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1. FUNCTIONAL POLYMERS 64. POTASSIUM IONIZATION OF DESORBED SPECIES (K+IDS) OF 2(2-HYDROXYPHENYL)2H-BENZOTRIAZOLES

Author

Lutz Stoeber, William J. Simonsick, Otto Vogl, and Andres Sustic

Subjects
Polymers and Plastics, Chemistry, Potassium, Analytical chemistry, chemistry.chemical_element, General Chemistry, Mass spectrometry, Weight range, medicine.disease_cause, Ionization, Materials Chemistry, Ceramics and Composites, medicine, Functional polymers, Volatility (chemistry), Ultraviolet
Abstract

Mass spectrometry using the potassium ionization of desorbed species (K+IDS) technique was found to be an unusually fruitful method to characterize 2(2-hydroxyphenyl)2H-benzotriazole derivatives. This class of compounds has the proper molecular weight range of 200 up to more than 1000 daltons (Da) and the proper volatility to show readily desirable concentrations in the mass spectrometer. This class of compounds is stable under the conditions of measurement which allows the determination of their purity. 2(2-Hydroxyphenyl)2H-benzotriazoles have recently been used most extensively for the ultraviolet stabilization of polymeric materials. In this work, over 100 2(2-hydroxyphenyl)2H-benzotriazoles have been characterized by K+IDS mass spectrometry.

Published
2000
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2. FUNCTIONAL POLYMERS 65. SYNTHESIS AND BRIEF CHARACTERIZATION OF SURFACE ACTIVE 2(2-HYDROXYPHENYL)2H-BENZO-TRIAZOLE ULTRAVIOLET STABILIZERS

Author

Otto Vogl, Lutz Stoeber, William J. Simonsick, and Andres Sustic

Subjects
chemistry.chemical_classification, Materials science, Polymers and Plastics, Triazole, General Chemistry, Polymer, Oligomer, Contact angle, chemistry.chemical_compound, Hydrocarbon, chemistry, Polymer chemistry, Materials Chemistry, Ceramics and Composites, Fluorocarbon, Functional polymers, Methyl methacrylate
Abstract

A number of 2(2-hydroxyphenyl)2H-benzotriazoles substituted in the 5-position with reactive hydroxyl and carboxyl groups have been synthesized. They include compounds with a tert butyl substitution in the 3-position or without substitution. The latter compounds were subjected to a reaction with N-hydroxy-methyl-(meth)acrylamide to form acrylic polymerizable 3(meth)acrylamidomethyl-2(2-hydroxyphenyl)2H-benzotriaz-oles. Hydroxyl reactive compounds were allowed to react with long chain acids, compounds with carboxyl groups with long chain hydrocarbon, fluorocarbon or silicon oligomer alcohols. The polymerizable 2(2-hydroxyphenyl)2H-benzotriazoles were then copolymerized with methyl methacrylate. Films made from such polymers showed by contact angle measurements, substantial migration of the fluorocarbon or silicon component to the surface of the film.

Published
2000
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4. Service Life Prediction of Organic Coatings

Author

DAVID R. BAUER, JONATHAN W. MARTIN, F. Louis Floyd, W. J. Burroughs, P. J. Neale, Nairanjana Dasgupta, Xiaomei Guan, Daryl R. Myers, D. M. Burch, J. W. Martin, S. E. Haagenrud, J. A. Chess, D. A. Cocuzzi, G. R. Pilcher, G. N. Van de Streek, William Q. Meeker, Luis A. Escobar, G. Jorgensen, C. Bingham, J. Netter, R. Goggin, A. Lewandowski, William Stephen Tait, P. Schutyser, D. Y. Perera, Fred Lee, Behnam Pourdeyhimi, Karlis Adamsons, Sam C. Saunders, Jacques Lemaire, Narcisse Siampiringue, Lance Litty, Kathryn Lloyd, Katherine Stika, Dennis Swartzfager, Dennis Walls, Barbara Wood, D. E. King, G. J. Jorgensen, Otto Vogl, Lutz Stoeber, Andres Sustic, John Crawford, Loren W. Hill, Dan Y. Perera, Patrick Schutyser, D. Vanden Eynde, M. E. Nichols, C. A. Darr, W. J. van Ooij, D. R. Bauer, J. R. Rumble, C. P. Sturrock, J. G. Kaufman, Raymond Brockhaus, Lawrence J. Kaetzel, DAVID R. BAUER, JONATHAN W. MARTIN, F. Louis Floyd, W. J. Burroughs, P. J. Neale, Nairanjana Dasgupta, Xiaomei Guan, Daryl R. Myers, D. M. Burch, J. W. Martin, S. E. Haagenrud, J. A. Chess, D. A. Cocuzzi, G. R. Pilcher, G. N. Van de Streek, William Q. Meeker, Luis A. Escobar, G. Jorgensen, C. Bingham, J. Netter, R. Goggin, A. Lewandowski, William Stephen Tait, P. Schutyser, D. Y. Perera, Fred Lee, Behnam Pourdeyhimi, Karlis Adamsons, Sam C. Saunders, Jacques Lemaire, Narcisse Siampiringue, Lance Litty, Kathryn Lloyd, Katherine Stika, Dennis Swartzfager, Dennis Walls, Barbara Wood, D. E. King, G. J. Jorgensen, Otto Vogl, Lutz Stoeber, Andres Sustic, John Crawford, Loren W. Hill, Dan Y. Perera, Patrick Schutyser, D. Vanden Eynde, M. E. Nichols, C. A. Darr, W. J. van Ooij, D. R. Bauer, J. R. Rumble, C. P. Sturrock, J. G. Kaufman, Raymond Brockhaus, and Lawrence J. Kaetzel

Subjects
Plastic coatings--Congresses, Service life (Engineering)--Congresses
Published
1999

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