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The book covers a diverse range of topics based on computational studies, including modeling and simulations based on quantum chemical studies and molecular dynamics (MD) simulations. It contains quantum chemical studies on several molecules, including biologically relevant molecules and liquid crystals and various aspects of superatomic clusters including superalkalis and superhalogens. It gives an overview of MD simulations and their applications on biomolecular systems such as HIV-1 protease and integrase.Features: Includes first principle methods, density functional theory, as well as molecular dynamics simulations. Explores quantum chemical studies on several molecules. Gives readers an overview of the power of computation. Discusses superatomic clusters, superalkalis, and superhalogens. Covers themes from molecules, clusters, materials, as well as biophysical systems. This book is aimed at researchers and graduate students in materials science and computational and theoretical chemistry.

Materials Science today is the base for all technological and industrial developments. The book provides the understanding of the advanced spectroscopic and microscopic instruments used for material characterization. The main issues addressed are 1) a detailed understanding of the instrument, including working and handling, 2) sample preparation, and 3) data analysis and interpretation. The book is divided in two parts i.e., Part A discusses microscopic instruments, consisting of Optical Microscope, Scanning Electron Microscopy, Atomic Force Microscopy, Field Emission Scanning Electron Microscope and X-Ray Diffraction. Part B is on spectroscopic instruments and covers FTIR Spectrometer, Raman Spectrometer, X-ray Photoelectron Spectroscopy, Ultraviolet Photoelectron Spectroscopy, Fluorescence Spectroscopy, and Nuclear Magnetic Resonance Spectroscopy.

The need for functional material is an important issue in the modern world as they play a significant role in our everyday life. New materials are used in technological advancements such as optical, magnetic, structural, or catalytic capabilities. Due to their high importance and significance in our life, many schools offer material chemistry courses and programs around the world. However, there is still a need for a textbook that covers different materials from both structure and property perspective. This book provides in-depth technical knowledge on material chemistry and their applications. It includes fundamental and history of material, as well as chemistry and application of common advanced materials. It has 8 chapters covering fundamentals of materials chemistry, solid materials, semiconductors, polymers, carbon materials, nanomaterials, composites and finally, common material characterization techniques. The information presented in this book is useful for chemistry, physics, and engineering students. It is also particularly valuable for industry researchers as a starting point for learning about materials.

This book provides a comprehensive overview of positron profilometry, specifically focusing on the analysis of defect depth distribution in materials. Positron profilometry plays a crucial role in understanding and characterizing defects in a wide range of materials, including metals, semiconductors, polymers, and ceramics. By analyzing the depth distribution of defects, researchers can gain insights into various material properties, such as crystal structure, defect density, and diffusion behavior. The author's extensive research spanning a period of two decades has primarily centered on subsurface zones. These regions, located beneath the surface and subjected to various surface processes, play a crucial role in generating defect distributions. Three experimental techniques and their data analysis are described in detail: a variable-energy positron beam (VEP) called sometimes a slow positron beam, a technique called implantation profile depth scanning (DSIP), and a sequential etching(SET) technique. The usability of these techniques is illustrated by many examples of measurements by the author and others.

The book covers various methods of characterization of advanced materials commonly used in engineering including understanding of the working principle and applicability of devices. It explores the techniques implemented for advanced materials like superalloys, thin films, powders, nanocomposites, polymers, shape memory alloys, high entropy alloys, and so on. Major instruments covered include X-ray diffraction, near-field scanning optical microscopy Raman, X-ray photospectroscopy, ultraviolet-visible-near-infrared spectrosphotometer, Fourier-transform infrared spectroscopy, differential scanning calorimeter, profilometer, and thermogravimetric analysis. Features: Covers material characterization techniques and the development of advanced characterization technology Includes multiple length scale characterization approaches for a large variety of materials, from nano- to micron-scale, as well as their constraints Discusses advanced material characterization technology in the microstructural and property characterization fields Reviews both practical and theoretical explanations of approaches for characterizing microstructure and properties Offers fundamentals, basic instrumentation details, experimental approaches, analyses, and applications with case studies This book is aimed at graduate students and researchers in materials science and engineering.

