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Additive manufacturing has the potential to repair damaged parts, but the performance of additive materials under high strain rate loading is still uncertain—especially with the added complexity of an interface with an existing wrought material. In this work, 304L stainless steel samples were intentionally damaged and then repaired with wire-fed laser additive manufacturing. The samples were subjected to shock loading to generate incipient spall. Velocimetry and post-mortem metallography results show that when the additive repair process parameters are optimized to reduce porosity and match the equation of state of the original material, the influence of the repair region on the shock propagation is negligible. The free-surface velocity profile and internal damage morphology of the repaired sample are shown to be practically identical to the pristine material. [ABSTRACT FROM AUTHOR]

Copyright of BHM Berg- und Hüttenmännische Monatshefte is the property of Springer Nature and its content may not be copied or emailed to multiple sites or posted to a listserv without the copyright holder's express written permission. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract. (Copyright applies to all Abstracts.)

Copyright of BHM Berg- und Hüttenmännische Monatshefte is the property of Springer Nature and its content may not be copied or emailed to multiple sites or posted to a listserv without the copyright holder's express written permission. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract. (Copyright applies to all Abstracts.)

The EN AB-46000 alloy castings are widely used in automotive industry due to their relative good strength combined with a low density and an excellent conductivity. Porosity of EN AB-46000 alloys is one of the most important defects, responsible for the low strength and poor plastic properties of castings as well as their tightness. Quantitative porosity measurement were performed using quantitative metallography and image analysis methods using ImageJ. The study shows that such parameters of high-pressure die casting are the piston speed in the second casting phase and the final pressure increase in the pressing phase. It has been shown that the appropriate selection of these parameters can significantly reduce the porosity of castings made of alloy EN AB-46000. [ABSTRACT FROM AUTHOR]

As anthropogenic activities have facilitated the spread of heavy metals into the environment, plants have been identified that may have the ability to tolerate exposure to high levels of these metals. Industrial hemp (Cannabis sativa L.) has been suggested as potentially having the ability to accumulate elevated concentrations of some contaminants from soils, including cadmium (Cd), a heavy metal that has been linked to serious health risks to humans. Therefore, there is an interest to document the ability of hemp to tolerate exposure to Cd to determine if there is a risk when products for medicinal consumption are made from the hemp plant. The objectives of this study were to perform histochemical localization of Cd at the cellular level and document potential changes in plant tissues in response to hemp exposure. Plants were grown in hydroponic solutions for 4 weeks and then exposed to either 0 or 10 mg·L-1 Cd for 17 days and harvested. There were no differences in dry weights (dw) of leaves, stems, and roots among treated and control 17 days after treatment (DAT). However, plants exposed to 10 mg·L-1 Cd had Cd concentrations of 1448.0 mg·kg-1 dw in roots and 23.2 mg·kg-1 dw in leaves at 17 DAT, whereas Cd was not detected in roots or leaves of control plants. On staining with dithizone, Cd was primarily localized in leaf epidermis, mesophyll, and trichomes, and in root rhizodermis, cortex, and pericycle in hemp plants exposed to 10 mg·L-1 Cd. Image analysis was able to further quantify these results based on area stained. Our results suggest that Cd is primarily accumulated throughout hemp roots, with lesser amounts translocated to the leaves, where it may be localized in the epidermis and trichomes. [ABSTRACT FROM AUTHOR]

Liquid metals (LMs) are emerging as unique fluids for a variety of applications, but their nanoscale solvation properties remain largely understudied. In this work, a combination of atomic force microscopy (AFM) and molecular dynamics (MD) simulations are used to investigate the structure of the interface between the bulk room temperature liquid metal (RTLM) and the LM oxide in nanodroplet systems of gallium, EGaIn (75.5% gallium, 24.5% indium), and Galinstan (68.5% gallium, 21.5% indium, 10% tin). Field's metal (51% indium, 32.5% bismuth, 16.5% tin) is also investigated, which melts at ≈62 °C, as a contrast to the other systems. AFM measurements reveal distinct sub‐oxide nanostructured layering in all three RTLM systems, and Field's metal above the melting point, to differing degrees. EGaIn and Galinstan show multiple penetration events between 20 and 30 nm, with smaller, less complex events in Ga. MD simulations suggest that this layering is a result of the near‐surface ordering of LM atoms beneath the oxide layer. Importantly, the atoms in this region do not behave as solids but are more ordered than in a pure disordered liquid system. The surface nanostructure elucidated here significantly expands the understanding of LM systems and their behavior at interfaces. [ABSTRACT FROM AUTHOR]

