and scanning electron microscopy (SEM). A close examination of the samples that were welded with ER5356 welding wire revealed a fine grain in the weld zone (WZ). In addition, the WZ of the ER4043 and ER4047 welded samples had a coarse grain structure. Because the hardness values of the welded samples were lower in the WZ than in the base metal (BM) and heat-affected zone (HAZ), the joints filled with ER5356 welding wire provided the highest hardness values compared to other filler metals. Additionally, the ER4047 filler metal yielded the lowest hardness in the weld zone. The welding wire of ER5356 produced the greatest results for ultimate tensile stress, yield stress, welding efficiency, and strain-hardening capacity (Hc), whereas the filler metal of ER4043 produced the highest percentage of elongation. In addition, the ER4047 fracture surface morphology revealed coarser and deeper dimples than the ER5356 fine dimples in the welded joints. Finally, the highest impact toughness was obtained at joints filled with the ER4047 filler metal, whereas the lowest impact toughness was obtained at the BM.

Abstract Post-weld heat treatment (PWHT) and solid-state thermomechanical treatment (TMT) via friction stir processing (FSP) have been shown to enhance the mechanical properties of aluminum alloys. The current work investigates the effects of PWHT and TMT on the microstructure and mechanical performance of AA6082-T6 welded butt joints welded using the MIG process. The 5 mm thick AA 6082-T6 plates were joined in butt configuration using MIG welding with ER 5356 filler wire, 120 A current, 0.3 mm/s weld speed, and argon shielding gas at 15 L/min flow rate. PWHT was performed on the MIG welds per the T6 temper procedure. TMT was implemented via FSP using a pinless tool rotating at 800 rpm and traversing speed at 200 mm/min with a 3° tilt angle. Microstructural analysis, hardness mapping, tensile testing, and fracture surface evaluation were utilized to characterize the as-welded, PWHT, and TMT samples. The results demonstrate that both PWHT and TMT significantly refine and homogenize the microstructures of the welded joints. However, the TMT samples displayed superior hardness and tensile strength compared to the as-welded and PWHT conditions. The TMT-processed welds achieved approximately 99% joint efficiency versus only 69% and 85% for the as-welded and PWHT samples. In summary, PWHT and especially TMT via FSP are effective at enhancing the mechanical properties of MIG welded AA6082-T6.

This article discusses the correlation between the microstructural and mechanical changes in the dual-matrix Al-Ni/SiC composites processed by Accumulative Roll Bonding (ARB) technique. Three different SiC concentrations, 1, 3, and 5% were considered to reinforce Al and Al-Ni dual-matrix composites. ARB process was applied up to 7 cycles to manufacture a composite with homogenous dispersion of the three phases. The results showed that the presence of Ni layer between Al and SiC particles enhanced the dispersion of SiC in the matrix, which positively affect the mechanical strength. The maximum tensile achieved was 257 MPa for composite containing 3 % SiC after 7 ARB cycles compared to 37.2 MPa for the AA1050. Increasing SiC content reduces the adhesion between Al and Ni layers, which reduces the elasticity of the composites. However, for the composites with 5% SiC, after 3 ARB cycles, the strength was reduced due to the cracking of the Ni layer caused by the stress concentration around the SiC particles. The hardness values of the ARBed AA1050, AA1050-Ni, and AA1050-Ni/5 wt% SiC are 85.5, 93.5, and 109.7, respectively, after 7 ARB cycles. In terms of strength, the samples with 3% SiC content showed the optimum stress enhancement with minimum reduction in the elongation, which achieve a compromised response for many applications.

This study investigated the effect of a hemispherical friction stir welding (FSW) tool on the heat generation and mechanical properties of dissimilar butt welded AA5083 and AA7075 alloys. FSW was performed on the dissimilar aluminum alloys AA5083-H111 and AA7075-T6 using welding speeds of 25, 50, and 75 mm/min. The tool rotation rate was kept constant at 500 rpm. An analytical model was developed to calculate heat generation and temperature distribution during the FSW process utilizing a hemispherical tool. The experimental results were compared to the calculated data. The latter confirms the accuracy of the analytical model, demonstrating a high degree of agreement. Sound FSW dissimilar joints were achieved at welding speeds of 50 and 25 mm/min. Meanwhile, joints created at a welding speed of 75 mm/min exhibited a tunnel-like defect, which can be attributed to the minimal heat generated at this particular welding speed. At a lower welding speed of 25 mm/min, a higher tensile strength of the dissimilar FSWed joints AA5083 and AA7075 was achieved with a joint efficiency of over 97%.