With the recent developments in the field of advanced materials, there exists a need for a systematic summary and detailed introduction of the modeling and simulation methods for these materials. This book provides a comprehensive description of the mechanical behavior of advanced materials using modeling and simulation. It includes materials such as high-entropy alloys, high-entropy amorphous alloys, nickel-based superalloys, light alloys, electrode materials, and nanostructured reinforced composites. Reviews the performance and application of a variety of advanced materials and provides the detailed theoretical modeling and simulation of mechanical properties Covers the topics of deformation, fracture, diffusion, and fatigue Features worked examples and exercises that help readers test their understanding This book is aimed at researchers and advanced students in solid mechanics, material science, engineering, material chemistry, and those studying the mechanics of materials.

This book presents commonly applied characterization techniques in material science, their brief history and origins, mechanism of operation, advantages and disadvantages, their biosensing applications, and troubleshooting for each technique, while addressing the challenges researchers face when working with these techniques. The book dedicates its focus to identifying physicochemical and electrochemical nature of materials including analyses of morphology, mass spectrometry, and topography, as well as the characterization of elemental, structural, thermal, wettability, electrochemical, and chromatography properties. Additionally, the main features and benefits of using coupled characterization techniques are discussed in this book.

Shock Compression and Chemical Reaction of Multifunctional Energetic Structural Materials provides an exhaustive overview of the mechanics, kinetics and physio-chemical behavior caused by shock-induced reaction and shock compression on multifunctional energetic structural materials (MESMs). The book covers foundational knowledge on shock waves and Equation of State (EOS), shock parameters, reaction kinetics, impedance matching, and more. In addition, it looks at more advanced subjects such as experimental analysis methods, numerical modeling techniques (from quasi-static to high-strain rates, including void collapse models), how EOS changes when reaction and detonation are involved, and more. Final chapters cover how to obtain EOS curves from experiments and various testing methods and numerical models for non-reactive porous solids and particulate composites, including 1-D reactive flow models. Flyer plate impact experiments are also discussed, as are the applications of hydrocodes and Lagrangian-framework-based methods. Provides an ideal balance of modeling concepts and experimental techniques Looks at mechanical testing processes of MESMs Outlines sample preparation, testing of samples, obtaining EOS from the testing, and using EOS for simulation Covers modeling for pore collapse, constituent material, and at a granular level

This book presents various questions of continuum mechanical modeling in the context of experimental and numerical methods, in particular, multi-field problems that go beyond the standard models of continuum mechanics. In addition, it discusses dynamic problems and practical solutions in the field of numerical methods. It focuses on continuum mechanics, which is often overlooked in the traditional division of mechanics into statics, strength of materials and kinetics. The book is dedicated to Prof. Volker Ulbricht, who passed away on April 9, 2021.

The structure–property relationship is a key topic in materials science and engineering. To understand why a material displays certain behaviors, the first step is to resolve its crystal structure and reveal its structure characteristics. Fundamentals of Crystallography, Powder X-ray Diffraction, and Transmission Electron Microscopy for Materials Scientists equips readers with an in-depth understanding of using powder x-ray diffraction and transmission electron microscopy for the analysis of crystal structures. Introduces fundamentals of crystallography Covers XRD of materials, including geometry and intensity of diffracted x-ray beams and experimental methods Describes TEM of materials and includes atomic scattering factors, electron diffraction, and diffraction and phase contrasts Discusses applications of HRTEM in materials research Explains concepts used in XRD and TEM lab training Based on the author's course lecture notes, this text guides materials science and engineering students with minimal reliance on advanced mathematics. It will also appeal to a broad spectrum of readers, including researchers and professionals working in the disciplines of materials science and engineering, applied physics, and chemical engineering.

Characterization enables a microscopic understanding of the fundamental properties of materials (Science) to predict their macroscopic behaviour (Engineering). With this focus, Principles of Materials Characterization and Metrology presents a comprehensive discussion of the principles of materials characterization and metrology. Characterization techniques are introduced through elementary concepts of bonding, electronic structure of molecules and solids, and the arrangement of atoms in crystals. Then, the range of electrons, photons, ions, neutrons and scanning probes, used in characterization, including their generation and related beam-solid interactions that determine or limit their use, is presented. This is followed by ion-scattering methods, optics, optical diffraction, microscopy, and ellipsometry. Generalization of Fraunhofer diffraction to scattering by a three-dimensional arrangement of atoms in crystals leads to X-ray, electron, and neutron diffraction methods, both from surfaces and the bulk. Discussion of transmission and analytical electron microscopy, including recent developments, is followed by chapters on scanning electron microscopy and scanning probe microscopies. The book concludes with elaborate tables to provide a convenient and easily accessible way of summarizing the key points, features, and inter-relatedness of the different spectroscopy, diffraction, and imaging techniques presented throughout. Principles of Materials Characterization and Metrology uniquely combines a discussion of the physical principles and practical application of these characterization techniques to explain and illustrate the fundamental properties of a wide range of materials in a tool-based approach. Based on forty years of teaching and research, this book incorporates worked examples, to test the reader's knowledge with extensive questions and exercises.

