9 results on '"Min Jung Chae"'
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2. A Study on the Environment-friendly Design Elements in Apartment Housing - Based on the 7 Brand Apartment
- Author
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Parkhyunok and Min-Jung Chae
- Subjects
Engineering ,Architectural engineering ,Apartment ,business.industry ,Design elements and principles ,business ,Environmentally friendly - Published
- 2011
- Full Text
- View/download PDF
3. A study on the characteristics of female shoes in 2000's
- Author
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Jin-Mee Chae, Min-Jung Chae, and Kyo-Jong Koo
- Subjects
body regions ,musculoskeletal diseases ,Engineering ,Artificial materials ,Natural materials ,business.industry ,technology, industry, and agriculture ,otorhinolaryngologic diseases ,business ,Pastel (color) ,Visual arts - Abstract
The purpose of this thesis is to conduct a thorough research on shoes of 2000s, understand the changes and analyze the differences and the characteristics of the shoe designs of the past and present in order to predict and indicate the future direction of the women shoe designs. The shoes of the millennium not only kept the old fashioned shapes but also showed futuristic shapes. With the increasing importance of shoes in fashion, shoes with various images were created. As far as the materials are concerned, natural materials and artificial materials were both used. The colors were vivid and the futuristic colors. On the other hand, pastel toned colors and romantic colors were used in many different designs and shapes regardlees of the seasons. Straps and hills differed from the oldies. Heavy decorations were added to strap shoes to form a whole new design and hills show geometrical platforms or the avantgarde like heights. Feminine images overwhelmed the shoe designs of the millennium. To elaborate, Pumps displayed feminine images the most for it showed a high frequency number regardless of the seasons. Shoes are presented in aesthetical perspective rather then functional or practical perspectives that are based on human nature. Cultural, social, environmental and some part religious factors had a great influence on the evolution on the shoes. Especially in the 2000s, future oriented concepts were implemented on shoe designs, resulting a wider range of expressiveness and in the end leading to a more creative shoe designing. Changes in shoe designs could be pointed out in many ways according to the shapes materials, colors, modeling of decorations or also with the diverting trends.
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- 2008
- Full Text
- View/download PDF
4. A novel one-pot synthesis of secondary alcohols from esters
- Author
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Duk Keun An, Min Jung Chae, Jae Kyo Park, and Ah Ram Jeon
- Subjects
chemistry.chemical_classification ,organic chemicals ,Carboxylic acid ,Organic Chemistry ,One-pot synthesis ,Alcohol ,Grignard reagent ,Alkylation ,Biochemistry ,chemistry.chemical_compound ,chemistry ,One pot reaction ,Reagent ,Yield (chemistry) ,Drug Discovery ,Organic chemistry - Abstract
Alkylation or vinylation by using organometallic reagents after partial reduction of carboxylic esters with LDBBA gave secondary alcohols, also involving allyl alcohols, without any isolation of intermediates in good yield (54–78%).
- Published
- 2011
- Full Text
- View/download PDF
5. Searches for Large-Scale Anisotropy in the Arrival Directions of Cosmic Rays Detected above Energy of $10^{19}$ eV at the Pierre Auger Observatory and the Telescope Array
- Author
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Telescope, Array, Pierre Auger Collaborations (Alexander Aab, Pedro, Abreu, Marco, Aglietta, Eun Joo Ahn, Imen Al Samarai, Ivone, Albuquerque, Ingomar, Allekotte, Jeff, Allen, Patrick, Allison, Alejandro, Almela, Jesus Alvarez Castillo, Jaime Alvarez Muñiz, Rafael Alves Batista, Michelangelo, Ambrosio, Amin, Aminaei, Luis, Anchordoqui, Sofia, Andringa, Carla, Aramo, Victor Manuel Aranda, Fernando, Arqueros, Hernán Gonzalo Asorey, Pedro, Assis, Julien, Aublin, Maximo, Ave, Michel, Avenier, Gualberto, Avila, Nafiun, Awal, Alina Mihaela Badescu, Barber, Kerri B., Julia, Bäuml, Colin, Baus, Jim, Beatty, Karl Heinz Becker, Bellido, Jose A., Corinne, Berat, Mario Edoardo Bertania, Xavier, Bertou, Peter, Biermann, Pierre, Billoir, Blaess, Simon G., Miguel, Blanco, Carla, Bleve, Hans, Blümer, Martina, Boháčová, Denise, Boncioli, Carla, Bonifazi, Raffaella, Bonino, Nataliia, Borodai, Jeffrey, Brack, Iliana, Brancus, Ariel, Bridgeman, Pedro, Brogueira, Brown, William C., Peter, Buchholz, Antonio, Bueno, Stijn, Buitink, Buscemi, Mario, Caballero Mora, Karen S., Barbara, Caccianiga, Lorenzo, Caccianiga, Marina, Candusso, Laurentiu, Caramete, Caruso, Rossella, Antonella, Castellina, Gabriella, Cataldi, Lorenzo, Cazon, Rosanna, Cester, Chavez, Alan