The aim of this study is to investigate friction stir welding (FSW) to join A304 austenitic stainless steel and low carbon steel A283 Gr. C in-lap configuration to clad the carbon steel with highly corrosion-resistant stainless steel. Thus, a wide range of FSW parameters were investigated such as FSW tool rotation rate from 200 to 400 rpm, tool traverse speed from 25 to 75 mm/min, and vertical forces of 20 to 32 KN. The FSW parameters combination of high welding rotation rate (400 rpm) and high vertical forces (32 KN) results in rejected joints in terms of surface appearance and clear surface defects. On the other hand, rotation rates of 200 and 300 rpm with different welding speeds and vertical forces resulted in some sound joints that were further investigated for microstructure and mechanical properties. The sound lap joints were examined via optical microstructure, SEM, and EDS investigations. For the mechanical properties, both tensile shear testing and hardness testing were used. The transverse macrographs showed intermixing between the two dissimilar materials with an almost irregular interface. The hardness profile in both materials showed a significant increase across the different regions from the Base Material (BM) to the nugget zone, with a maximum value of 260 Hv in the stainless steel and 245 Hv in the carbon steel. This increase is mainly attributed to the grain refining in the weld region due to the dynamic recrystallization and transformations upon the thermomechanical cycle. The tensile shear load of the joints varied from 20 to 27 KN for the FSWed joints, with the highest joint tensile shear load of 27 KN for that produced at 300 rpm tool rotation and 25 mm/min welding speed.

The current work investigates the possibility of fabricating additive manufacturing products in solid-state form, from AA2011-T6 of 40 mm diameter rods as a feedstock, using an additive friction stir deposition (A-FSD) technique. The use of large diameter feedstocks, especially high-strength aluminum alloys (2XXX series), is a challenge, as it necessitates high power and the critical selection of the optimal A-FSD parameters, such as feed rate and spindle rotation speed. The study included applying a wide range of spindle rotation speeds, ranging from 400 to 1200 rpm, at three levels of feeding rates of 1, 3, and 5 mm/min. The AA2011-T6 friction stir deposited parts (FSDPs) were visually evaluated. This was followed by an examination of macrostructures through the thickness of the fabricated specimens. The characterization of microstructures was also carried out using optical microscopy and a scanning electron microscope equipped with advanced EDS analysis. Furthermore, the mechanical properties in terms of hardness and compressive strength of the AA2011-T6 base material (BM) and deposited materials were evaluated. Sound, additively manufactured products were successfully fabricated from 40 mm diameter AA2011-T6 feedstocks using the suggested deposition variables of 600 and 800 rpm spindle speeds and feeding rates of 1, 3, and 5 mm/min. The results indicated that the spindle speed and feeding rate govern the quality of the FSDPs. Furthermore, the axial load during the A-FSD process increased with increasing these parameters. In comparison to the AA2011-T6 BM, the additively deposited materials showed a refined grain structure and uniform dispersion of the fragment precipitates in their continuous multi-layers. The reduction ratio in grain size attains 71.56%, 76%, and 81.31% for the FSDPs processed at 800 rpm spindle speed and feeding rates of 1, 3 and 5 mm/min, respectively, compared to the grain size of BM. The Al2Cu and Al7Cu2Fe intermetallics are detected in the AA2011-T6 BM, and their deposited parts are in different shapes of spherical, almost spherical, irregular, and rod-like shapes. The compressive strength and hardness of the deposited parts increased with increasing spindle speed and feeding speeds. At a spindle speed of 800 rpm and a 5 mm/min feeding rate, the higher hardness and compressive strength gained were 85% and 93%, respectively, from that of the AA2011-T6 feedstock.