The additive manufacturing (AM) is a relative new manufacturing process that belongs to the fourth industrial revolution, thus yielding new challenges that are worth the study in terms of reliability. In that sense, this work presents a comparative study of as printed and optimally heat-treated 1.2709 maraging steel manufactured by laser powder bead fusion (LPBF) AM process. The results suggest that parts were sound in terms of visual inspection and microstructural analysis. In the case of mechanical properties, the results suggest that the highest variability occurred after the heat treatment. The high cycle fatigue samples revealed a fracture without exhibiting a considerable amount of plastic deformation. On the other hand, the low cycle fatigue results revealed that at 1% strain the optimally heat-treated specimens have lower fatigue life due to the presence of surface discontinuities and the reduction of ductility after the heat treatment. [ABSTRACT FROM AUTHOR]

This article presents researches conducted on samples obtained by micro alloying aluminum alloys with germanium oxide. Experiments were carried out on aluminum-magnesium, aluminum-copper and aluminum-manganese aluminum alloys, and the hardness and microstructure of the samples obtained by casting were studied. The samples were melted in the open air in a resistance furnace and poured into sand-clay molds. Germanium oxide was added to the charge in a rolled state using a special aluminum coating. Depending on the weight of the charge and the oxide's germanium concentration, between 0.1 and 0.3 percent of germanium oxide was added to aluminum alloys. An optical metallographic microscope was used for microscopic analysis of cast samples. Studies have shown that the germanium addition significantly destroys the microstructure of an aluminum alloy with intermetallic granules. Moreover, the hardness of the researched samples was studied. The authors outlined their recommendations and conclusions at the end of the article. [ABSTRACT FROM AUTHOR]

One of the most frequent causes of coal fired power plant shutdown is boiler tube leak. Superheaters are crucial components of boilers operating under high temperatures and pressures. Understanding the superheater potential damages is essential to define the rectification action needed to keep and elevate overall power plant productivity. This paper highlights the analysis of platen superheater tube failure in a 2x150 MW coal-fired power plant in South Sumatera. Various test including chemical composition, hardness, tensile, metallography, SEM fracture surface examination, and XRD compound analysis were conducted for investigation purposed. The failure was initiated by the plugging of the tube elbow due to deposits and ashes adhering to the tube's interior. This obstruction prevented saturated steam flow inside the tube, leading to overheating and a subsequent drop in mechanical strength. Overheating was confirmed by the presence of spheroid particles in the ferrite matrix. Prolonged overheating resulted in the formation of microvoids, leading to creep failure and crack formation in the tube. The improvements made by adding refractory material give positive results. The platen superheater tubes which previously exceeded temperature limits, currently operate within normal range temperatures, reduced spray water consumption 6-10 tons/day, and significantly increased boiler efficiency from 83.19% to 83.54%. [ABSTRACT FROM AUTHOR]

This study explores the microstructural characterization of pearlite phase transformation in high-strength low-alloy API X60 steel, which is used in pipelines. Understanding the formation, phase percentages, and morphology of the pearlitic phase is crucial since it affects the mechanical properties of the considered steel. In this research, a phase-field model, particularly the Cahn-Hilliard approach, was used in order to simulate the formation and morphology of the pearlite phase in response to different heat treatments. Both double- and triple-well potentials were considered for comprehensively studying pearlite's morphology in the simulations. The simulation results were then compared with experimental outcomes obtained by metallography and field-emission scanning electron microscopy analyses. Considering the doublewell potential can help simulate only two phases, ferrite and cementite, which is less compatible with the experiment results than the triple-well potential, which gives the possibility of simulating a three-phase microstructure, ferrite, cementite, and austenite, and a better match with experimental data. The study revealed that as the cooling rate increases, the interlamellar spacing and layer thickness decrease. Additionally, the difference between experimental and simulation results using triple-well potential was approximately ~10%. Therefore, triple-well potential formulation predictions have better agreements with experimental results for the development circumstance of pearlitic structures. [ABSTRACT FROM AUTHOR]

The EN AB-46000 alloy castings are widely used in automotive industry due to their relative good strength combined with a low density and an excellent conductivity. Porosity of EN AB-46000 alloys is one of the most important defects, responsible for the low strength and poor plastic properties of castings as well as their tightness. Quantitative porosity measurement were performed using quantitative metallography and image analysis methods using ImageJ. The study shows that such parameters of high-pressure die casting are the piston speed in the second casting phase and the final pressure increase in the pressing phase. It has been shown that the appropriate selection of these parameters can significantly reduce the porosity of castings made of alloy EN AB-46000.