G., Andrea, Chiavassa, Jose Augusto Chinellato, Jiri, Chudoba, Marco, Cilmo, Clay, Roger W., Giuseppe, Cocciolo, Roberta, Colalillo, Alan, Coleman, Laura, Collica, Maria Rita Coluccia, Ruben, Conceição, Fernando, Contreras, Cooper, Mathew J., Alain, Cordier, Stephane, Coutu, Corbin, Covault, James, Cronin, Alex, Curutiu, Richard, Dallier, Bruno, Daniel, Sergio, Dasso, Kai, Daumiller, Dawson, Bruce R., de Almeida, Rogerio M., Manlio De Domenico, de Jong, Sijbrand J., Joao de Mello Neto, Ivan De Mitri, Jaime de Oliveira, Vitor de Souza, Luis del Peral, Olivier, Deligny, Hans, Dembinski, Niraj, Dhital, Claudio Di Giulio, Armando Di Matteo, Johana Chirinos Diaz, Mary Lucia Díaz Castro, Francisco, Diogo, Carola, Dobrigkeit, Wendy, Docters, Juan Carlos D'Olivo, Alexei, Dorofeev, Qader Dorosti Hasankiadeh, Maria Teresa Dova, Jan, Ebr, Ralph, Engel, Martin, Erdmann, Mona, Erfani, Escobar, Carlos O., Joao, Espadanal, Alberto, Etchegoyen, Pedro Facal San Luis, Heino, Falcke, Fang, Ke, Glennys, Farrar, Anderson, Fauth, Norberto, Fazzini, Ferguson, Andrew P., Mateus, Fernandes, Brian, Fick, Juan Manuel Figueira, Alberto, Filevich, Andrej, Filipčič, Brendan, Fox, Octavian, Fratu, Uwe, Fröhlich, Benjamin, Fuchs, Toshihiro, Fujii, Romain, Gaior, Beatriz, García, Sayri Tupac Garcia Roca, Diego Garcia Gamez, Diego Garcia Pinto, Gianpaolo, Garilli, Alberto Gascon Bravo, Florian, Gate, Hartmut, Gemmeke, Piera Luisa Ghia, Ugo, Giaccari, Marco, Giammarchi, Maria, Giller, Christian, Glaser, Henry, Glass, Mariano Gómez Berisso, Gómez Vitale, Primo F., Patrícia, Gonçalves, Gonzalez, Javier G., Nicolás, González, Ben, Gookin, Jacob, Gordon, Alessio, Gorgi, Peter, Gorham, Philippe, Gouffon, Stefan, Grebe, Nathan, Griffith, Aurelio, Grillo, Grubb, Trent D., Fausto, Guarino, Germano, Guedes, Matías Rolf Hampel, Patricia, Hansen, Diego, Harari, Harrison, Thomas A., Sebastian, Hartmann, John, Harton, Andreas, Haungs, Thomas, Hebbeker, Dieter, Heck, Philipp, Heimann, Herve, Alexander E., Hill, Gary C., Carlos, Hojvat, Nicholas, Hollon, Ewa, Holt, Piotr, Homola, Jörg, Hörandel, Pavel, Horvath, Miroslav, Hrabovský, Daniel, Huber, Tim, Huege, Antonio, Insolia, Paula Gina Isar, Ingolf, Jandt, Stefan, Jansen, Cecilia, Jarne, Mariela, Josebachuili, Alex, Kääpä, Olga, Kambeitz, Karl Heinz Kampert, Peter, Kasper, Igor, Katkov, Balazs, Kégl, Bianca, Keilhauer, Azadeh, Keivani, Ernesto, Kemp, Roger, Kieckhafer, Hans, Klages, Matthias, Kleifges, Jonny, Kleinfeller, Raphael, Krause, Nicole, Krohm, Oliver, Krömer, Daniel Kruppke Hansen, Daniel, Kuempel, Norbert, Kunka, Danielle, Lahurd, Luca, Latronico, Robert, Lauer, Markus, Lauscher, Pascal, Lautridou, Sandra Le Coz, Milton, Leão, Didier, Lebrun, Paul, Lebrun, Marcelo Augusto Leigui de Oliveira, Antoine Letessier Selvon, Isabelle Lhenry Yvon, Katrin, Link, Rebeca, López, Angeles Lopez Agüera, Karim, Louedec, Julio Lozano Bahilo, Lu, Lu, Agustin, Lucero, Marianne, Ludwig, Max, Malacari, Simone, Maldera, Manuela, Mallamaci, Jennifer, Maller, Dusan, Mandat, Paul, Mantsch, Analisa, Mariazzi, Vincent, Marin, Ioana, Mariş, Giovanni, Marsella, Daniele, Martello, Lilian, Martin, Humberto, Martinez, Oscar Martínez Bravo, Diane, Martraire, Jimmy Masías Meza, Hermann Josef Mathes, Sebastian, Mathys, James, Matthews, John, Matthews, Giorgio, Matthiae, Detlef, Maurel, Daniela, Maurizio, Eric, Mayotte, Peter, Mazur, Carlos, Medina, Gustavo Medina Tanco, Rebecca, Meissner, Maximilien, Melissas, Diego, Melo, Alexander, Menshikov, Stefano, Messina, Rishi, Meyhandan, Saša, Mićanović, Maria Isabel Micheletti, Lukas, Middendorf, Minaya, Ignacio A., Lino, Miramonti, Bogdan, Mitrica, Laura Molina Bueno, Silvia, Mollerach, Maria, Monasor, Delphine Monnier Ragaigne, François, Montanet, Carlo, Morello, Miguel, Mostafá, Moura, Celio A., Marcio Aparecido Muller, Gero, Müller, Sarah, Müller, Moritz, Münchmeyer, Roberto, Mussa, Gianni, Navarra, Sergio, Navas, Petr, Necesal, Lukas, Nellen, Anna, Nelles, Jens, Neuser, Nguyen, Phong H., Marcus, Niechciol, Lukas, Niemietz, Tim, Niggemann, Dave, Nitz, Dalibor, Nosek, Vladimir, Novotny, Lyberis, Nožka, Livingstone, Ochilo, Angela, Olinto, Micael, Oliveira, Noelia, Pacheco, Daniel Pakk Selmi Dei, Miroslav, Palatka, Juan, Pallotta, Nunzia, Palmieri, Philipp, Papenbreer, Gonzalo, Parente, Alejandra, Parra, Thomas, Paul, Miroslav, Pech, Jan, Pękala, Rodrigo, Pelayo, Iuri, Pepe, Lorenzo, Perrone, Emily, Petermann, Christine, Peters, Sergio, Petrera, Yevgeniy, Petrov, Jamyang, Phuntsok, Ricardo, Piegaia, Tanguy, Pierog, Pablo, Pieroni, Mário, Pimenta, Valerio, Pirronello, Manuel, Platino, Matthias, Plum, Alessio, Porcelli, Czeslaw, Porowski, Raul Ribeiro Prado, Paolo, Privitera, Michael, Prouza, Victor, Purrello, Quel, Eduardo J., Sven, Querchfeld, Sean, Quinn, Julian, Rautenberg, Olivier, Ravel, Diego, Ravignani, Benoît, Revenu, Jan, Ridky, Simone, Riggi, Markus, Risse, Pablo, Ristori, Vincenzo, Rizi, Washington