6 results on '"Lorenz Fuchs"'
Search Results
2. Crack-free in situ heat-treated high-alloy tool steel processed via laser powder bed fusion: microstructure and mechanical properties
- Author
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Simon Bergmueller, Lukas Kaserer, Lorenz Fuchs, Jakob Braun, Nikolaus Weinberger, Ilse Letofsky-Papst, and Gerhard Leichtfried
- Subjects
LPBF ,High carbon steel ,High-speed steel ,Additive manufacturing ,Heat treatment ,Microstructure ,Science (General) ,Q1-390 ,Social sciences (General) ,H1-99 - Abstract
In this study, high-alloy tool steel S390 was processed crack-free and dense for the first time using laser powder bed fusion (LPBF). The resulting mechanical properties and microstructure of the LPBF steel parts were investigated. High-alloy tool steels, such as high-performance high-speed Boehler S390 steel (containing 1.64 wt% C and W, Mo, V, Co, and Cr in the ratio 10:2:5:8:5 wt%), are prone to cracking when processed using LPBF because these steels have high carbon and carbide-forming alloying elements content. Cracks are induced by thermal stresses and solid-phase transformation, combined with weak grain boundaries caused by segregated primary carbides. Substrate plate heating reduces thermal stresses and enables in situ heat treatment, thus modulating solid-phase transformation and carbide precipitation and preventing cracking during cooling. The resulting microstructure, precipitations, and mechanical properties of the as-built LPBF specimens, which were in situ heat-treated at 800 °C, and the conventionally post-heat-treated specimens were assessed using optical microscopy, scanning electron microscopy, transmission electron microscopy, energy-dispersive X-ray spectroscopy, electron backscatter diffraction, X-ray diffraction, hardness testing, bending testing, and density measurement. In situ heat treatment impacts microstructure, precipitation behavior, and solid-phase transformation, causing a change in the microstructure of the material along the build direction due to different thermal histories. The as-built specimens exhibit a hardness gradient along the build direction of 500 HV1 to 800 HV1 in the top layer. The average bending strength is 2500 MPa, measured from the tensile stresses on the harder side and the compressive stresses on the softer side. Conventional post-heat treatment yields a mean hardness of 610 HV1 and a mean bending strength of 2800 MPa.
- Published
- 2022
- Full Text
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3. Liquid Ammonia: More than an Innocent Solvent for Zintl Anions
- Author
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Gärtner, Stefanie, Witzmann, Michael, Lorenz-Fuchs, Corinna, Gschwind, Ruth M., and Korber, Nikolaus
- Abstract
Liquid ammonia as the original solvent for Zintl anions has been replaced by easier to handle or more versatile solvents in most recent Zintl chemistry. However, methodological advances have made it possible to structurally investigate the anions in ammoniate crystals via crystallography or in the solutions themselves via nuclear magnetic resonance. While in some cases liquid ammonia acts as an innocent solvent, it also provides different possibilities of direct involvement in chemical reactions. In addition to simple dissolution without changes to the anions observed in the solid starting materials, protonation of the anion, incongruent dissolution involving redox processes, and further oxidation and reduction products have been observed. The use of the solvent liquid ammonia under ambient pressure is limited to low temperatures, which in turn allows the monitoring of kinetically stabilized species, some of which cannot be accessed at higher temperatures. In this work, the available literature reports are summarized or referenced, and compounds that have been characterized as new ammoniate crystals are presented and contextualized. Innocent dissolution is observed for clusters involved in K2.9Rb5.1[Si4][Si9]·15NH3, Cs4Sn9·12NH3, Cs4Pb9·5NH3, and [Rb@[18]crown-6]2[Rb@[2.2.2]crypt]Rb[Ge9]·4NH3. Formal protonation of [Ge4]4–results in the crystallization of [Na@[2.2.2]crypt]2[H2Ge4]·3NH3. Tt52–(Tt = Sn or Pb) and HSi93–cannot be accessed in a binary solid state material but can be crystallized in co-crystals of PPh3in [Rb@[2.2.2]crypt]2[Sn5][PPh3]2·NH3, [Rb@[2.2.2]crypt]2[Pb5][PPh3]2·NH3, and [K@[2.2.2]crypt]3[HSi9][PPh3]·5NH3.