• The waste-with-waste treatment is used to successfully remove heavy metals from slag. • Separation at high-temperature with Si-Cu additives recovered more than 90% of metals. • EPMA analyses allowed for quantifiable comparisons of all elements present in slag. • Concentrations of heavy metals reduced from 2400 ppm to 41.7 ppm in the remaining slag. The smelting processes account for over 80 % of global copper production, generating various slags in large quantities. Most of these slags do not contain the required amounts of valuable metals to justify economic revalorization, yet the concentrations present may negatively affect the environment. In this study, heavy and potentially toxic metals were removed by keeping the liquefied slag at 1300 °C for four hours, while the metals gathering was enhanced by adding silicon-copper compounds. Crystallography, metallography, gravimetric, thermogravimetric, and differential thermal analysis were employed to characterize the slag. Electron probe microanalysis was utilized to examine the distribution of heavy and potentially toxic metals from the original copper slag to the remaining slag and mattes formed in the lower portion of the containing vessel. In all instances, concentrations of the arsenic and zinc were reduced below the detection limit. Moreover, the cumulative concentrations of six heavy metals were reduced from 2400 ppm in the initial slag to 41.7 ppm in the remaining slag when using 30 wt%Si70wt%Cu additive. All potentially valuable or toxic metals gathered in the mattes that had oxygen concentrations about 50 times lower than in the initial slag, at 0.82, 0.56, and 0.68 wt% after the mixing slag with 10 wt%Si90%Cu, 30 wt%Si70wt%Cu, and 50 wt%Si50wt%Cu additives, respectively. Investigated practices can mitigate the threat of heavy and potentially toxic metals associated with the disposal of copper slags while also enabling the recovery of valuable metals and rendering the remaining slag suitable for construction or mine backfill purposes. [ABSTRACT FROM AUTHOR]

The upcoming energy transition requires not only renewable energy sources but also novel electricity storage systems such as batteries. Despite Li-ion batteries being the main storage systems, other batteries have been proposed to fulfil the requirements on safety, costs, and resource availability. Moving away from lithium, materials such as sodium, magnesium, zinc, and calcium are being considered. Water-based electrolytes are known for their improved safety, environmentally friendliness, and affordability. The key, however, is how to utilize the negative metal electrode, as using water-based electrolytes with these metals becomes an issue with respect to oxidation and/or dendrite formation. This work studied magnesium, where we aimed to determine if it can be electrochemically deposited in aqueous solutions with alginate-based additives to protect the magnesium. In order to do so, atomic force microscopy was used to research the morphological structure of magnesium deposition at the local scale by using a probe—the tip of a cantilever—as the active electrode, during charging and discharging. The second goal of using the AFM probe technology for magnesium deposition and stripping was an extension of our previous study in which we investigated, for lithium, whether it is possible to measure ion current and perform nonfaradaic impedance measurements at the local scale. The work presented here shows that this is possible in a relatively simple way because, with magnesium, no dendrite formation occurs, which hinders the stripping process. [ABSTRACT FROM AUTHOR]

Hastinapur is one of the prominent painted grey ware archaeological sites in the Ganga Valley. In the present communication, we report the results of the metallurgical analysis of the excavated slag samples from the site. The existence of a large number of iron objects for this site can be dated between c. 6th century BCE and c. 16th century CE, with early iron from the 8th century BCE. The morphological, microstructural and elemental studies of the excavated slag indicate a high amount of carbon in iron, indicating crucible carburization activities at this site. In addition, the presence of niobium, cobalt, etc. in the slag indicates the usage of non-traditional iron ores in the primary ironmaking stage. [ABSTRACT FROM AUTHOR]

An in-depth understanding of the fracture behavior and mechanism of metallic shells under internal explosive loading can help develop material designs for warheads and regulate the quantity and mass distribution of the fragments formed. This study investigated the fragmentation performance of a new high-carbon silicon-manganese (HCSiMn) steel cylindrical shell through fragment recovery experiments. Compared with the conventional 45Cr steel shell, the number of small mass fragments produced by the HCSiMn steel shell was significantly increased with a scale parameter of 0.57 g fitted by the Weibull distribution model. The fragmentation process of the HCSiMn shell exhibited more brittle tensile fracture characteristics, with the microcrack damage zone on the outer surface being the direct cause of its high fragmentation. On the one hand, the doping of alloy elements resulted in grain refinement by forming metallographic structure of tempered sorbite, so that microscopic intergranular fracture reduces the characteristic mass of the fragments; on the other hand, the distribution of alloy carbides can exert a "pinning" effect on the substrate grains, causing more initial cracks to form and propagate along the brittle carbides, further improving the shell fragmentation. Although the killing power radius for light armored vehicles was slightly reduced by about 6%, the dense killing radius of HCSiMn steel projectile against personnel can be significantly increased by about 26% based on theoretical assessment. These results provided an experimental basis for high fragmentation warhead design, and to some extent, revealed the correlation mechanism between metallographic structure and shell fragmentation. [ABSTRACT FROM AUTHOR]