Selecting an economically suitable welding technique and optimizing welding parameters to obtain high joint quality is considered a challenge for expanding the 5xxx aluminum alloy series in various industrial applications. This work aims to investigate the effect of applying different welding techniques, tungsten inert gas (TIG) and metal inert gas (MIG), as fusion welding processes compared to friction stir welding (FSW), a solid-state joining process, on the joint performance of the produced 5 mm thick similar AA5083-H111 butt weldments at different welding conditions. Different methods were used to evaluate the quality of the produced joints, including visual inspection, radiographic testing (RT), and macrostructure evaluation, in addition to hardness and tensile tests. The fracture surface of the tensile-failed specimens was also investigated using a scanning electron microscope (SEM). Furthermore, the current study ended with an economic analysis of the welding techniques used. The results showed that, for the friction stir-welded joints, the radiographic films revealed defect-free joints at the two applied travel speeds of 100 mm/min and 400 mm/min and a constant tool rotating speed of 400 rpm. In addition, only one joint was welded by MIG at a welding current of 130 Amp, with a 19 L/min flow rate of pure argon. In contrast, the radiographic films showed internal defects such as lack of fusion (LOF), lack of penetration (LOP), and porosity (P) for the two joints welded by TIG and one joint welded by MIG. The hardness of the welded joints was enhanced over the AA5083-H111 base material (BM) by 24–29, 31–35, and 46–50% for the MIG, TIG, and FSW joints, respectively. The maximum ultimate tensile strength was obtained for the FSW joint welded at a 400 mm/min travel speed. Adopting FSW in shipbuilding applications can further produce the AA5083-H11 joints with higher quality and efficiency than fusion welding techniques such as MIG and TIG processes. In addition, time and cost comparisons between TIG, MIG, and FSW were performed for five-millimeter-thick and one-meter-long AA5083-H111.

The current research designed a statistical model for the bobbin tool friction stir processing (BT-FSP) of AA1050 aluminum alloy using the Response Surface Method (RSM). The analysis studied the influence of tool travel speeds of 100, 200, and 300 mm/min and different pin geometries (triangle, square, and cylindrical) at a constant tool rotation speed (RS) of 600 rpm on processing 8 mm thickness AA1050. The developed mathematical model optimizes the effect of the applied BT-FSP parameters on machine torque, processing zone (PZ) temperature, surface roughness, hardness values, and ultimate tensile strength (UTS). The experimental design is based on the Face Central Composite Design (FCCD), using linear and quadratic polynomial equations to develop the mathematical models. The results show that the proposed model adequately predicts the responses within the processing parameters, and the pin geometry is the most influential parameter during the BT-FSP of AA1050. The analysis of variance exhibit that the developed mathematical models can effectively predict the values of the machine torque, PZ temperature, surface roughness, hardness, and UTS with a confidence level of over 95% for the AA1050 BT-FSP. The optimization process shows that the optimum parameters to attain the highest mechanical properties in terms of hardness and tensile strength at the lowest surface roughness and machine torque are travel speed (TS) of 200 mm/min using cylindrical (Cy) pin geometry at the constant RS of 600 rpm. The PZ temperature of the processed specimens decreased with increasing TS at different pin geometries. Meanwhile, the surface roughness of the processed passes and machine torque increased with increasing the TS at different pin geometries. Increasing TS from 100 to 300 mm/min increases the hardness values of the processed materials using different pin geometries. The highest UTS of 79 MPa for the processed specimens was attained at the TS of 200 mm/min and RS of 600 rpm using the Cy pin geometry.

In this study, AZ91/23 vol.% short carbon fiber composite was produced by a squeeze casting technique using a cylindrical pre-form of treated carbon fibers, in which the fibers are randomly oriented in the horizontal plane. Cylindrical specimens (height = 9 mm and diameter = 6 mm) were machined from the as-cast AZ91 matrix and its composite. The full behavior of the produced composite was studied through the test specimens machined in two directions, namely parallel to the reinforced plane (in the radial direction of the cast cylinder) and normal to the reinforced plane (in the axial direction of the cast composite). The microstructures of the produced composite specimens were investigated using SEM equipped with EDS analysis. Density, hardness, compressive, and wear behavior were also investigated. For comparison, the AZ91 matrix was evaluated as a reference. The microstructure of the produced AZ91 matrix alloy and its composite revealed dense materials without casting defects. Both composite specimens show improvement in hardness, compressive strength, and wear properties over the AZ91 matrix. The compressive and wear properties are more fiber orientation-dependent than the hardness results. The parallel composite specimen depicts the highest compressive properties in terms of yield compressive strength (311 MPa) and ultimate compressive strength (419 MPa), compared to that shown by the AZ91 matrix and the normal composite specimen. This improvement in compressive strength was at the expense of ductility. The parallel composite specimen shows the lowest ductility (R = 3.8%), compared to that given by the normal composite specimen (R = 7.1) and the AZ91 matrix alloy (R = 13.6). The wear testing results showed that at the highest wear load of 5 N, the material weight loss of the parallel composite specimen decreases by 44% and 64% compared to the AZ91 matrix and the normal composite specimen, respectively.