Für die Schadensanalyse ist es von großer Bedeutung, das Material zunächst zu identifizieren, um Rückschlüsse auf Ursachen oder Versagensmuster treffen zu können.Mittels einfacher Bestimmungsmethoden ist es möglich, ohne großen apparativen Aufwand und mit nur wenig chemischen Vorkenntnissen eine Identifizierung durchzuführen. um Rückschlüsse auf Ursache oder Versagensmuster treffen zu können.Weitreichendere Informationen liefert die Kenntnis der Dichte eines Werkstoffes. Mit Hilfe von Dichtemessungen sind neben der Identifizierung von Reinmaterialien Aussagen über Verarbeitungsfehler und Füllstoffgehalte möglich.Methoden der Massenanalyse sind:- Einfache Bestimmungsmethoden (z. B. Bruchprobe, Lösemitteltest, Brandverhalten etc.)- Dichtebestimmung- Feuchtigkeitsbestimmung- Gehalt an Füll- und Verstärkungsstoffen- Bestimmung flüchtiger Bestandteile- Thermogravimetrie- Messunsicherheit- Kunststoff-Bestimmungstafel

This book presents a complex approach to material composition determination based on the analysis of the joint X-ray spectrum, including fluorescence, scattering, and diffraction reflections. It considers fluorescence, scattered, and diffracted radiations within the common problem of analytical spectrum formation. The complex methods for analyzing the material composition by joint spectra of fluorescence, Compton scattering and diffraction proposed here allow for a widening of the area of the application of X-ray methods.The book will be useful for specialists in the field of solid state physics, as well as advanced and post-graduate students.

Scanning Nonlinear Dielectric Microscopy: Investigation of Ferroelectric, Dielectric, and Semiconductor Materials and Devices is the definitive reference on an important tool to characterize ferroelectric, dielectric and semiconductor materials. Written by the inventor, the book reviews the methods for applying the technique to key materials applications, including the measurement of ferroelectric materials at the atomic scale and the visualization and measurement of semiconductor materials and devices at a high level of sensitivity. Finally, the book reviews new insights this technique has given to material and device physics in ferroelectric and semiconductor materials. The book is appropriate for those involved in the development of ferroelectric, dielectric and semiconductor materials devices in academia and industry. Presents an in-depth look at the SNDM materials characterization technique by its inventor Reviews key materials applications, such as measurement of ferroelectric materials at the nanoscale and measurement of semiconductor materials and devices Analyzes key insights on semiconductor materials and device physics derived from the SNDM technique

“Real time” imaging techniques have assisted materials science studies especially for non-ambient environments. These techniques have never been collectively featured in a single venue. The book is an assembly of materials studies utilizing cutting edge real time imaging techniques, emphasizing the significance and impact of those techniques.

This compendium provides a comprehensive collection of the emergent applications of big data, machine learning, and artificial intelligence technologies to present day physical sciences ranging from materials theory and imaging to predictive synthesis and automated research. This area of research is among the most rapidly developing in the last several years in areas spanning materials science, chemistry, and condensed matter physics.Written by world renowned researchers, the compilation of two authoritative volumes provides a distinct summary of the modern advances in instrument — driven data generation and analytics, establishing the links between the big data and predictive theories, and outlining the emerging field of data and physics-driven predictive and autonomous systems.

This book presents the principles, methods and techniques to characterize materials and technical systems. The book is organized with concise text-graphics compilations in three parts:The first part describes the fundamentals of measurement, testing and sensor technology, including a survey of sensor types for dimensional metrology, kinematics, dynamics, and temperature. It describes also microsensors and embedded sensors.The second part gives an overview of materials and explains the application of measurement, testing and sensor technology to characterize composition, microstructure, properties and performance of materials as well as deterioration mechanisms and reliability.The third part introduces the general systems theory for the characterization of technical systems, exemplified by mechatronic and tribological systems. It describes technical diagnostics for structural health monitoring and performance control.