This study presents a microstructural investigation of the printing parameters of an AlSi7Mg0.6 alloy produced by powder bed fusion (PBF) using laser beam melting (LB/M) technology. The investigation focused on the effects of laser power, exposure velocity, and hatching distance on the microhardness, porosity, and microstructure of the produced alloy. The microstructure was characterized in the plane of printing on a confocal microscope. The results showed that the printing parameters significantly affected the microstructure, whereas the energy density had a major effect. Decreasing the laser power and decreasing the hatching distance resulted in increased porosity and the increased participation of non-melted particles. A mathematical model was created to determine the porosity of a 3D-printed material based on three printing parameters. Microhardness was not affected by the printing parameters. The statistical model created based on the porosity investigation allowed for the illustration of the technological window and showed certain ranges of parameter values at which the porosity of the produced samples was at a possible low level. [ABSTRACT FROM AUTHOR]

The foundation of materials science and engineering is the establishment of process–microstructure–property links, which in turn form the basis for materials and process development and optimization. At the heart of this is the characterization and quantification of the material's microstructure. To date, microstructure quantification has traditionally involved a human deciding what to measure and included labor-intensive manual evaluation. Recent advancements in artificial intelligence (AI) and machine learning (ML) offer exciting new approaches to microstructural quantification, especially classification and semantic segmentation. This promises many benefits, most notably objective, reproducible, and automated analysis, but also quantification of complex microstructures that has not been possible with prior approaches. This review provides an overview of ML applications for microstructure analysis, using complex steel microstructures as examples. Special emphasis is placed on the quantity, quality, and variance of training data, as well as where the ground truth needed for ML comes from, which is usually not sufficiently discussed in the literature. In this context, correlative microscopy plays a key role, as it enables a comprehensive and scale-bridging characterization of complex microstructures, which is necessary to provide an objective and well-founded ground truth and ultimately to implement ML-based approaches. [ABSTRACT FROM AUTHOR]

2219-T87 is a precipitation hardenable aluminum-copper alloy which sees wide use in structural aerospace components. Thick panels of this alloy are joined via self-reacting friction welding (SRFSW); however, this thermomechanical process can result in significant loss of the alloy's strengthening precipitates and large residual stresses which are detrimental to mechanical behavior and performance. High-resolution maps of the residual strain and stress states along the normal, transverse, and longitudinal directions of 2219-T87 SRFSW were obtained using neutron diffraction measurements. Residual stress had the highest tensile value in the heat-affected zone (HAZ) and the largest compressive stress in the base metal region of the normal and transverse directions. Line profile residual stress distributions displayed an "M"-shaped distribution in each direction with the longitudinal direction being the most pronounced while 2D residual stresses displayed an hourglass-shaped pattern. Average maximal longitudinal residual stress values ranged from 60.6 to 85.6% of yield. Microhardness testing across the transverse weld section produced a "V"-shaped curve with slight hardness recovery in the stir zone. Maximal and minimal microhardness values were observed in the base metal (154 HV) and thermomechanically affected zone (82 HV), respectively. Microstructural evolution was recorded using optical microscopy and showed decreasing grain size from the HAZ to the stir zone. [ABSTRACT FROM AUTHOR]

Copyright of Chemical Industry / Hemijska Industrija is the property of Association of Chemical Engineers and its content may not be copied or emailed to multiple sites or posted to a listserv without the copyright holder's express written permission. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract. (Copyright applies to all Abstracts.)

An experimental metallographic method for determining strain distribution in a cold formed workpiece is presented in this paper. The method, based on the dependence of recrystallized grain size on prior deformation, was applied to a bulk formed element made of low carbon steel. Strain distribution was obtained by the calibration curve which gives the relation between recrystallized grain size and prior deformation. To determine strain values, the average grain size was measured in the longitudinal cross-section of the formed element. To accurately differentiate deformation zones, additional observation of carbides and nonmetallic inclusions morphology was utilized, also. The grain size and strain noticeably differ through the cross-section. It is observed that in the middle part, material flows freely through the die opening without significant deformation. From this zone, strain increases gradually, reaching the highest value at the contact surface of the die slope, while the top part flows radially having intermediate values of strain.