Rodrigues de Carvalho, Iago Rodriguez Cabo, Gonzalo Rodriguez Fernandez, Jorge Rubén Rodriguez Rojo, Maria Dolores Rodríguez Frías, Dmytro, Rogozin, Germán, Ros, Jaime, Rosado, Tomas, Rossler, Markus, Roth, Esteban, Roulet, Adrian, Rovero, Saffi, Steven J., Alexandra, Saftoiu, Francesco, Salamida, Humberto, Salazar, Ahmed, Saleh, Francisco Salesa Greus, Gaetano, Salina, Federico, Sánchez, Patricia Sanchez Lucas, Santo, Catarina E., Edivaldo Moura Santos, Eva, Santos, Fred, Sarazin, Biswaijt, Sarkar, Raul, Sarmento, Ricardo, Sato, Nils, Scharf, Viviana, Scherini, Harald, Schieler, Peter, Schiffer, David, Schmidt, Olaf, Scholten, Harm, Schoorlemmer, Petr, Schovánek, Alexander, Schulz, Johannes, Schulz, Johannes, Schumacher, Sergio, Sciutto, Alberto, Segreto, Mariangela, Settimo, Amir, Shadkam, Shellard, Ronald C., Iván, Sidelnik, Guenter, Sigl, Octavian, Sima, Andrzej, Śmiałkowski, Radomir, Šmída, Gregory, Snow, Paul, Sommers, Sorokin, J., Ruben, Squartini, Srivastava, Yogendra N., Samo, Stanič, James, Stapleton, Jaroslaw, Stasielak, Maurice, Stephan, Anne, Stutz, Federico, Suarez, Tiina, Suomijärvi, Daniel Supanitsky, A., Michael, Sutherland, John, Swain, Zbigniew, Szadkowski, Marek, Szuba, Oscar Alejandro Taborda, Alex, Tapia, Mathieu, Tartare, Andreas, Tepe, Vanessa Menezes Theodoro, Charles, Timmermans, Todero Peixoto, Carlos J., Gabriel, Toma, Lenka, Tomankova, Bernardo, Tomé, Aurelio, Tonachini, Guillermo Torralba Elipe, Diego Torres Machado, Petr, Travnicek, Enrica, Trovato, Matias, Tueros, Ralf, Ulrich, Michael, Unger, Martin, Urban, Valdés Galicia, Jose F., Ines, Valiño, Laura, Valore, Guus van Aar, Patrick van Bodegom, van den Berg, Ad M., Sjoert van Velzen, Arjen van Vliet, Enrique, Varela, Bernardo Vargas Cárdenas, Gary, Varner, Vázquez, Jose R., Ricardo, Vázquez, Darko, Veberič, Valerio, Verzi, Jakub, Vicha, Mariela, Videla, Luis, Villaseñor, Brian, Vlcek, Serguei, Vorobiov, Hernan, Wahlberg, Oscar, Wainberg, David, Walz, Alan, Watson, Marc, Weber, Klaus, Weidenhaupt, Andreas, Weindl, Felix, Werner, Allan, Widom, Lawrence, Wiencke, Barbara, Wilczyńska, Henryk, Wilczyński, Martin, Will, Christopher, Williams, Tobias, Winchen, David, Wittkowski, Brian, Wundheiler, Sarka, Wykes, Tokonatsu, Yamamoto, Tolga, Yapici, Guofeng, Yuan, Alexey, Yushkov, Bruno, Zamorano, Enrique, Zas, Danilo, Zavrtanik, Marko, Zavrtanik, Ingyin, Zaw, Arnulfo, Zepeda, Jing, Zhou, Yue, Zhu, Marcelo Zimbres Silva, Michael, Ziolkowski, Francesca, Zuccarello, Rasha, Abbasi, Michihiko, Abe, Tareq Abu Zayyad, Monica, Allen, Robyn, Anderson, Ryuji, Azuma, Elliott, Barcikowski, Belz, John W., Bergman, Douglas R., Samuel Adam Blake, Robert, Cady, Min Jung Chae, Byung Gu Cheon, Junsei, Chiba, Michiyuki, Chikawa, Woo Ram Cho, Masaki, Fukushima, Takashi, Goto, William, Hanlon, Yoshio, Hayashi, Naoaki, Hayashida, Kinya, Hibino, Ken, Honda, Daisuke, Ikeda, Naoya, Inoue, Takaaki, Ishii, Rie, Ishimori, Hideo Ito (Utah, U., Riken, Dmitri, Ivanov, Jui, Charles C. H., Kenichi, Kadota, Fumio, Kakimoto, Oleg, Kalashev, Katsuaki, Kasahara, Hideyuki, Kawai, Saburo, Kawakami, Shingo, Kawana, Kazumasa, Kawata, Eiji, Kido, Hang Bae Kim, Ji Hee Kim, Ji Hyun Kim, Seiji, Kitamura, Yuki, Kitamura, Vadim, Kuzmin, Young Joon Kwon, Jian, Lan, Sun In Lim, Jon Paul Lundquist, Kazuhiro, Machida, Kai, Martens, Takeshi, Matsuda, Toshio, Matsuyama, Matthews, John N., Mayuko, Minamino, Keijiro, Mukai, Isaac, Myers, Keisuke, Nagasawa, Shigehiro, Nagataki, Toru, Nakamura, Toshiyuki, Nonaka, Asuka, Nozato, Shoichi, Ogio, Jun, Ogura, Munehiro, Ohnishi, Hideyuki, Ohoka, Kaoru, Oki, Takeshi, Okuda, Masaomi, Ono, Akitoshi, Oshima, Shunsuke, Ozawa, Park, Il H., Pshirkov, Maxim S., Douglas Chase Rodriguez, Grigory, Rubtsov, Dongsu, Ryu, Hiroyuki, Sagawa, Nobuyuki, Sakurai, Sampson, Amanda L., Scott, Lauren M., Priti Dhanesh Shah, Fumiya, Shibata, Tatsunobu, Shibata, Hideaki, Shimodaira, Bok Kyun Shin, Smith, Jeremy D., Pierre, Sokolsky, Wayne Springer, R., Benjamin Taylor Stokes, Stratton, Sean R., Thomas, Stroman, Takumi, Suzawa, Mai, Takamura, Masahiro, Takeda, Ryuji, Takeishi, Akimichi, Taketa, Masato, Takita, Yuichiro, Tameda, Hideki, Tanaka, Koichi, Tanaka, Manobu, Tanaka, Thomas, Stanton B., Thomson, Gordon B., Peter, Tinyakov, Igor, Tkachev, Hisao, Tokuno, Takayuki, Tomida, Sergey, Troitsky, Yoshiki, Tsunesada, Kazuki, Tsutsumi, Yukio, Uchihori, Shigeharu, Udo, Federico, Urban, Gina, Vasiloff, Tiffany, Wong, Hiroshi, Yamaoka, Katsuya, Yamazaki, Jongmann, Yang, Kenta, Yashiro, Shigeru, Yoshida, Hisashi, Yoshii, Rhett, Zollinger, Zachary, Zundel, Shogo, Konishi, Shingo, Wachi, Yoshiki, Nishimoto, Heungsu, Shin, Mai, Tsujimoto, Tomoya, Matsuhira, Laboratoire de Physique Nucléaire et de Hautes Énergies (LPNHE), Université Pierre et Marie Curie - Paris 6 (UPMC)-Institut National de Physique Nucléaire et de Physique des Particules du CNRS (IN2P3)-Université Paris Diderot - Paris 