Containing selected papers on Materials Characterisation this volume presents the latest research in the field. Material and contact characterisation is a rapidly advancing field that requires the application of a combination of numerical and experimental methods. Contributions come from both industry and research communities using computational methods and performing experiments. Demand for high quality production from both industry and consumers has led to rapid developments in materials science and engineering. Current research is focussed on modification technologies that can increase the surface durability of materials. The characteristics of the system reveal which surface engineering methods should be chosen and as a consequence it is essential to study the combination of surface treatment and contact mechanics. The accurate characterisation of the physical and chemical properties of materials requires the application of both experimental techniques and computer simulation methods in order to gain a correct analysis. A very wide range of materials, starting with metals through polymers and semiconductors to composites, necessitates a whole spectrum of characteristic experimental techniques and research methods. The papers in this book examine various combinations of techniques across various topics.

This book focuses on the widely used experimental techniques available for the structural, morphological, and spectroscopic characterization of materials. Recent developments in a wide range of experimental techniques and their application to the quantification of materials properties are an essential side of this book. Moreover, it provides concise but thorough coverage of the practical and theoretical aspects of the analytical techniques used to characterize a wide variety of functional nanomaterials. The book provides an overview of widely used characterization techniques for a broad audience: from beginners and graduate students, to advanced specialists in both academia and industry.

“Equal Channel Angular Extrusion” (ECAE) is a significant method in industrial forming applications, which is the most important method for the production of ultrafine grained bulk samples, where plastic strains are introduced into the bulk material without any changes in the cross section. ECAE has different die channel angles from which an optimum die channel angle should be identified so that efficient mechanical properties will be obtained. This study is focused on the plastic deformation behavior of Al alloys by modeling ECAE with experimental and finite element software. A solid model was generated using CATIA. The STL files of ECAE die generated in CATIA were used in DEFORM-3D for simulations. The experiments are performed by designing the ECAE tools such as die, punch and billet. A series of numerical experiments were carried out for the die angles of 115°, 125°and 135° and outer corner angle of 6°, using a billet diameter of 9mm and a height of 70mm. A detailed analysis of the strains introduced by ECAP (“Equal Channel Angular Pressing”) in a single passage through the die is noted. The experiments are conducted by attaching the ECAE tools to the Universal Testing Machine on aluminum alloy. The dimensions are followed for ECAE by taking considerations from the existing literature into account. On the basis of the experiment and simulation results, load, displacement, and punch force are evaluated and compared with each other.

Dieses Praktikerbuch bietet eine kompakte Übersicht zu 50 wichtigen werkstoffanalytischen Verfahren, die jeweils auf einer Doppelseite kurz und übersichtlich dargestellt werden. Diese Verfahren dienen der Ermittlung von Eigenschaften und Defekten im makroskopischen, mikroskopischen und nanoskopischen Bereich. Darunter fällt insbesondere die Bestimmung der Materialzusammensetzung, der Kristallstruktur, der Phasen und der Realstruktur (z.B. Gitterkonstanten, Orientierungen, Eigenspannungen, Versetzungsdichten, Strukturdefekte) sowie weiterer werkstoffrelevanter Größen an Proben und Bauteilen. Der inhaltliche Zugang erfolgt wahlweise über die Anwendungsgebiete mit zugehörigen Verfahren oder über die Übersicht nach Verfahrensgruppen. In komprimierter Form werden die einzelnen Methodenbeschreibungen nach Anwendungen, Funktionsprinzip, Leistungsprofil und Probenpräparation untergliedert sowie mit jeweils typischen Instrumentierungs- und Applikationsbeispielen komplettiert.Das Kompendium bietet einen ersten Einstieg zur effektiven und zielsicheren Auswahl werkstoffdiagnostischer Methoden.

Retaining its proven concept, the second edition of this ready reference specifically addresses the need of materials engineers for reliable, detailed information on modern material characterization methods. As such, it provides a systematic overview of the increasingly important field of characterization of engineering materials with the help of neutrons and synchrotron radiation. The first part introduces readers to the fundamentals of structure-property relationships in materials and the radiation sources suitable for materials characterization. The second part then focuses on such characterization techniques as diffraction and scattering methods, as well as direct imaging and tomography. The third part presents new and emerging methods of materials characterization in the field of 3D characterization techniques like three-dimensional X-ray diffraction microscopy. The fourth and final part is a collection of examples that demonstrate the application of the methods introduced in the first parts to problems in materials science. With thoroughly revised and updated chapters and now containing about 20% new material, this is the must-have, in-depth resource on this highly relevant topic.