This publication presents the chemical compositions of carbon reducers used in the production of ferroalloys, with particular emphasis on the content of Al, Ca, Mg, Mn, Cr, Ti, P, or S in their mineral substances. A certain amount of these elements is transferred to the produced alloys, creating inclusions and precipitations in the metal structure. Most of them are undesirable and adversely affect the final effect of the production process. The work includes sample images of the microstructure of alloys, the chemical compositions of the samples at the test point, and diffragrams. On the basis of the obtained metallographic data, technological observations are made, especially of the crushing process and the amount of grain fractions obtained. [ABSTRACT FROM AUTHOR]

Turbine blades recovered from the Apollo Saturn V rocket F-1 engines were examined to determine an appropriate conservation protocol. Significant corrosion damage was observed in the turbine blades which appear to be made of a nickel based γ–γ′ superalloy. Pitting corrosion appears to have breached the surface of the turbine blades, and subsequently a form of dealloying corrosion preferentially attacked the γ′ phase. This corrosion left behind a thin network of interconnected γ phase, causing a severe loss of density of the blades and fragility of the blades. The particular alloy used for these turbine blades does not appear to be a known production alloy and may have been developed specifically for use in the F-1 rocket engines, with an increased concentration of refractory (Mo, Nb) elemental additions. The analytical results helped conservators determine a suitable treatment protocol for more than 400 blades and 100 fragments from four recovered turbines. [ABSTRACT FROM AUTHOR]

In this study, a decorative electric heater was manufactured to reduce carbon emissions related to residential and office heating, and this heater was metallographically evaluated. In addition, the heating performance of the manufactured plate was investigated by examining its heat transfer capacity by natural convection. For this purpose, the surface of the tempered glass plate was coated with graphene by spraying to improve its electrical and heat conduction properties. Copper strips were attached to both sides of the plate to allow for an electric current. The plate was connected to mains electricity, and its change in surface temperature over time was measured. Using the measured temperature values, the heat transfer rate by natural convection on the plate surface was calculated. As a result of the calculations, it was determined that the graphene-coated tempered glass plate reached a heating performance of 40 watts after 2400 s of electrical energy supply. This value can be increased by increasing the heat transfer surface area. This study, taking advantage of the excellent thermophysical properties of graphene, will contribute to other studies conducted in this field. [ABSTRACT FROM AUTHOR]

An experimental metallographic method for determining strain distribution in a cold formed workpiece is presented in this paper. The method, based on the dependence of recrystallized grain size on prior deformation, was applied to a bulk formed element made of low carbon steel. Strain distribution was obtained by the calibration curve which gives the relation between recrystallized grain size and prior deformation. To determine strain values, the average grain size was measured in the longitudinal cross-section of the formed element. To accurately differentiate deformation zones, additional observation of carbides and nonmetallic inclusions morphology was utilized, also. The grain size and strain noticeably differ through the cross-section. It is observed that in the middle part, material flows freely through the die opening without significant deformation. From this zone, strain increases gradually, reaching the highest value at the contact surface of the die slope, while the top part flows radially having intermediate values of strain. [ABSTRACT FROM AUTHOR]

This article used Mn-Mo-Cr-B low-carbon bainitic steel as the experimental material. The continuous cooling transformation curve of the steel during continuous cooling was determined using a Gleeble-1500D thermal simulation test machine, and a corresponding phase transformation model for bainitic steel during continuous cooling was established. The influence of different cooling rates and final cooling temperatures on the microstructure and mechanical properties of the steel was investigated. Employing metallography, SEM, and EBSD techniques, the microstructure, crystallographic orientation, and grain boundary angle distribution of the low-carbon bainitic steel were explored, and their relationship with the steel's strength and toughness was studied. The research findings reveal that varying cooling rates and final cooling temperatures impact the phase transformation process and microstructure of the steel, consequently affecting its mechanical properties indirectly. With increasing cooling rate, the diffusion and fineness of martensite increase, and the quantity of lath bainite grows while the laths become finer. Elevated final cooling temperatures lead to larger martensiticaustenitic (MA) islands and reduced lath bainite quantity, causing the laths to become wider. Through analysis of the substructure of bainitic steel, it was determined that the bainite organization in the tested steel comprises primary austenite grains, lath packet, and lath block in succession. Lath packets are composed of lath blocks with different orientations, where lath size predominantly controls strength. Finer lath size corresponds to higher strength, and the influence of substructure on toughness is comparatively minor. [ABSTRACT FROM AUTHOR]