7 (UPD7)-Centre National de la Recherche Scientifique (CNRS), Laboratoire SUBATECH Nantes (SUBATECH), Mines Nantes (Mines Nantes)-Université de Nantes (UN)-Institut National de Physique Nucléaire et de Physique des Particules du CNRS (IN2P3)-Centre National de la Recherche Scientifique (CNRS), Unité Scientifique de la Station de Nançay (USN), Observatoire des Sciences de l'Univers en région Centre (OSUC), Institut national des sciences de l'Univers (INSU - CNRS)-Observatoire de Paris, Université Paris sciences et lettres (PSL)-Université Paris sciences et lettres (PSL)-Université d'Orléans (UO)-Centre National de la Recherche Scientifique (CNRS)-Institut national des sciences de l'Univers (INSU - CNRS)-Observatoire de Paris, Université Paris sciences et lettres (PSL)-Université d'Orléans (UO)-Centre National de la Recherche Scientifique (CNRS), Laboratoire de l'Accélérateur Linéaire (LAL), Université Paris-Sud - Paris 11 (UP11)-Institut National de Physique Nucléaire et de Physique des Particules du CNRS (IN2P3)-Centre National de la Recherche Scientifique (CNRS), Laboratoire de Physique Subatomique et de Cosmologie (LPSC), Université Joseph Fourier - Grenoble 1 (UJF)-Institut polytechnique de Grenoble - Grenoble Institute of Technology (Grenoble INP )-Institut National de Physique Nucléaire et de Physique des Particules du CNRS (IN2P3)-Institut Polytechnique de Grenoble - Grenoble Institute of Technology-Centre National de la Recherche Scientifique (CNRS), Institut de Physique Nucléaire d'Orsay (IPNO), PIERRE AUGER, Centre National de la Recherche Scientifique (CNRS)-Université Paris Diderot - Paris 7 (UPD7)-Institut National de Physique Nucléaire et de Physique des Particules du CNRS (IN2P3)-Université Pierre et Marie Curie - Paris 6 (UPMC), Centre National de la Recherche Scientifique (CNRS)-Institut National de Physique Nucléaire et de Physique des Particules du CNRS (IN2P3)-Université de Nantes (UN)-Mines Nantes (Mines Nantes), Centre National de la Recherche Scientifique (CNRS)-Observatoire de Paris, Université Paris sciences et lettres (PSL)-Université Paris sciences et lettres (PSL)-Institut national des sciences de l'Univers (INSU - CNRS)-Observatoire des Sciences de l'Univers en région Centre (OSUC), Université Paris sciences et lettres (PSL)-Université d'Orléans (UO)-Centre National de la Recherche Scientifique (CNRS)-Université d'Orléans (UO), Centre National de la Recherche Scientifique (CNRS)-Institut National de Physique Nucléaire et de Physique des Particules du CNRS (IN2P3)-Université Paris-Sud - Paris 11 (UP11), Institut polytechnique de Grenoble - Grenoble Institute of Technology (Grenoble INP )-Institut Polytechnique de Grenoble - Grenoble Institute of Technology-Institut National de Physique Nucléaire et de Physique des Particules du CNRS (IN2P3)-Université Joseph Fourier - Grenoble 1 (UJF)-Centre National de la Recherche Scientifique (CNRS), A., Aab, P., Abreu, M., Aglietta, E. J., Ahn, I., Al Samarai, I. F. M., Albuquerque, I., Allekotte, J., Allen, P., Allison, A., Almela, J., Alvarez Castillo, J., Alvarez Mu?iz, R., Alves Batista, M., Ambrosio, A., Aminaei, L., Anchordoqui, S., Andringa, Aramo, Carla, F., Arquero, H., Asorey, P., Assi, J., Aublin, M., Ave, M., Avenier, G., Avila, A. M., Badescu, K. B., Barber, J., B?uml, C., Bau, J. J., Beatty, K. H., Becker, J. A., Bellido, C., Berat, M. E., Bertaina, X., Bertou, P. L., Biermann, P., Billoir, M., Blanco, C., Bleve, H., Bl?mer, M., Boh??ov?, D., Boncioli, C., Bonifazi, R., Bonino, N., Borodai, J., Brack, I., Brancu, P., Brogueira, W. C., Brown, P., Buchholz, A., Bueno, S., Buitink, Buscemi, Mario, K. S., Caballero Mora, B., Caccianiga, L., Caccianiga, M., Candusso, L., Caramete, R., Caruso, A., Castellina, G., Cataldi, L., Cazon, R., Cester, A. G., Chavez, A., Chiavassa, J. A., Chinellato, J., Chudoba, Cilmo, Marco, R. W., Clay, G., Cocciolo, Colalillo, Roberta, A., Coleman, L., Collica, M. R., Coluccia, R., Concei??o, F., Contrera, M. J., Cooper, A., Cordier, S., Coutu, C. E., Covault, J., Cronin, A., Curutiu, R., Dallier, B., Daniel, S., Dasso, K., Daumiller, B. R., Dawson, R. M., de Almeida, M., De Domenico, S. J., de Jong, J. R. T., de Mello Neto, I., De Mitri, J., de Oliveira, V., de Souza, L., del Peral, O., Deligny, H., Dembinski, N., Dhital, C., Di Giulio, A., Di Matteo, J. C., Diaz, M. L., D?az Castro, F., Diogo, C., Dobrigkeit, W., Docter, J. C., D'Olivo, A., Dorofeev, Q., Dorosti Hasankiadeh, M. T., Dova, J., Ebr, R., Engel, M., Erdmann, M., Erfani, C. O., Escobar, J., Espadanal, A., Etchegoyen, P., Facal San Lui, H., Falcke, K., Fang, G., Farrar, A. C., Fauth, N., Fazzini, A. P., Ferguson, M., Fernande, B., Fick, J. M., Figueira, A., Filevich, A., Filip?i?, B. D., Fox, O., Fratu, U., Fr?hlich, B., Fuch, T., Fuji, R., Gaior, B., Garc?a, S. T., Garcia Roca, D., Garcia Gamez, D., Garcia Pinto, G., Garilli, A., Gascon