Light-weight metal matrix composites, especially magnesium-based composites, have recently become more widespread for high-efficiency applications, including aerospace, automobile, defense, and telecommunication industries. The squeeze cast AZ91 base material (AZ91-BM) and its composites having 23 vol.% short carbon fibers were fabricated and investigated. The composite specimens were machined normal to the reinforced plane (Composite-N) and parallel to the reinforced plane (Composite-P). All the as-casted materials were subjected to different tests, such as hardness, compression, and wear testing, evaluating the mechanical properties. Dry wear tests were performed using a pin-on-disk machine at room temperature under different applied wear loads (1–5 N) and different sliding distances (0.4461×104–3.12×104 m). The microstructures and worn surfaces of the fabricated AZ91-BM and the two composite specimens were investigated using a scanning electron microscope (SEM) equipped with an energy dispersive spectroscopy (EDS) advanced analysis system. The wear debris was collected and investigated also under the SEM. The results showed significant improvement in hardness, compressive strength, and wear resistance of the composite specimens (Composite-N and Composite-P) over the AZ91-BM. The compressive strength and wear resistance are more fibers orientation sensitive than the hardness results. When the fiber orientation is parallel to the sliding direction (Composite-N), the weight loss is somewhat lower than that of the fiber orientation perpendicular to the sliding direction (Composite-P) at a constant wear load of 2 N and the sliding distances of 0.4461×104, 1.34×104 , and 2.23×104 m. In contrast, the weight loss of Composite-P is lower than Composite-N, especially at the highest sliding distance of 3.12×104 m due to the continuous feeding of graphite lubricant film and the higher compressive strength. Plastic deformation, oxidation, and abrasive wear are the dominant wear mechanisms of AZ91-BM; in contrast, abrasive and delamination wear are mainly the wear mechanisms of the two composites under the applied testing conditions.

This work aims to optimize the performance evaluation characteristics such as the temperature at the weld center of the lap joint (Tw), the tensile shear load (TSL), and the hardness using an experimental design experiment for bobbin tool friction stir welding (BT-FSW) of AA1050 lap joints. BT-FSW is characterized by a fully penetrated pin and double-sided shoulder that promote symmetrical solid-state welds. This study contributes to improving the quality of 10 mm thick lap joints and addressing challenges to obtaining a sound weld deprived of any defects. Taguchi L9 orthogonal array (OA) experimental design was performed. Three different pin shapes (cylindrical, triangular, and square) and three levels of welding travel speeds of 200, 400, and 600 mm/min were selected as input controllable process parameters at a constant tool rotation speed of 600 rpm. A travel speed of 200 mm/min with square pin geometry significantly improves the TSL of the joint up to 6491 N. However, the hardness characteristic is optimized by using 600 mm/min travel speed and a cylindrical tool pin. The minimum temperature in the weld joint can be obtained using 600 mm/min or more with triangular pin geometry. From ANOVA results, it was seen that the BT-FSW of AA 1050 thick lap joints performance in terms of TLS and Tw were greatly influenced by travel speed; however, the tool shape influences the hardness more. For the validation of the models, BT-FSW experiments have been carried out for AA1050 using the applied processing parameters. Furthermore, regression models were developed to predict the Tw, TSL, and hardness. The calculated performance properties from the mathematical models were in an acceptable range compared to the measured experimental values.