The fire at Notre-Dame de Paris led to the discovery of several series of previously unknown iron armatures, which were systematically recorded. Amongst them, several iron staples from the top of the eaves walls, lead crest reinforcements and a sample of the tie rods used in the choir in the 19th century were analysed by metallography and tensile tests in order to determine their nature and mechanical characteristics. These results can be put into perspective with previous studies on such monuments. The chemical analysis with SEM-EDS of the slag inclusions contained in the matrix of these ferrous alloys makes it possible to determine the technical processes used for their production throughout the construction and restoration of the building, highlighting several differences depending on the typologies of the iron armatures. This information is complemented by a series of radiocarbon dates currently being carried out to better understand the periods of use of these ferrous reinforcements. When compared with those of other materials, these dates could be used to recalibrate the phasing of the building. [ABSTRACT FROM AUTHOR]

In this article, mechanical performance testing of 45# carbon steel samples with Ni/Co alloy plasma cladding was conducted through a combination of experiments and numerical simulations. The thickness of the coating of the Ni and Co base has two types of working conditions: 1mm and 0.5mm thick. The differences of the mechanical properties under different cladding thickness of the samples were experimental tested by metallographic analysis, hardness testing, abrasion resistance testing and impact resistance, by which the samples preparation has been confirmed to be essentially qualified. Then, in order to examine the improvement effect of plasma cladding technology on the sand shovel mechanical properties, the two materials were used to simulate the sand collection process of straight blade and bent blade. By analyzing mechanical representation such as stress, strain and fatigue damage, it is found that with the cladding thickness and the shovel shape difference, the force performance of the shovel is relatively different. Therefore, these factors should be comprehensively considered when selecting an appropriate cladding thickness and shovel curve to enhance the performance of the sand shovel during the sand collection process. [ABSTRACT FROM AUTHOR]

Multiple GH4169 samples were prepared with the regulation of the forming process of selective laser melting(SLM), particularly in laser power and scanning speed. The microstructure including defect morphology and distribution was observed by using metallography. The sample porosity was acquired using X-ray computed tomography(XCT), and the three-dimensional characteristics of defect were also statistically studied. The correlation of forming process and defect characteristics was finally analyzed. The results show that when the optimized energy input density is 59.1 J/mm3, the forming samples share common features of overlapping melting trace with a tidy morphology, randomly distributed pores with sizes of less than 30 -m and the density is as high as 99.9998%. Within a narrow window of forming process(220-300 W, 700-1300 mm/s), the scanning speed takes more responsibility for the sample density, and its high value tends to form extremely irregular lack of fusions(LOFs) that distribute in the overlap of melting trace. As deviating from the optimized process, the number of defects has increased, and some defect sizes are also greater than 30 ^m. The shapes of pores and LOFs respectively formed by high laser power or high scanning speed are closely related to their own sizes, that is, the larger the size, the more irregular the shape, which produces more detrimental effects than regular pores. [ABSTRACT FROM AUTHOR]

Magnesium matrix composites were developed as a form of material selection that can save fuel use due to excess magnesium, which has very low specific gravity and still has good mechanical properties. In this study, a magnesium matrix composite with nano-Al2O3 reinforcement was successfully fabricated using the stir casting method. When compared with magnesium monolithic, the addition of nano-Al2O3 particles of 0.05, 0.10, 0.15, 0.20, and 0.25 %Vf in magnesium composite casting was investigated to improve the mechanical properties of Mg/nano-Al2O3 composites. Magnesium composites with 0.20% Vf reinforcement were found to be the best composition of impact price, wear rate, density, and porosity. This is because the more reinforcement given, the more mechanical properties increase, but the agglomeration tendency of nano-Al2O3 particles is higher so that at a composition of 0.25 %Vf, there is a mechanism anomaly because the reinforcement carried out is less homogeneous. In addition to the number of amplifiers, the improvement of mechanical properties is influenced by the fabrication process, i.e. stir casting. This study uses chemical characterization of OES, EDS, and XRD, hard damage, impact, wear, density and porosity testing, and metallographic observations using OM and SEM. [ABSTRACT FROM AUTHOR]

Cast (real) damascus steel (so-called “wootz”) is an ancient tool/weapon material. Due to relatively high carbon amounts, the wootz is hard to forge (or other hot-forming shaping). In some cases, the forging of wootz is impossible. During forging, cracks are often created that lead to absolutely disintegration of bulk material. In this paper is given one relationship between wootz microstructure and the forging impossibility.