Bravo, F., Gate, H., Gemmeke, P. L., Ghia, U., Giaccari, M., Giammarchi, M., Giller, C., Glaser, H., Gla, M., G?mez Berisso, P. F., G?mez Vitale, P., Gon?alve, J. G., Gonzalez, N., Gonz?lez, B., Gookin, A., Gorgi, P., Gorham, P., Gouffon, S., Grebe, N., Griffith, A. F., Grillo, T. D., Grubb, Y., Guardincerri, Guarino, Fausto, G. P., Guede, M. R., Hampel, P., Hansen, D., Harari, T. A., Harrison, S., Hartmann, J. L., Harton, A., Haung, T., Hebbeker, D., Heck, P., Heimann, A. E., Herve, G. C., Hill, C., Hojvat, N., Hollon, E., Holt, P., Homola, J. R., H?randel, P., Horvath, M., Hrabovsk?, D., Huber, T., Huege, A., Insolia, P. G., Isar, K., Islo, I., Jandt, S., Jansen, C., Jarne, M., Josebachuili, A., K??p?, O., Kambeitz, K. H., Kampert, P., Kasper, I., Katkov, B., K?gl, B., Keilhauer, A., Keivani, E., Kemp, R. M., Kieckhafer, H. O., Klage, M., Kleifge, J., Kleinfeller, R., Krause, N., Krohm, O., Kr?mer, D., Kruppke Hansen, D., Kuempel, N., Kunka, G., La Rosa, D., Lahurd, L., Latronico, R., Lauer, M., Lauscher, P., Lautridou, S., Le Coz, M. S. A. B., Le?o, D., Lebrun, P., Lebrun, M. A., Leigui de Oliveira, A., Letessier Selvon, I., Lhenry Yvon, K., Link, R., L?pez, A., Lopez Ag?era, K., Louedec, J., Lozano Bahilo, L., Lu, A., Lucero, M., Ludwig, M. C., Maccarone, M., Malacari, S., Maldera, M., Mallamaci, J., Maller, D., Mandat, P., Mantsch, A. G., Mariazzi, V., Marin, I. C., Mari?, G., Marsella, D., Martello, L., Martin, H., Martinez, O., Mart?nez Bravo, D., Martraire, J. J., Mas?as Meza, H. J., Mathe, S., Mathy, J. A. J., Matthew, J., Matthew, G., Matthiae, D., Maurel, D., Maurizio, E., Mayotte, P. O., Mazur, C., Medina, G., Medina Tanco, M., Melissa, D., Melo, E., Menichetti, A., Menshikov, S., Messina, R., Meyhandan, S., Mi?anovi?, M. I., Micheletti, L., Middendorf, I. A., Minaya, L., Miramonti, B., Mitrica, L., Molina Bueno, S., Mollerach, M., Monasor, D., Monnier Ragaigne, F., Montanet, C., Morello, M., Mostaf?, C. A., Moura, M. A., Muller, G., M?ller, M., M?nchmeyer, R., Mussa, G., Navarra, S., Nava, P., Necesal, L., Nellen, A., Nelle, J., Neuser, M., Niechciol, L., Niemietz, T., Niggemann, D., Nitz, D., Nosek, V., Novotny, L., No?ka, L., Ochilo, A., Olinto, M., Oliveira, N., Pacheco, D., Pakk Selmi Dei, M., Palatka, J., Pallotta, N., Palmieri, P., Papenbreer, G., Parente, A., Parra, T., Paul, M., Pech, J., P?kala, R., Pelayo, I. M., Pepe, L., Perrone, R., Pesce, E., Petermann, C., Peter, S., Petrera, A., Petrolini, Y., Petrov, J., Phuntsok, R., Piegaia, T., Pierog, P., Pieroni, M., Pimenta, V., Pirronello, M., Platino, M., Plum, A., Porcelli, C., Porowski, R. R., Prado, P., Privitera, M., Prouza, V., Purrello, E. J., Quel, S., Querchfeld, S., Quinn, J., Rautenberg, O., Ravel, D., Ravignani, B., Revenu, J., Ridky, S., Riggi, M., Risse, P., Ristori, V., Rizi, J., Robert, W., Rodrigues de Carvalho, I., Rodriguez Cabo, G., Rodriguez Fernandez, J., Rodriguez Rojo, M. D., Rodr?guez Fr?a, G., Ro, J., Rosado, T., Rossler, M., Roth, E., Roulet, A. C., Rovero, S. J., Saffi, A., Saftoiu, F., Salamida, H., Salazar, A., Saleh, F., Salesa Greu, G., Salina, F., S?nchez, P., Sanchez Luca, C. E., Santo, E., Santo, E. M., Santo, F., Sarazin, B., Sarkar, R., Sarmento, R., Sato, N., Scharf, V., Scherini, H., Schieler, P., Schiffer, O., Scholten, H., Schoorlemmer, P., Schov?nek, A., Schulz, J., Schulz, J., Schumacher, S. J., Sciutto, A., Segreto, M., Settimo, A., Shadkam, R. C., Shellard, I., Sidelnik, G., Sigl, O., Sima, A., ?mia?kowski, R., ?m?da, G. R., Snow, P., Sommer, J., Sorokin, R., Squartini, Y. N., Srivastava, S., Stani?, J., Stapleton, J., Stasielak, M., Stephan, A., Stutz, F., Suarez, T., Suomij?rvi, A. D., Supanitsky, M. S., Sutherland, J., Swain, Z., Szadkowski, M., Szuba, O. A., Taborda, A., Tapia, M., Tartare, V. M., Theodoro, C., Timmerman, C. J., Todero Peixoto, G., Toma, L., Tomankova, B., Tom?, A., Tonachini, G., Torralba Elipe, D., Torres Machado, P., Travnicek, E., Trovato, M., Tuero, R., Ulrich, M., Unger, M., Urban, Galicia, J. F. Vald?s., I., Vali?o, Valore, Laura, G., van Aar, A. M., van den Berg, S., van Velzen, A., van Vliet, E., Varela, B., Vargas C?rdena, G., Varner, J. R., V?zquez, R. A., V?zquez, D., Veberi?, V., Verzi, J., Vicha, M., Videla, L., Villase?or, B., Vlcek, S., Vorobiov, H., Wahlberg, O., Wainberg, D., Walz, A. 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P., Lundquist, K., Machida, K., Marten, T., Matsuda, T., Matsuyama, J. N., Matthew, M., Minamino, K., Mukai, I., Myer, K., Nagasawa, S., Nagataki, T., Nakamura, T., Nonaka, A., Nozato, S., Ogio, J., Ogura, M., Ohnishi, H., Ohoka, K., Oki, T., Okuda, M., Ono, A., Oshima, S., Ozawa, I. H., Park, M. S., Pshirkov, D. C., Rodriguez, G., Rubtsov, D., Ryu, H., Sagawa, N., Sakurai, A. L., Sampson, L. M., Scott, P. D., Shah, F., Shibata, T., Shibata, H., Shimodaira, B. K., Shin, J. D., Smith, P., Sokolsky, R. W., Springer, B. T., Stoke, S. R., Stratton, T. A., Stroman, T., Suzawa, M., Takamura, M., Takeda, R., Takeishi, A., Taketa, M., Takita, Y., Tameda, H., Tanaka, K., Tanaka, M., Tanaka, S. B., Thoma, G. 