In the current work, mild steel used in shipbuilding applications was friction-stir-welded (FSWed) with the aim of investigating the microstructure and mechanical properties of the FSWed joints. Mild steel of 5 mm thickness was friction-stir-welded at a constant tool rotation rate of 500 rpm and two different welding speeds of 20 mm/min and 50 mm/min and 3° tool tilt angle. The microstructure of the joints was investigated using optical and scanning electron microscopes. Additionally, the grain structure and crystallographic texture of the nugget (NG) zone of the FSWed joints was investigated using electron backscattering diffraction (EBSD). Furthermore, the mechanical properties were investigated using both tensile testing and hardness testing. The microstructure of the low-welding-speed joint was found to consist of fine-grain ferrite and bainite (acicular ferrite) with an average grain size of 3 µm, which indicates that the temperature experienced above A1, where a ferrite and austenite mixture is formed, and upon cooling, the austenite transformed into bainite. The joint produced using high welding speed resulted in a microstructure consisting mainly of polygonal ferrite and pearlite. This could be due to the temperature far below A1 experienced during FSW. In terms of joint efficiency expressed in terms of relative ultimate tensile, the stress of the joint to the base material was found to be around 92% for the low-speed joint and 83% for the high-welding-speed joint. A reduction in welding was attributed to the microstructure, as well as the microtunnel defect formed near the advancing side of the joint. The tensile strain was preserved at 18% for low welding speed and increased to 24% for the high welding speed. This can be attributed to the NG zone microstructural constituents. In terms of crystallographic texture, it is dominated by a simple shear texture, with increased intensity achieved by increasing the welding speed. In both joints, the hardness was found to be significantly increased in the NG zone of the joints, with a greater increase in the case of the low-welding-speed joint. This hardness increase is mainly attributed to the fine-grained structure formed after FSW.

The current work investigates the viability of utilizing a friction stir deposition (FSD) technique to fabricate continuous multilayer high-performance, metal-based nanoceramic composites. For this purpose, AA2011/nano Al2O3 composites were successfully produced using AA2011 as a matrix in two temper conditions (i.e., AA2011-T6 and AA2011-O). The deposition of matrices without nano Al2O3 addition was also friction stir deposited for comparison purposes. The deposition process parameters were an 800 rpm rod rotation speed and a 5 mm/min feed rate. Relative density and mechanical properties (i.e., hardness, compressive strength, and wear resistance) were evaluated on the base materials, deposited matrices, and produced composites. The microstructural features of the base materials and the friction stir deposited materials were investigated using an optical microscope (OM) and a scanning electron microscope (SEM) equipped with an EDS analysis system. The worn surface was also examined using SEM. The suggested technique with the applied parameters succeeded in producing defect-free deposited continuous multilayer AA2011-T6/nano Al2O3 and AA2011-O/nano Al2O3 composites, revealing well-bonded layers, grain refined microstructures, and homogeneously distributed Al2O3 particles. The deposited composites showed higher hardness, compressive strengths, and wear resistance than the deposited AA2011 matrices at the two temper conditions. Using the AA2011-T6 temper condition as a matrix, the produced composite showed the highest wear resistance among all the deposited and base materials.

In the current study, a 2 mm thick low-carbon steel sheet (A283M—Grade C) was joined with a brass sheet (CuZn40) of 1 mm thickness using friction stir spot welding (FSSW). Different welding parameters including rotational speeds of 1000, 1250, and 1500 rpm, and dwell times of 5, 10, 20, and 30 s were applied to explore the effective range of parameters to have FSSW joints with high load-carrying capacity. The joint quality of the friction stir spot-welded (FSSWed) dissimilar materials was evaluated via visual examination, tensile lap shear test, hardness test, and macro- and microstructural investigation using SEM. Moreover, EDS analysis was applied to examine the mixing at the interfaces of the dissimilar materials. Heat input calculation for the FSSW of steel–brass was found to be linearly proportional with the number of revolutions per spot joint, with maximum heat input obtained of 11 kJ at the number of revolutions of 500. The temperature measurement during FSSW showed agreement with the heat input dependence on the number of revolution. However, at the same revolutions of 500, it was found that the higher rotation speed of 1500 rpm resulted in higher temperature of 583 °C compared to 535 °C at rotation speed of 1000 rpm. This implies the significant effect for the rotation speed in the increase of temperature. The macro investigations of the friction stir spot-welded joints transverse sections showed sound joints at the different investigated parameters with significant joint ligament between the steel and brass. FSSW of steel/brass joints with a number of revolutions ranging between 250 to 500 revolutions per spot at appropriate tool speed range (1000–1500 rpm) produces joints with high load-carrying capacity from 4 kN to 7.5 kN. The hardness showed an increase in the carbon steel (lower sheet) with maximum of 248 HV and an increase of brass hardness at mixed interface between brass and steel with significant reduction in the stir zone hardness. Microstructural investigation of the joint zone showed mechanical mixing between steel and brass with the steel extruded from the lower sheet into the upper brass sheet.