Archaeological research at Hoeke, a Late Medieval outer harbour of Bruges (Belgium), has revealed large quantities of iron slags, fuel and other remains of iron working. Archaeometrical study has provided an enhanced insight into the historic iron working process, a craft activity which had up till now remained completely unknown in one of the largest economic hubs of medieval Europe. Several petrological, mineralogical and geochemical analytical methods have been applied for this purpose. The metallographic analysis was performed using reflected light optical microscopy, while the mineralogical composition of the slags was characterized X-ray Diffraction (XRD) Spectrometry. Macroscopic identification of plano-convex bottom slag and hammerscales, combined with the geochemical data pointed out that the examined slag is indicating smithing activity, while no traces for iron ore melting were discovered. [ABSTRACT FROM AUTHOR]

Friction stir welding has found wide application in aircraft and rocket engineering, primarily due to the possibility of obtaining welded joints with a strength close to the strength of the base material. One of the most promising methods of such welding is spot friction stir welding that can serve as an alternative to electric contact spot welding and rivet joints. For the introduction of spot friction stir welding into the production of critical products, it is necessary to consider issues related to nondestructive quality control of welded joints obtained by this welding method. The purpose of this work is to substantiate the applicability of the ultrasonic echo method to quality control of welded joints obtained by spot friction stir welding. The relevance of the work is confirmed by the fact that to date there is no sufficiently complete information about the results of experimental studies aimed at analyzing the characteristics of welded joints obtained by spot friction stir welding. The authors of the article propose to use the ultrasonic echo method. The testing was carried out using an ultrasonic flaw detector with a dual-element piezoelectric transducer on samples prepared using spot friction stir welding. As a result of ultrasonic testing, defects such as lack of penetration and sloting were found in three samples; this was confirmed by metallographic studies. Samples with no defects were subjected to mechanical tests, as a result of which it was found that the strength of the resulting welded joints is comparable to the strength of the base metal in the samples. Metallographic studies carried out on the samples after mechanical tests also confirmed the lack of defects in the welded joints. Thus, we show the relationship between the results of ultrasonic testing, metallographic studies, and mechanical tests, which allows us to substantiate the applicability of the ultrasonic echo method to quality control of welded joints obtained by spot friction stir welding. [ABSTRACT FROM AUTHOR]

In the present incident, one of the rollers of grinding mill in cement plant failed during operation, exhibiting longitudinal cracking over inner surface. Deposition welding was carried out just before the incident to match the worn-out profile of the roller. Investigation revealed that the subsurface of the cracked region contained discontinuities like blow holes (≤1.0 mm) and fine cracks (0.2–2.0 mm length). Chemical analysis of the alloy showed low nickel (0.5 wt.%) and high tungsten (~1.0 wt.%) concentration. The deviation in composition reduced the ductility of the component. Microstructure of the alloy consisted of complex carbides (50–200 μm) embedded in martensite–austenite matrix. Under cyclic loading, the fatigue crack was initiated from subsurface containing discontinuities and bulky carbides. Low toughness (~2 J) and high residual tensile stress (~170 Mpa) of the material facilitated crack propagation through thickness direction. Final failure of the component occurred due to overload. [ABSTRACT FROM AUTHOR]

Although the recycling of materials such as copper and glass is widely known and generally well understood within archaeological contexts, far less is known about the recycling of iron. Iron recycling is more complex than that of other metals for two reasons. First, normal manufacturing processes, which include forging several components to make a composite object, offer the opportunity to include recycled iron. Second, the material itself is more complex than Cu alloys. The alloys of Fe, depending primarily on C content, are very different in terms of properties and can be interconverted by (normally) removing C such as decarburizing cast iron to make wrought iron. Thus, recycling practices are potentially intimately combined with such processes. These factors, combined with the poor preservation of archaeological iron and the consequent reluctance to carry out extensive studies (which often require destructive analysis via metallography), mean that there are no clear criteria for identifying recycled iron. However, limited historical documentation suggests, at least indirectly, that such recycling was common. This paper is neither comprehensive nor definitive, but merely intends to promote discussion and awareness of iron recycling by hypothesizing several possible mechanisms and providing a few illustrative archaeological examples. [ABSTRACT FROM AUTHOR]