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Diaz, M. L. Díaz, F. Diogo, C. Dobrigkeit, W. Docter, J. C. D'Olivo, A. Dorofeev, Q. D. Hasankiadeh, M. T. Dova, J. Ebr, R. Engel, M. Erdmann, M. Erfani, C. O. Escobar, J. Espadanal, A. Etchegoyen, P. F. San, H. Falcke, K. Fang, G. Farrar, A. C. Fauth, N. Fazzini, A. P. Ferguson, M. Fernande, B. Fick, J. M. Figueira, A. Filevich, A. Filipčič, B. D. Fox, O. Fratu, U. Fröhlich, B. Fuch, T. Fuji, R. Gaior, B. García, S. T. Garcia, D. Garcia-Gamez, D. Garcia-Pinto, G. Garilli, A. G. Bravo, F. Gate, H. Gemmeke, P. L. Ghia, U. Giaccari, M. Giammarchi, M. Giller, C. Glaser, H. Gla, M. G. Berisso, P. F. Gómez, P. Gonçalve, J. G. Gonzalez, N. González, B. Gookin, A. Gorgi, P. Gorham, P. Gouffon, S. Grebe, N. Griffith, A. F. Grillo, T. D. Grubb, Y. Guardincerri, F. Guarino, G. P. Guede, M. R. Hampel, P. Hansen, D. Harari, T. A. Harrison, S. Hartmann, J. L. Harton, A. Haung, T. Hebbeker, D. Heck, P. Heimann, A. E. Herve, G. C. Hill, C. Hojvat, N. Hollon, E. Holt, P. Homola, J. R. Hörandel, P. Horvath, M. Hrabovský, D. Huber, T. Huege, A. Insolia, P. G. Isar, K. Islo, I. Jandt, S. Jansen, C. Jarne, M. Josebachuili, A. Kääpä, O. Kambeitz, K. H. Kampert, P. Kasper, I. Katkov, B. Kégl, B. Keilhauer, A. Keivani, E. Kemp, R. M. Kieckhafer, H. O. Klage, M. Kleifge, J. Kleinfeller, R. Krause, N. Krohm, O. Krömer, D. Kruppke-Hansen, D. Kuempel, N. Kunka, G. L. Rosa, D. LaHurd, L. Latronico, R. Lauer, M. Lauscher, P. Lautridou, S. L. Coz, M. S. A., D. Lebrun, P. Lebrun, M. A. Leigui, A. Letessier-Selvon, I. Lhenry-Yvon, K. Link, R. López, A. L. Agüera, K. Louedec, J. L. Bahilo, L. Lu, A. Lucero, M. Ludwig, M. C. Maccarone, M. Malacari, S. Maldera, M. Mallamaci, J. Maller, D. Mandat, P. Mantsch, A. G. Mariazzi, V. Marin, I. C. Mariş, G. Marsella, D. Martello, L. Martin, H. Martinez, O. M. Bravo, D. Martraire, J. J. Masía, H. J. Mathe, S. Mathy, J. A. J., J. Matthew, G. Matthiae, D. Maurel, D. Maurizio, E. Mayotte, P. O. Mazur, C. Medina, G. Medina-Tanco, M. Melissa, D. Melo, E. Menichetti, A. Menshikov, S. Messina, R. Meyhandan, S. Mićanović, M. I. Micheletti, L. Middendorf, I. A. Minaya, L. Miramonti, B. Mitrica, L. Molina-Bueno, S. Mollerach, M. Monasor, D. M. Ragaigne, F. Montanet, C. Morello, M. Mostafá, C. A. Moura, M. A. Muller, G. Müller, M. Münchmeyer, R. Mussa, G. Navarra, S. Nava, P. Necesal, L. Nellen, A. Nelle, J. Neuser, M. Niechciol, L. Niemietz, T. Niggemann, D. Nitz, D. Nosek, V. Novotny, L. Nožka, L. Ochilo, A. Olinto, M. Oliveira, N. Pacheco, D. P. Selmi-Dei, M. Palatka, J. Pallotta, N. Palmieri, P. Papenbreer, G. Parente, A. Parra, T. Paul, M. Pech, J. Pękala, R. Pelayo, I. M. Pepe, L. Perrone, R. Pesce, E. Petermann, C. Peter, S. Petrera, A. Petrolini, Y. Petrov, J. Phuntsok, R. Piegaia, T. Pierog, P. Pieroni, M. Pimenta, V. Pirronello, M. Platino, M. Plum, A. Porcelli, C. Porowski, R. R. Prado, P. Privitera, M. Prouza, V. Purrello, E. J. Quel, S. Querchfeld, S. Quinn, J. Rautenberg, O. Ravel, D. Ravignani, B. Revenu, J. Ridky, S. Riggi, M. Risse, P. Ristori, V. Rizi, J. Robert, W. R. de, I. R. Cabo, G. R. Fernandez, J. R. Rojo, M. D. Rodríguez-Fría, G. Ro, J. Rosado, T. Rossler, M. Roth, E. Roulet, A. C. Rovero, S. J. Saffi, A. Saftoiu, F. Salamida, H. Salazar, A. Saleh, F. S. Greu, G. Salina, F. Sánchez, P. Sanchez-Luca, C. E. Santo, E. Santo, E. M. Santo, F. Sarazin, B. Sarkar, R. Sarmento, R. Sato, N. Scharf, V. Scherini, H. Schieler, P. Schiffer, O. Scholten, H. Schoorlemmer, P. Schovánek, A. Schulz, J. Schulz, J. Schumacher, S. J. Sciutto, A. Segreto, M. Settimo, A. Shadkam, R. C. Shellard, I. Sidelnik, G. Sigl, O. Sima, A. Śmiałkowski, R. Šmída, G. R. Snow, P. Sommer, J. Sorokin, R. Squartini, Y. N. Srivastava, S. Stanič, J. Stapleton, J. Stasielak, M. Stephan, A. Stutz, F. Suarez, T. Suomijärvi, A. D. Supanitsky, M. S. Sutherland, J. Swain, Z. Szadkowski, M. Szuba, O. A. Taborda, A. Tapia, M. Tartare, V. M. Theodoro, C. Timmerman, C. J. Todero, G. Toma, L. Tomankova, B. Tomé, A. Tonachini, G. T. Elipe, D. T. Machado, P. Travnicek, E. Trovato, M. Tuero, R. Ulrich, M. Unger, M. Urban, J. F. Valdé, I. Valiño, L. Valore, G. v. Aar, A. M. van, S. v. Velzen, A. v. Vliet, E. Varela, B. V. Cárdena, G. Varner, J. R. Vázquez, R. A. Vázquez, D. Veberič, V. Verzi, J. Vicha, M. Videla, L. Villaseñor, B. Vlcek, S. Vorobiov, H. Wahlberg, O. Wainberg, D. Walz, A. A. Watson, M. Weber, K. Weidenhaupt, A. Weindl, F. Werner, A. Widom, L. Wiencke, B. Wilczyńska, H. Wilczyński, M. Will, C. William, T. Winchen, D. Wittkowski, B. Wundheiler, S. Wyke, T. Yamamoto, T. Yapici, P. Younk, G. Yuan, A. Yushkov, B. Zamorano, E. Za, D. Zavrtanik, M. Zavrtanik, I. Zaw, A. Zepeda, J. Zhou, Y. Zhu, M. Z. Silva, M. Ziolkowski, T. P. Auger, R. U. Abbasi, M. Abe, T. Abu-Zayyad, M. Allen, R. Anderson, R. Azuma, E. Barcikowski, J. W. Belz, D. R. Bergman, S. A. Blake, R. Cady, M. J. Chae, B. G. Cheon, J. Chiba, M. Chikawa, W. R. Cho, T. Fujii, M. Fukushima, T. Goto, W. Hanlon, Y. Hayashi, N. Hayashida, K. Hibino, K. Honda, D. Ikeda, N. Inoue, T. Ishii, R. Ishimori, H. Ito, D. Ivanov, C. C. H., K. Kadota, F. Kakimoto, O. Kalashev, K. Kasahara, H. Kawai, S. Kawakami, S. Kawana, K. Kawata, E. Kido, H. B. Kim, J. H. Kim, S. Kitamura, Y. Kitamura, V. Kuzmin, Y. J. Kwon, J. Lan, S. I. Lim, J. P. Lundquist, K. Machida, K. Marten, T. Matsuda, T. Matsuyama, J. N. Matthew, M. Minamino, K. Mukai, I. Myer, K. Nagasawa, S. Nagataki, T. Nakamura, T. Nonaka, A. Nozato, S. Ogio, J. Ogura, M. Ohnishi, H. Ohoka, K. Oki, T. Okuda, M. Ono, A. Oshima, S. Ozawa, I. H. Park, M. S. Pshirkov, D. C. Rodriguez, G. Rubtsov, D. Ryu, H. Sagawa, N. Sakurai, A. L. Sampson, L. M. Scott, P. D. Shah, F. Shibata, T. Shibata, H. Shimodaira, B. K. Shin, J. D. Smith, P. Sokolsky, R. W. Springer, B. T. Stoke, S. R. Stratton, T. A. Stroman, T. Suzawa, M. Takamura, M. Takeda, R. Takeishi, A. Taketa, M. Takita, Y. Tameda, H. Tanaka, K. Tanaka, M. Tanaka, S. B. Thoma, G. B. Thomson, P. Tinyakov, I. Tkachev, H. Tokuno, T. Tomida, S. Troitsky, Y. Tsunesada, K. Tsutsumi, Y. Uchihori, S. Udo, F. Urban, G. Vasiloff, T. Wong, R. Yamane, H. Yamaoka, K. Yamazaki, J. Yang, K. Yashiro, Y. Yoneda, S. Yoshida, H. Yoshii, R. Zollinger, Z. Zundel, T. T. Array, and Research unit Astroparticle Physics
- Subjects
Ciencias Físicas ,Astronomy ,Rays ,Astrophysics ,Astroparticle physics ,Cosmic rays ,01 natural sciences ,law.invention ,Pierre ,law ,Anisotropy ,Telescope ,010303 astronomy & astrophysics ,High Energy Astrophysical Phenomena (astro-ph.HE) ,Physics ,[PHYS]Physics [physics] ,Energy ,[SDU.ASTR.HE]Sciences of the Universe [physics]/Astrophysics [astro-ph]/High Energy Astrophysical Phenomena [astro-ph.HE] ,Astrophysics::Instrumentation and Methods for Astrophysics ,astroparticle physic ,Radiación cósmica ,Auger ,Cosmic ,Arrival ,ComputingMethodologies_DOCUMENTANDTEXTPROCESSING ,Física nuclear ,Astrophysics - High Energy Astrophysical Phenomena ,Astrophysics - Instrumentation and Methods for Astrophysics ,CIENCIAS NATURALES Y EXACTAS ,High ,[PHYS.ASTR.HE]Physics [physics]/Astrophysics [astro-ph]/High Energy Astrophysical Phenomena [astro-ph.HE] ,[PHYS.ASTR.IM]Physics [physics]/Astrophysics [astro-ph]/Instrumentation and Methods for Astrophysic [astro-ph.IM] ,Astrophysics::High Energy Astrophysical Phenomena ,FOS: Physical sciences ,Cosmic ray ,SURFACE DETECTOR ,ICECUBE ,AIR-SHOWER ARRAY ,Directions ,cosmic rays ,0103 physical sciences ,Instrumentation and Methods for Astrophysics (astro-ph.IM) ,Ciencias Exactas ,Pierre Auger Observatory ,SPECTRUM ,010308 nuclear & particles physics ,Array ,Spectral density ,Spherical harmonics ,Física ,Astronomy and Astrophysics ,ASTROFÍSICA ,Ultra ,[SDU.ASTR.IM]Sciences of the Universe [physics]/Astrophysics [astro-ph]/Instrumentation and Methods for Astrophysic [astro-ph.IM] ,Astronomía ,Dipole ,RESOLUTION ,Space and Planetary Science ,Experimental High Energy Physics ,Quadrupole ,Observatory ,[PHYS.ASTR]Physics [physics]/Astrophysics [astro-ph] - Abstract
Spherical harmonic moments are well-suited for capturing anisotropy at any scale in the flux of cosmic rays. An unambiguous measurement of the full set of spherical harmonic coefficients requires full-sky coverage. This can be achieved by combining data from observatories located in both the northern and southern hemispheres. To this end, a joint analysis using data recorded at the Telescope Array and the Pierre Auger Observatory above 1019 eV is presented in this work. The resulting multipolar expansion of the flux of cosmic rays allows us to perform a series of anisotropy searches, and in particular to report on the angular power spectrum of cosmic rays above 1019 eV. No significant deviation from isotropic expectations is found throughout the analyses performed. Upper limits on the amplitudes of the dipole and quadrupole moments are derived as a function of the direction in the sky, varying between 7% and 13% for the dipole and between 7% and 10% for a symmetric quadrupole., Facultad de Ciencias Exactas
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- 2014
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6. ChemInform Abstract: A Novel One-Pot Synthesis of Secondary Alcohols from Esters
- Author
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Ah Ram Jeon, Jae Kyo Park, Min Jung Chae, and Duk Keun An
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Reduction (complexity) ,Chemistry ,organic chemicals ,One-pot synthesis ,technology, industry, and agriculture ,Organic chemistry ,lipids (amino acids, peptides, and proteins) ,macromolecular substances ,General Medicine ,Alkylation - Abstract
Partial reduction of the esters and subsequent alkylation or vinylation provides the desired alcohols.