The engineering of materials with advanced features is driving the research towards the design of innovative materials with high performances. New materials often deliver the best solution for structural applications, precisely contributing towards the finest combination of mechanical properties and low weight. The mimicking of nature's principles lead to a new class of structural materials including biomimetic composites, natural hierarchical materials and smart materials. Meanwhile, computational modeling approaches are the valuable tools complementary to experimental techniques and provide significant information at the microscopic level and explain the properties of materials and their very existence. The modeling also provides useful insights to possible strategies to design and fabricate materials with novel and improved properties. The book brings together these two fascinating areas and offers a comprehensive view of cutting-edge research on materials interfaces and technologies the engineering materials. The topics covered in this book are divided into 2 parts: Engineering of Materials, Characterizations & Applications and Computational Modeling of Materials. The chapters include the following: Mechanical and resistance behavior of structural glass beams Nanocrystalline metal carbides - microstructure characterization SMA-reinforced laminated glass panel Sustainable sugarcane bagasse cellulose for papermaking Electrospun scaffolds for cardiac tissue engineering Bio-inspired composites Density functional theory for studying extended systems First principles based approaches for modeling materials Computer aided materials design Computational materials for stochastic electromagnets Computational methods for thermal analysis of heterogeneous materials Modelling of resistive bilayer structures Modeling tunneling of superluminal photons through Brain Microtubules Computer aided surgical workflow modeling Displaced multiwavelets and splitting algorithms

Materials Characterization Using Nondestructive Evaluation (NDE) Methods discusses NDT methods and how they are highly desirable for both long-term monitoring and short-term assessment of materials, providing crucial early warning that the fatigue life of a material has elapsed, thus helping to prevent service failures. Materials Characterization Using Nondestructive Evaluation (NDE) Methods gives an overview of established and new NDT techniques for the characterization of materials, with a focus on materials used in the automotive, aerospace, power plants, and infrastructure construction industries. Each chapter focuses on a different NDT technique and indicates the potential of the method by selected examples of applications. Methods covered include scanning and transmission electron microscopy, X-ray microtomography and diffraction, ultrasonic, electromagnetic, microwave, and hybrid techniques. The authors review both the determination of microstructure properties, including phase content and grain size, and the determination of mechanical properties, such as hardness, toughness, yield strength, texture, and residual stress. Gives an overview of established and new NDT techniques, including scanning and transmission electron microscopy, X-ray microtomography and diffraction, ultrasonic, electromagnetic, microwave, and hybrid techniques Reviews the determination of microstructural and mechanical properties Focuses on materials used in the automotive, aerospace, power plants, and infrastructure construction industries Serves as a highly desirable resource for both long-term monitoring and short-term assessment of materials

This book focuses on robust characterization and prediction methods for materials in technical applications as well as the materials'safety features during operation. In particular, it presents methods for reliably predicting material properties, an aspect that is becoming increasingly important as engineering materials are pushed closer and closer to their limits to boost the performance of machines and structures. To increase their engineering value, components are now designed under the consideration of their multiphysical properties and functions, which requires much more intensive investigation and characterization of these materials. The materials covered in this monograph range from metal-based groups such as lightweight alloys, to advanced high-strength steels and modern titanium alloys. Furthermore, a wide range of polymers and composite materials (e.g. with micro- and nanoparticles or fibres) is covered. The book explores methods for property prediction from classical mechanical characterization-related fields of application, for example, from wear, creep, fatigue and crack growth, to specific surface properties, to dielectric and electrochemical values. As in all fields of modern engineering, the process is often accompanied by numerical simulation and optimization.

