The study aims to produce CuO/Ag thin films by means of sputtering technique at the frequency of 13,56 MHz, that apply as photocatalic degradation of methylene blue dye waste from textile processing. The charakterizations consist of XRD, EDAX, and UV-Vis, as well as optical properties. CuO/Ag thin films were grown onto glass substrat, with variation of depositionstime , whereas the argon- and oxygen partial pressure was held constant at 2.5 × 10-2 mbar, and 0.2 × 10-2 mbar, respectively, using power of 70 Watt, that correspond to 800 V of DC-bias. Research on photodegradation of methylene blue using CuO / Ag photocatalyst by ultraviolet light was carried out by knowing the characteristics of CuO/Ag thin films in the form of optical properties, while the photodegradation was tested at 15 ppm methylene, for 6 hours of irradiation. The light used for irradiation was 10 watt ultraviolet light with 200 Lux intensity. The energy gap was analyzed using swanepoel and tauc method/ equations, resulted the value of 2.12 eV, 2.07 eV, 2.02 eV, and 1.96 eV, for the depositionstime of 1, 2, 3 and 4 minutes, respectively. Results of XRD showed the crystalline phases that are typical of CuO, having peaks 2θ at 38.97° (200), 46.252° (-112), and 51.228⁰ (112), as well as 2θ = 64,523 (110) for Ag The composition of the elements, showed by EDAX, contained 9.07% of Ag, and 35,56% of Cu, as well as 27.47% of O. Photodegradation of methylene blue resulted a high photocatalytic activity, with a degradation of methylene blue by around 88%. [ABSTRACT FROM AUTHOR]