Friction stir welding (FSW) as a solid-state process is an excellent candidate for high softening temperature materials welding; however, extending the tool life is required to make the process cost-effective. This work investigates the use of a high pin to shoulder ratio (65%) tungsten carbide (WC) tool for friction stir welding of 5 mm thick 2205 DSS to extend the tool life of this low-cost tool material. In addition, the effect of FSW parameters in terms of rotational rates, travel speeds, and downward forces on the microstructural features and mechanical properties of the welded joints were investigated. Characterization in terms of visual inspection, macro and microstructures, hardness, and tensile testing was conducted. The obtained results indicated that the combined rotational rate, travel speed, and downward force parameters govern the production of defect-free joints. The 2205 DSS friction stir welds show an enhancement in hardness compared to the base material. The stir zone showed a significantly refined grain structure of ferrite and austenite with the reduction in the average grain size from 8.8 µm and 13.3 µm for the base material to 2.71 µm and 2.24 µm, respectively. Moreover, this joint showed higher yield strength and ultimate tensile strength compared to the DSS as-received material.

In the current investigation, additive friction stir-deposition (AFS-D) of as-cast hypoeutectic A356 Al alloy was conducted. The effect of feeding speeds of 3, 4, and 5 mm/min at a constant rotational speed of 1200 rpm on the macrostructure, microstructure, and hardness of the additive manufacturing parts (AMPs) was investigated. Various techniques (OM, SEM, and XRD) were used to evaluate grain microstructure, presence phases, and intermetallics for the as-cast material and the AMPs. The results showed that the friction stir deposition technique successfully produced sound additive manufactured parts at all the applied feeding speeds. The friction stir deposition process significantly improved the microstructure of the as-cast alloy by eliminating porosity and refining the dendritic α-Al grains, eutectic Si phase, and the primary Si plates in addition to intermetallic fragmentation. The mean values of the grain size of the produced AMPs at the feeding speeds of 3, 4, and 5 mm/min were 0.62 ± 0.1, 1.54 ± 0.2, and 2.40 ± 0.15 µm, respectively, compared to the grain size value of 30.85 ± 2 for the as-cast alloy. The AMPs exhibited higher hardness values than the as-cast A356 alloy. The as-cast A356 alloy showed highly scattered hardness values between 55 and 75.8 VHN. The AMP fabricated at a 3 mm/min feeding speed exhibited the maximum hardness values between 88 and 98.1 VHN.

In the current study, solid-state additive manufacturing (SSAM) of two temper conditions AA2011 was successfully conducted using the friction stir deposition (FSD) process. The AA2011-T6 and AA2011-O consumable bars of 20 mm diameter were used as a feeding material against AA5083 substrate. The effect of the rotation rate and feeding speed of the consumable bars on the macrostructure, microstructure, and hardness of the friction stir deposited (FSD) materials were examined. The AA2011-T6 bars were deposited at a constant rotation rate of 1200 rpm and different feeding speeds of 3, 6, and 9 mm/min, whereas the AA2011-O bars were deposited at a constant rotation rate of 200 mm/min and varied feeding speeds of 1, 2, and 3 mm/min. The obtained microstructure was investigated using an optical microscope and scanning electron microscope equipped with EDS analysis to evaluate microstructural features. Hardness was also assessed as average values and maps. The results showed that this new technique succeeded in producing sound additive manufactured parts at all the applied processing parameters. The microstructures of the additive manufactured parts showed equiaxed refined grains compared to the coarse grain of the starting materials. The detected intermetallics in AA2011 alloy are mainly Al2Cu and Al7Cu2Fe. The improvement in hardness of AA2011-O AMPs reached 163% of the starting material hardness at the applied feeding speed of 1 mm/min. The hardness mapping analysis reveals a homogeneous hardness profile along the building direction. Finally, it can be said that the temper conditions of the starting AA2011 materials govern the selection of the processing parameters in terms of rotation rate and feeding speed and affects the properties of the produced additive manufactured parts in terms of hardness and microstructural features.