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- 2011
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7. ChemInform Abstract: A New and General One-Pot Synthesis of Propargyl Alcohols from Esters
- Author
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Duk Keun An, Tom Livinghouse, Min Jung Chae, and Ah Ram Jeon
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chemistry ,Reducing agent ,Propargyl ,One-pot synthesis ,chemistry.chemical_element ,Lithium ,General Medicine ,Combinatorial chemistry - Abstract
Intermediates easily prepared by partial reduction of various esters with LDBBA as a reducing agent smoothly react with lithium acetylides to give propargyl alcohols, without isolation of partial reduction intermediates, in good yields (73–83%).
- Published
- 2011
- Full Text
- View/download PDF
8. A new and general one-pot synthesis of propargyl alcohols from esters
- Author
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Min Jung Chae, Tom Livinghouse, Ah Ram Jeon, and Duk Keun An
- Subjects
Reducing agent ,Propanols ,One-pot synthesis ,Metals and Alloys ,chemistry.chemical_element ,Esters ,General Chemistry ,Lithium ,Catalysis ,Surfaces, Coatings and Films ,Electronic, Optical and Magnetic Materials ,chemistry ,Alkynes ,Propargyl ,Materials Chemistry ,Ceramics and Composites ,Organic chemistry ,Oxidation-Reduction - Abstract
Intermediates easily prepared by partial reduction of various esters with LDBBA as a reducing agent smoothly react with lithium acetylides to give propargyl alcohols, without isolation of partial reduction intermediates, in good yields (73–83%).
- Published
- 2011
9. Chemoselective Reduction of Esters to Aldehydes by Potassium Diisobutyl-t-butoxyaluminum Hydride (PDBBA)
- Author
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Jung In Song, Min Jung Chae, and Duk Keun An
- Subjects
Benzaldehyde ,chemistry.chemical_classification ,chemistry.chemical_compound ,Benzonitrile ,Chemistry ,Benzyl alcohol ,Yield (chemistry) ,Alkoxy group ,General Chemistry ,Medicinal chemistry ,Aldehyde ,Isopropyl ,Ethyl benzoate - Abstract
The reduction of ester to aldehyde is one of the most useful synthetic transformations in organic synthesis, and a large number of reducing agents for this purpose have been reported. Among them, diisobutylaluminum hydride (DIBALH), which is commercially available, is used as one of the most popular reducing agents, although this reagent provides moderate yields (48-88%) and requires a very low temperature (−78 C). Very recently, we reported that lithium diisobutyl-t-butoxyaluminum hydride (LDBBA) and sodium diisobutyl-t-butoxyaluminum hydride (SDBBA), the alkoxy derivatives of DIBALH, were new partial reducing agents which could reduce various esters to aldehydes. Among them, LDBBA was especially effective for partial reduction of isopropyl esters to aldehydes in most cases with >90% yield at 0 C, and SDBBA was also effective for partial reduction of methyl and ethyl esters in very good yield (73-93%) at 0 C. As a part of our research program directed toward the discovery of new reducing agents through simple modification of commercial DIBALH, we recently found that potassium diisobutyl-t-butoxyaluminum hydride (PDBBA) was easily prepared by reacting an equimolar amount of potassium t-butoxide with DIBALH in THF at 0 C or room temperature (Scheme 1). We applied this reagent for the partial reduction of esters and nitriles to aldehydes. We first examined the partial reduction of representative esters and nitriles such as ethyl benzoate (entry 1 in Table 2), ethyl caproate (entry 15 in Table 2), benzonitrile (entry 19 in Table 2) and capronitrile (entry 20 in Table 2) with PDBBA in THF at 0 C. The reduction of these esters provides corresponding aldehydes in very good yield (88-89%) in 2448 h. In contrast, nitriles were not reduced at all. It was found that PDBBA essentially did not attack nitriles at 0 C. Therefore, partial reduction of esters to the correspondig aldehydes chemoselectively in the presence of nitriles was attempted. Indeed, as shown in Table 1, we achieved quantitative conversion of ethyl benzoate into benzaldehyde in mixtures with benzonitrile, with essentially no reduction of the benzonitrile. Accordingly, we applied PDBBA for the synthesis of aldehydes from various esters. The results for representative esters are summarized in Table 2. As shown in Table 2, ethyl benzoate was efficiently reduced to benzaldehyde in 89% yield (entry 1 in Table 2). Under identical conditions, reduction with DIBALH alone provided only benzyl alcohol (entry 2 in Table 2). Isopropyl benzoate need larger amount of hydride (1.5 eq) than sterically unhindered esters such as ethyl benzoate, presumably due to the bulky isopropyl group (entry 3 in Table 2). Also, esters of electron-withdrawing substituents such as ethyl 4fluorobenzoate, methyl 3-chlorobenzoate, ethyl 4-chlorobenzoate, ethyl 2-bromobenzoate, ethyl 4-bromobenzoate and ethyl 4-nitrobenzoate, and electron-donating substituents such as ethyl 2-toluate, ethyl 4-toluate and ethyl 4-methoxybenzoate were readily reduced to the corresponding aldehydes in 71-91% yield (entries 4-12 in Table 2). Among these, the reduction of ethyl 4-methoxybenzoate required a longer reaction time (48 h) than common esters. This may be attributed to the strong electron donating effect of the methoxy group. Similarly, reduction of other aromatic esters such as ethyl 2-naphthalate, a poly-aromatic ester and ethyl 2-furoate, a heterocyclic ester gave the corresponding aldehydes in 88% and 84% yield, respectively (entries 13 and 14 in Table 2). Furthermore, aliphatic esters such as ethyl caproate, isopropyl caproate, ethyl undecanoate and ethyl cyclohexanecarboxylate were efficiently reduced to the corresponding aldehydes in 78-90% yield (entries 15-18 in Table 2). In summary, we easily prepared PDBBA by reacting commercially available DIBALH with potassium t-butoxide.
- Published
- 2007
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