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Raw data for "Imaging Cu2O nanocube hollowing in solution by quantitative in situ X-ray ptychography" Ptychographic data sets The file "raw_data_ptychography.zip" contains one HDF5 archive for each ptychographic scan. The archives are structured as follows: section experiment: identifiers of the lightsource, beamline, beamtime, session number, and scan number section measured: N diffraction patterns of size 512x512 px N scan positions in mm one detector mask of size 512x512 px slice separation in mm for multi slice reconstruction section parameters: distance between sample and detector in mm pixel size of detector in mm photon energy in keV cropping of diffraction patterns in px used during reconstruction The following list shows the scan numbers with their corresponding reaction times and slice separations for the in situ series measured at beamline P06 at 15.25 keV. scan number slice distance, mm reaction time, h 232 1 0.20 233 1 0.56 234 1 0.92 235 1 1.27 236 1 1.63 237 1 2.01 238 0.98 2.36 239 0.96 2.72 240 0.94 3.08 241 0.9 3.43 242 0.88 3.83 243 0.86 4.19 244 0.84 4.54 245 0.82 4.90 246 0.82 5.26 247 0.82 5.63 248 0.8 5.98 249 0.8 6.34 250 0.8 6.70 251 0.78 7.05 252 0.78 7.43 253 0.78 7.79 254 0.76 8.15 255 0.76 8.50 256 0.76 8.86 257 0.74 9.23 258 0.74 9.58 259 0.72 9.94 260 0.72 10.30 261 0.7 10.65 262 0.68 11.07 263 0.66 11.42 264 0.64 11.78 266 0.62 12.17 267 0.6 12.53 268 0.58 12.89 269 0.56 13.24 270 0.54 13.60 271 0.52 13.99 272 0.5 14.37 273 0.46 14.72 274 0.42 15.08 275 0.4 15.44 277 0.4 15.87 278 0.4 16.22 279 0.36 16.58 280 0.3 16.93 281 0.25 17.29 282 0.25 17.68 283 0.25 18.04 289 0.2 20.45 290 0.2 21.47 Ptychographic reconstructions The file "ptychographic_reconstructions.zip" contains the ptychographic reconstructions shown in the article and supplementary information in tiff format. Stacks of images corresponding to time series: P06_15.25_keV_scans_00232-00283_entrance_window_aligned.tif P06_15.25_keV_scans_00232-00283_exit_window_aligned.tif cSAXS_8.98_keV_scans_00200-00324_aligned.tif Single images (the file name indicates the respective figure): P06_15.25_keV_scan_00289_Figure_6_a.tif P06_15.25_keV_scan_00290_Supplementary_Figure_11.tif cSAXS_8.98_keV_scan_00347_Supplementary_Figure_13_d.tif cSAXS_8.98_keV_scan_00586_Supplementary_Figure_14_a.tif SEM images The file "SEM_images.zip" contains the SEM images shown in the article and supplementary information in tiff format. The file names indicate the respective figure: Figure_5_h.tif Figure_5_i.tif Figure_6_b.tif Supplementary_Figure_14_b.tif, Acknowledgements: This work was supported by the Bundesministerium für Bildung und Forschung (BMBF) within the Röntgen-Ångström-Cluster via the project 05K2020 - 2019-06104 XStereoVision (grant no. 05K20GUA), by the European Research Council within the project LINCHPIN (grant no. 818941), and by the Cluster of Excellence "CUI: Advanced Imaging of Matter" of the Deutsche Forschungsgemeinschaft (DFG) – EXC 2056 – project ID 390715994.