Accumulating interest from academia and industry, the part of quality assurance in metal additive manufacturing (AM) is achieving incremental recognition owing to its distinct advantages over conventional manufacturing methods. In this paper, we introduced a convolutional neural network, YOLOv8 approach toward robust metallographic image quality inspection. Metallographic images accommodate key information relating to metal properties, such as structural strength, ductility, toughness, and defects, which are employed to select suitable materials for multiple engineering execution. Therefore, by comprehending the microstructures, one can understand insights into the behavior of a metal component and make predictive assessments of failure under specific conditions. Deep learning-based image segmentation is a robust technique for the detection of microstructural defects like cracks, inclusion, and gas porosity. Therefore, we improvise the YOLOv8 with dilated convolution mechanisms to acquire automatic micro-structure defect characterization. More specifically, for the first time, the YOLOv8 algorithm was proposed in the metallography dataset from additive manufacturing of steels (Metal DAM) to identify defects like cracks and porosity as a novel approach. A total of 414 images from ArcelorMittal engineers were used as an open-access database. The experimental results demonstrated that the YOLOv8 model successfully detected and identified cracks and porosity in the metal AM dataset, achieving an improved defect detection accuracy of up to 96% within just 0.5 h compared to previous automatic defect recognition processes. [ABSTRACT FROM AUTHOR]

The microstructure and tribological properties of the modified surface of 12Kh2N4A (its equivalent is E3310) and 38Kh2MYuA (its equivalent is A290C1M) structural alloy steels after laser treatment (LT) are studied using an ytterbium continuous-wave fiber laser. The laser surface treatment is carried out in air at a laser power of 75 and 100 W and a laser beam scanning velocity varying in the range of 2 to 14 mm/s. The micro- and macrostructures of the steels are examined using metallography and durometry; the structure of the laser-affected areas (LAZ) and steel constituents are determined. The scanning velocity at a laser power of 100 W is shown to have the most significant effect on the LAZ dimensions. The maximum depth of the LAZ during LT without surface melting in the studied modes is 310 μm for 12Kh2N4A steel and 170 μm for 38Kh2MYuA steel. According to the hardening mode, the microhardness in the LAZ increases from 1.36 to 1.97 times for 12Kh2N4A steel and by 2.0–2.6 times for 38Kh2MYuA steel. The tribotests performed using a pin-on-disk configuration show that the reduction of linear wear and wear rate in the 12Kh2N4A and 38Kh2MYuA steels at a hardened layer depth of ~100 μm is 26.6 and 43.9%, respectively. [ABSTRACT FROM AUTHOR]

This paper deals with the evaluation of material properties of the additively manufactured austenistic alloy 08CH18N10T, which is widely used in the Czech Republic nuclear power plants Temelín and Dukovany and other VVER reactors around the world. For purposes of utilization of additive manufacturing technologies for nuclear core components fabrication, two sets of samples were prepared from horizontally and vertically L-DED printed blocks from 08CH18N10T material. Experiments such as microstructure analysis, porosity and Vickers hardness were then performed on L-DED printed and heat-treated 08CH18N10T material, and the obtained material properties were then compared with the properties of L-DED printed 08CH18N10T material without heat-treatment for examination of its effect and also with material properties of conventionally made 08CH18N10T material. [ABSTRACT FROM AUTHOR]

A comparative analysis of the macro- and microstructure of a lead casting and a lead rod obtained from it by isostatic pressing is reported. The effect of segregation of antimony as the main dopant of the investigated alloy on the quality of a product has been demonstrated using advanced nonferrous optical metallography methods. It has been established that the upper part of a casting with a surface crack caused by adding the crystallized casting with lead contains an increased amount of antimony, nonmetallic inclusions, and pores on the fusion surface. Inside the casting, there is a shrinkage cavity along the casting axis, which results from shrinkage of the material during its crystallization. The content of the main element of the alloy (antimony) in lead of the castings corresponds to the PbSb0.9 alloy according to GOST (State Standard) 1292-81 "Lead‒antimony alloys. Specifications," but the impurity content exceeds the value recommended by GOST the total impurity content is limited to 0.1%, while the total content of copper, cadmium, bismuth, and palladium in the investigated castings is ~1%. The casting microstructure investigations have shown that the main structural defect is a shrinkage cavity located along the casting axis. The occurrence of this cavity is related to an excessively high temperature of lead casting into a mold. This has led to a long crystallization time, as evidenced by the antimony segregation in the surface areas of the shrinkage cavity. The metal of the surface layers of the shrinkage cavity is characterized by the increased antimony contents, nonmetallic inclusions, and discontinuities, which significantly changes its mechanical properties as compared with the base metal, including the plasticity, which plays a decisive role in the plastic strain processing of the casting. [ABSTRACT FROM AUTHOR]