Bobbin tool friction stir welding (BT-FSW) is characterized by a fully penetrated pin and double-sided shoulder that promote symmetrical solid-state joints. However, control of the processing parameters to obtain defect-free thick lap joints is still difficult and needs more effort. In this study, the BT-FSW process was used to produce 10 mm AA1050-H14 similar lap joints. A newly designed bobbin tool (BT) with three different pin geometries (cylindrical, square, and triangular) and concave shoulders profile was designed, manufactured, and applied to produce the Al alloy lap joints. The experiments were carried out at a constant tool rotation speed of 600 rpm and a wide range of various welding travel speeds of 200, 400, 600, 800, and 1000 mm/min. The generated temperature during the BT-FSW process was recorded and analyzed at the joints’ center line, and at both advancing and retreating sides. Visual inspection, macrostructures, hardness, and tensile properties were investigated. The fracture surfaces after tensile testing were also examined. The results showed that the pin geometry and travel speed are considered the most important controlling parameters in BT-FSW thick lap joints. The square (Sq) pin geometry gives the highest BT-FSW stir zone temperature compared to the other two pins, cylindrical (Cy) and triangular (Tr), whereas the Tr pin gives the lowest stir zone temperature at all applied travel speeds from 200 to 1000 mm/min. Furthermore, the temperature along the lap joints decreased with increasing the welding speed, and the maximum temperature of 380 °C was obtained at the lowest travel speed of 200 mm/min with applying Sq pin geometry. The temperature at the advancing side (AS) was higher than that at the retreating side (RS) by around 20 °C. Defect-free welds were produced using a bobbin tool with Cy and Sq pin geometries at all the travel welding speeds investigated. BT-FSW at a travel speed of 200 mm/min leads to the highest tensile shear properties, in the case of using the Sq pin. The hardness profiles showed a significant effect for both the tool pin geometry and the welding speed, whereas the width of the softened region is reduced dramatically with increasing the welding speed and using the triangular pin.

In this work, three mathematical models for the heat generation during bobbin tool friction stir welding (BT-FSW) of aluminum using three tool pin geometries have been proposed. The models have utilized and updated the available models for the heat generation during the conventional tool friction stir welding (CT-FSW). For the validation of the models, BT-FSW experiments have been carried out for aluminum alloy AA1050 using three different pin geometries (cylindrical, square, and triangular), at different welding speeds of 200, 400, 600, 800, and 1000 mm/min and a constant tool rotation speed of 600 rpm. The welding temperatures during BT-FSW have been measured to be compared with that calculated from the models at the same parameters. It has been found that the calculated welding temperatures from the models and that measured during BT-FSW are in good agreement at all the investigated welding speeds especially in case of the square and cylindrical pins, proving the validity of the developed models for the predication of the heat generation as well as the welding temperatures. This will allow proper designing of the BT-FSW parameters and avoiding the conditions that can deteriorate the joint quality and properties.

Equal Channel Angular Pressing (ECAP) is a promising severe plastic deformation technique that has gained significant attention for its ability to refine grain structure and enhance mechanical properties in metallic materials. This study focuses on investigating the impact of ECAP with route A and up to three passes on the mechanical properties and microstructure of 1050 aluminum. The study yielded compelling evidence of substantial enhancements in yield strength, ultimate tensile strength, and hardness. Specifically, these properties increased from 58.19 MPa, 67.06 MPa, and 23.85 HV in the annealed state to 133.02 MPa,141.21 MPa, and 38.96 HV after the third pass of the ECAP process, respectively. Furthermore, an interesting observation was made regarding the hardness ratio, which demonstrated a noticeable decrease with an increasing number of ECAP passes. This phenomenon correlated with a reduction in the size of dimples on the fracture surface. Microstructural analysis via scanning electron microscopy SEM confirms a significant reduction in grain size after ECAP passes, indicating the effectiveness of the process in inducing microstructural refinement. These findings collectively underscore the potential of ECAP with route A in enhancing the mechanical properties and microstructure of 1050 aluminum. This research contributes valuable insights into the application of ECAP with route A as a viable strategy for improving the performance of aluminum alloys.