Strong bonds form stronger materials. For this reason, the investigation on thermal degradation of materials is a significantly important area in research and development activities. The analysis of thermal stability can be used to assess the behavior of materials in the aggressive environmental conditions, which in turn provides valuable information about the service life span of the materiel. Unlike other books published so far that have focused on either the fundamentals of thermal analysis or the degradation pattern of the materials, this book is specifically on the mechanism of degradation of materials. The mechanism of rapturing of chemical bonds as a result of exposure to high-temperature environment is difficult to study and resulting mechanistic pathway hard to establish. Limited information is available on this subject in the published literatures and difficult to excavate. Chapters in this book are contributed by the experts working on thermal degradation and analysis of the wide variety of advanced and traditional materials. Each chapter discusses the material, its possible application, behavior of chemical entities when exposed to high-temperature environment and mode and the mechanistic route of its decomposition. Such information is crucial while selecting the chemical ingredients during the synthesis or development of new materials technology.

This book covers novel research results for process and techniques of materials characterization for a wide range of materials. The authors provide a comprehensive overview of the aspects of structural and chemical characterization of these materials. The articles contained in this book covers state of the art and experimental techniques commonly used in modern materials characterization. The book includes theoretical models and numerous illustrations of structural and chemical characterization properties.

This book provides a comprehensive presentation of the concepts, properties, and applications of classical materials. It also provides the first unified treatment for the broad subject of classical materials. The authors use a fundamental approach to define the structure and properties of a wide range of solids on the basis of the local chemical bo

This book, which is a result of a coordinated effort by 22 researchers from five different countries, addresses the methods of determining the local and global mechanical properties of a variety of materials: metals, plastics, rubber, and ceramics. The first chapter treats nanoindentation techniques comprehensively. Chapter 2 concerns polymer surfa

This book offers a comprehensive presentation of the concepts, properties, and applications of complex materials. Authors of each chapter use a fundamental approach to define the structure and properties of a wide range of solids on the basis of the local chemical bonding and atomic order present in the material. Emphasizing the physical and chemical origins of different material properties, this important volume focuses on the most technologically important materials being utilized and developed by scientists and engineers.

Practical Materials Characterization covers the most common materials analysis techniques in a single volume. It stands as a quick reference for experienced users, as a learning tool for students, and as a guide for the understanding of typical data interpretation for anyone looking at results from a range of analytical techniques. The book includes analytical methods covering microstructural, surface, morphological, and optical characterization of materials with emphasis on microscopic structural, electronic, biological, and mechanical properties. Many examples in this volume cover cutting-edge technologies such as nanomaterials and life sciences.

Due to their continuing role in electricity generation, it is important that coal power plants operate as efficiently and cleanly as possible. Coal Power Plant Materials and Life Assessment reviews the materials used in coal plants, and how they can be assessed and managed to optimize plant operation. Part I considers the structural alloys used in coal plants. Part II then reviews performance modelling and life assessment techniques, explains the inspection and life-management approaches that can be adopted to optimize long term plant operation, and considers the technical and economic issues involved in meeting variable energy demands. Summarizes key research on coal-fired power plant materials, their behavior under operational loads, and approaches to life assessment and defect management Details the range of structural alloys used in coal power plants, and the life assessment techniques applicable to defect-free components under operational loads Reviews the life assessment techniques applicable to components containing defects and the approaches that can be adopted to optimize plant operation and new plant and component design

Voids in Materials treats voids of different shapes and forms in various materials, and examines their effects on material properties. The book covers the origins of voids in materials, how they are sometimes introduced in the form of hollow spheres, and the resultant properties of materials containing voids. There are many books that focus on foams (which intentionally incorporate voids into materials) and that cover voids incidental to or unwanted in the fabrication of non-porous materials. In fact, all materials have voids. This book starts from the premise that voids are pervasive in all material on some level. It goes beyond foams to provide a comprehensive overview of voids, a central reference for scientists and engineers to use for the effect of voids in materials. Includes 3D renderings of void geometries Explains how and why voids are introduced into materials across the length scales; from nanometer-scale voids up to macro-scale voids Provides a continuous picture of how material properties change as the volume fraction of voids increases, and the implications for product design

This volume examines important experimental techniques needed to characterise inorganic materials in order to elucidate their properties for practical application. Addressing methods that examine the structures and properties of materials over length scales ranging from local atomic order to long-range order on the meso- and macro-scopic scales, Multi Length-Scale Characterisation contains five detailed chapters: Measurement of Bulk Magnetic Properties Thermal Methods Atomic Force Microscopy Gas Sorption in the Analysis of Nanoporous Solids Dynamic Light Scattering Ideal as a complementary reference work to other volumes in the series (Local Structural Characterisation and Structure from Diffraction Methods) or as an examination of the specific characterisation techniques in their own right, Multi Length-Scale Characterisation is a valuable addition to the Inorganic Materials Series.