- Published
- 2024
- Full Text
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4. Systematic approach to process parameter optimization for laser powder bed fusion of low-alloy steel based on melting modes
- Author
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Simon Bergmueller, Lukas Gerhold, Lorenz Fuchs, Lukas Kaserer, and Gerhard Leichtfried
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Control and Systems Engineering ,Mechanical Engineering ,Industrial and Manufacturing Engineering ,Software ,Computer Science Applications - Abstract
In the metal additive manufacturing (AM) process of laser powder bed fusion (LPBF), there are a limited number of materials suitable for producing parts with high density and desired mechanical properties. To establish novel materials, it is essential to determine optimized process parameters in order to overcome process-related challenges and mitigate defects such as lack of fusion, keyholing, and balling. Scaling laws based on thermophysical properties and process parameters can be used to transfer knowledge from other materials or LPBF systems. In this work, a scaling law is used to adjust process parameters for single-track experiments over a wide range, which are laser power PL (100–1000 W), scan speed vs (300–2500 mm/s), and laser spot size ds (0.08–0.25 mm). Compared to existing studies, the parameter range is thus extended towards large laser spot sizes and high laser powers. The scaling law used is based on the calculation of the normalized enthalpy $$\frac{\Delta H}{{h}_{s}}$$ Δ H h s . The ratio of the deposited energy density $$\Delta$$ Δ H and the melting enthalpy hs correlates with the dimensions of the melt pool. According to the aspect ratio $${\delta }_{\mathrm{c}}$$ δ c of the melt pool of each single track, the respective melting mode—conduction, transition, and keyhole mode—was identified. The process parameters of the single tracks in transition mode were used to optimize the density of the LPBF specimens with varying hatch distance hd (0.06–0.12 mm), resulting in specimens with a relative density of > 99.8%. The proposed methodology can accelerate the process parameter finding for new alloys and avoid process-related defects. Graphical Abstract
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- 2023
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5. Supercurrent rectification and magnetochiral effects in symmetric Josephson junctions
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Denis Kochan, Sergei Gronin, Simon Reinhardt, Nicola Paradiso, Tyler Lindemann, Lorenz Fuchs, Paulo E. Faria Junior, Geoffrey C. Gardner, Christoph Strunk, Christian Baumgartner, Jaroslav Fabian, Michael J. Manfra, and Andreas Costa
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Superconductivity ,Physics ,Josephson effect ,Condensed matter physics ,Supercurrent ,ddc:530 ,Biomedical Engineering ,Bioengineering ,Condensed Matter::Mesoscopic Systems and Quantum Hall Effect ,Condensed Matter Physics ,530 Physik ,01 natural sciences ,Atomic and Molecular Physics, and Optics ,010305 fluids & plasmas ,Magnetic field ,Inductance ,Rectification ,Condensed Matter::Superconductivity ,0103 physical sciences ,General Materials Science ,Electrical and Electronic Engineering ,010306 general physics ,Quantum well ,Diode - Abstract
Transport is non-reciprocal when not only the sign, but also the absolute value of the current depends on the polarity of the applied voltage. It requires simultaneously broken inversion and time-reversal symmetries, for example, by an interplay of spin–orbit coupling and magnetic field. Hitherto, observation of nonreciprocity was tied to resistivity, and dissipationless non-reciprocal circuit elements were elusive. Here we engineer fully superconducting non-reciprocal devices based on highly transparent Josephson junctions fabricated on InAs quantum wells. We demonstrate supercurrent rectification far below the transition temperature. By measuring Josephson inductance, we can link the non-reciprocal supercurrent to an asymmetry of the current–phase relation, and directly derive the supercurrent magnetochiral anisotropy coefficient. A semiquantitative model explains well the main features of our experimental data. Non-reciprocal Josephson junctions have the potential to become for superconducting circuits what pn junctions are for traditional electronics, enabling new non-dissipative circuit elements. Diodes exhibit non-reciprocal current–voltage relations, that is, the resistivity depends on the direction of the current flow. Now an array of Josephson junctions with large spin–orbit interaction acts as the superconducting version of a diode, where dissipation-free supercurrent flows in one direction, but not the other.
- Published
- 2021
6. Josephson inductance as a probe for highly ballistic semiconductor-superconductor weak links
- Author
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Michael J. Manfra, Simon Reinhardt, Linus Frész, Nicola Paradiso, Christoph Strunk, Geoffrey C. Gardner, Sergei Gronin, Lorenz Fuchs, and Christian Baumgartner
- Subjects
Josephson effect ,Superconductivity ,Physics ,Condensed matter physics ,business.industry ,Condensed Matter - Superconductivity ,Supercurrent ,Phase (waves) ,General Physics and Astronomy ,FOS: Physical sciences ,Heterojunction ,01 natural sciences ,Inductance ,Superconductivity (cond-mat.supr-con) ,Semiconductor ,Interference (communication) ,Condensed Matter::Superconductivity ,0103 physical sciences ,010306 general physics ,business - Abstract
We present simultaneous measurements of Josephson inductance and DC transport characteristics of ballistic Josephson junctions based upon an epitaxial Al-InAs heterostructure. The Josephson inductance at finite current bias directly reveals the current-phase relation. The proximity-induced gap, the critical current and the average value of the transparency $\bar{\tau}$ are extracted without need for phase bias, demonstrating, e.g.,~a near-unity value of $\bar{\tau}=0.94$. Our method allows us to probe the devices deeply in the non-dissipative regime, where ordinary transport measurements are featureless. In perpendicular magnetic field the junctions show a nearly perfect Fraunhofer pattern of the critical current, which is insensitive to the value of $\bar{\tau}$. In contrast, the signature of supercurrent interference in the inductance turns out to be extremely sensitive to $\bar{\tau}$., Comment: 13 pages, 13 figures
- Published
- 2020
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