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Nanocellulose of different morphologies was extracted from Sunn Hemp (Crotalaria Juncea) using acid hydrolysis. The work focused on two objectives: first, to valorize the Sunn Hemp fibers for nanocellulose (NC) production, and second, to study the effects of acid concentration on different morphologies of NC and their properties. The study extracted nanocellulose at five different concentrations of H 2 SO 4 : 16 %, 32 %, 48 %, 64 %, and 72 %. Obtained nanocellulose was characterized by Scanning Electron Microscopy (FE-SEM), Atomic Force Microscopy (AFM), Fourier Transform Infrared Spectroscopy (FTIR), X-ray Diffraction (XRD) and Thermogravimetric Analysis (TGA). AFM and FE-SEM confirmed the production of three different morphologies of nanocellulose. The NC-32 had a web-like structure typically observed for cellulose nanofibrils (CNF), whereas NC-48 and NC-64 were observed as cellulose nanocrystals (CNC) with rod-like and needle-like shapes, respectively, and NC-72 displayed spherical particles termed cellulose nanospheres (CNS). The total crystallinity index of NC was calculated using FTIR, and a similar trend of crystallinity was also observed from XRD analysis. NC-32 was obtained with the highest yield of 94.83 %, followed by 91.40 % and 81.70 % for NC-48 and NC-64, respectively, whereas NC-72 yielded the lowest yield of 12.03 %. NC-72 had the highest thermal stability among other NC morphologies., Competing Interests: Declaration of competing interest The authors declare that there are no conflicts of interest., (Copyright © 2023 Elsevier B.V. All rights reserved.)

Agricultural waste residues (agro-waste) are the source of carbohydrates that generally go in vain or remain unused despite their interesting morphological, chemical, and mechanical properties. With rapid urbanization, there is a need to valorize this waste due to limited non-renewable resources. Utilizing agro-waste also prevents the problems like burning and inefficient disposal that otherwise lead to immense pollution worldwide. In addition, conversion of biomass to value-added products like earthen cups, weaving baskets, and bricks is equally beneficial for the rural population as it provides secondary income, creates jobs, and improves rural people's lifestyles. This review paper will discuss an overview of different applications utilizing agro-waste residues. In particular, agro-wastes used as construction material, bio-fertilizers, pulp and paper products, packaging products, tableware, heating applications, biocomposites, nano-cellulosic materials, soil stabilizers, bioplastics, fire-retardant additive, dye removal, and biofuels will be summarized. Finally, several commercially available agro-waste products will also be discussed, emphasizing the circular economy., (© 2022. The Author(s), under exclusive licence to Springer-Verlag GmbH Germany, part of Springer Nature.)

An increase in population compels the textile industry to expand production to fulfill the apparel requirement, resulting in huge textile waste. These wastes are managed either by landfilling or incineration processes, which negatively contribute to the environment. Converting waste into value-added products is essential to reducing environmental pollution and thereby achieving a circular economy through proper waste management practices. This paper provides a comprehensive overview of different categories and forms of textile waste, their source of generation, the reusing capability of the textile industry, other valorization potentials in different fields, and various challenges associated with their valorization practices. This review presents textile wastes as the raw material source for preparing different value-added products such as in manufacturing textiles, packaging materials, plastics, composites, construction applications, energy generation, chemical additives, composting, and several other applications., (© 2022. The Author(s), under exclusive licence to Springer-Verlag GmbH Germany, part of Springer Nature.)