A comprehensive review of ion beam application in modern materials research is provided, including the basics of ion beam physics and technology. The physics of ion-solid interactions for ion implantation, ion beam synthesis, sputtering and nano-patterning is treated in detail. Its applications in materials research, development and analysis, developments of special techniques and interaction mechanisms of ion beams with solid state matter result in the optimization of new material properties, which are discussed thoroughly. Solid-state properties optimization for functional materials such as doped semiconductors and metal layers for nano-electronics, metal alloys, and nano-patterned surfaces is demonstrated. The ion beam is an important tool for both materials processing and analysis. Researchers engaged in solid-state physics and materials research, engineers and technologists in the field of modern functional materials will welcome this text.

Now in its second edition, this continues to serve as an ideal textbook for introductory courses on materials characterization, based on the author's experience in teaching advanced undergraduate and postgraduate university students. The new edition retains the successful didactical concept of introductions at the beginning of chapters, exercise questions and an online solution manual. In addition, all the sections have been thoroughly revised, updated and expanded, with two major new topics (electron backscattering diffraction and environmental scanning electron microscopy), as well as fifty additional questions - in total about 20% new content. The first part covers commonly used methods for microstructure analysis, including light microscopy, X-ray diffraction, transmission and scanning electron microscopy, as well as scanning probe microscopy. The second part of the book is concerned with techniques for chemical analysis and introduces X-ray energy dispersive spectroscopy, fluorescence X-ray spectroscopy and such popular surface analysis techniques as photoelectron and secondary ion mass spectroscopy. This section concludes with the two most important vibrational spectroscopies (infra-red and Raman) and the increasingly important thermal analysis. The theoretical concepts are discussed with a minimal involvement of mathematics and physics, and the technical aspects are presented with the actual measurement practice in mind. Making for an easy-to-read text, the book never loses sight of its intended audience.

A complete and comprehensive theory of failure is developed for homogeneous and isotropic materials. The full range of materials types are covered from very ductile metals to extremely brittle glasses and minerals. Two failure properties suffice to predict the general failure conditions under all states of stress. With this foundation to build upon, many other aspects of failure are also treated, such as extensions to anisotropic fiber composites, cumulative damage, creep and fatigue, and microscale and nanoscale approaches to failure.

The principal aim of this book is to provide the reader with the understanding of the possibilities and features of THz identification as opposed to more traditional techniques such as X-rays, microwaves, etc. by elucidating and illustrating the principles of THz identification and its applications in a systematical way. Its scope includes a description of the physical principles of THz generation, transmission and detection, as well as of the applications of THz identification.The inherent advantages and potential benefits of the terahertz (THz) phenomenon, potential that encompasses various aspects such as THz sensing, imaging and material properties investigation with THz radiation for Defense (military) and security applications serve as an important stimulus for the interest in emerging THz science and technology, in particular, the very rapid growth of this new field.This text presents some of the leading fundamental research efforts towards the realization of practical THz devices applications for military and security applications. Relevant chapters contain fundamentals and/or measurements of THz radiation in solid-state materials such as high explosives (e.g. HMX, PETN, RDX, etc.), biological tissues and organic-semiconductor nanostructures. Individual chapters also address the present capabilities of THz equipment for the effective utilization of screening packages and personnel. This book contains descriptions and analyses of the most innovative research in the field; the presented material introduces novel devices and/or concepts that enhance THz source and detector performance — enabling completely new types of sensor performance at THz frequency (e.g. detection at molecular and nanoscale levels), and defining innovative sensing modalities (e.g. remote object and personnel identification) for defense and security.

Special topic volume with invited peer reviewed papers only.

The extensive use of low-energy accelerators in non-nuclear physics has now reached the stage where these activities are recognized as a natural field of investigation. Many other areas in physics and chemistry have undergone similarly spectacular development: beam foil spectroscopy in atomic physics, studies in atomic collisions, materials implantation, defects creation, nuclear microanalysis, and so on. Now, this most recent activity by itself and in its evident connec­ tion with the others has brought a new impetus to both the funda­ mental and the applied aspects of materials science. A summer school on'Material Characterization Using Ion Beams'has resulted from these developments and the realization that the use of ion beams is not restricted to accelerators but covers a wide energy range in the developing technology. The idea of the ion beam as a common denominator of many act1v1t1es dealing with surface and near-surface characterization was enthu­ siastically received by many scientists and a school on this subject received the positive endorsement of NATO. The Advanced Study Institute on Materials Science has assumed for us the status of an'institution'leading to better contact among the many laboratories engaged in this field. The fourth Institute in this series was held in Aleria, Corsica, between August 22 and September 12, 1976.

A technique that is useful in the study of pharmaceutical products and biological molecules, polarization IR spectroscopy has undergone continuous development since it first emerged almost 100 years ago. Capturing the state of the science as it exists today, Linearly Polarized IR Spectroscopy: Theory and Applications for Structural Analysis demonstrates how the technique can be properly utilized to obtain important information about the structure and spectral properties of oriented compounds. The book starts with the theoretical basis of linear-dichroic infrared (IR-LD) spectroscopy and then moves on to examine the background of the orientation method of colloid suspensions in a nematic host. It explores the orientation procedure itself, experimental design, and mathematical tools for the interpretation of the IR spectroscopic patterns. Next, the authors describe the structural elucidation of inorganic and organic compounds and glasses. Finally, they discuss applications in pharmaceutical analysis and the chemistry of dyes. Filled with more than 140 illustrations along with a color insert, the book explains both the scope of the polarized IR spectroscopy method as well as its limitations. A powerful source of information not only for specialists in IR spectroscopy, but also for those working in the field of structural analysis, this volume moves the field closer to developing an inherently classical method for the structural characterization of compounds.

Be­triebs­fes­tig­keit be­deu­tet die si­che­re Be­mes­sung von Bau­tei­len un­ter re­a­lis­ti­schen Um­ge­bungs­be­din­gun­gen mit dem Ziel Leicht­bau. Im Mit­tel­punkt steht die Schwing­be­an­spru­chung. Bei der Be­mes­sung wird die zu erwartende Be­an­spru­chung (Be­las­tung) mit der Be­an­spruch­bar­keit (Fes­tig­keit) verglichen, wo­bei die für den An­wen­dungs­fall not­wen­di­ge Si­cher­heit ge­währ­leis­tet wer­den muss. Vo­raus­set­zung für die be­triebs­fes­te Be­mes­sung ist eine zu­ver­läs­si­ge Last­an­nah­me. Die Autoren stellen dar, wie die im Be­trieb ge­mes­se­nen Be­an­spru­chungs­zeit­funk­ti­o­nen durch Zähl­ver­fah­ren in Kol­lek­ti­ve oder Ma­tri­zen trans­for­miert wer­den kön­nen. Aus­führ­lich be­han­delt wird, wel­che As­pek­te zu be­ach­ten sind, um eine zu­ver­läs­si­ge Last­an­nah­me für die Be­mes­sung si­cher­zu­stel­len. Dazu wird ein­mal der the­o­re­ti­sche Hin­ter­grund der Le­bens­dau­er­ab­schät­zung von Bau­tei­len er­läu­tert, zum an­de­ren wer­den die Vor­ge­hens­wei­sen in zahl­rei­chen tech­ni­schen An­wen­dungs­fäl­len dis­ku­tiert. Für die Pra­xis um­setz­ba­re Emp­feh­lun­gen zu ge­ben, ist ein we­sent­li­ches An­lie­gen der Au­to­ren.

This book presents reviews of various aspects of radiation/matter interactions, be these instrumental developments, the application of the study of the interaction of X-rays and materials to a particular scientific field, or specific methodological approaches. The overall aim of the book is to provide reference summaries for a range of specific subject areas within a pedagogical framework. Each chapter is written by an author who is well known within their field and who has delivered an invited lecture on their subject area as part of the “RX2009 – X-rays and Materials” colloquium that took place in December 2009 at Orsay in France. The book consists of five chapters on the subject of X-ray diffraction, scattering and absorption. Chapter 1 gives a detailed presentation of the capabilities and potential of beam lines dedicated to condensed matter studies at the SOLEIL synchrotron radiation source. Chapter 2 focuses on the study of nanoparticles using small-angle X-ray scattering. Chapter 3 discusses the quantitative studies of this scattering signal used to analyze these characteristics in detail. Chapter 4 discusses relaxor materials, which are ceramics with a particularly complex microstructure. Chapter 5 discusses an approach enabling the in situ analysis of these phase transitions and their associated microstructural changes.