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Soil organic carbon (SOC) prediction from remote sensing is often hindered by disturbing factors at the soil surface, such as photosynthetic active and non–photosynthetic active vegetation, variation in soil moisture or surface roughness. With the increasing amount of freely available satellite data, recent studies have focused on stabilizing the soil reflectance by building reflectance composites using time series of images. Although composite imagery has demonstrated its potential in SOC prediction, it is still not well established if the resulting composite spectra mirror the reflectance fingerprint of the optimal conditions to predict topsoil properties (i.e. a smooth, dry and bare soil). We have collected 303 photos of soil surfaces in the Belgian loam belt where five main classes of surface conditions were distinguished: smooth seeded soils, soil crusts, partial cover by a growing crop, moist soils and crop residue cover. Reflectance spectra were then extracted from the Sentinel–2 images coinciding with the date of the photos. After the growing crop was removed by an NDVI < 0.25, the Normalized Burn Ratio (NBR2) was calculated to characterize the soil surface, and a threshold of NBR2 < 0.05 was found to be able to separate dry bare soils from soils in unfavorable conditions i.e. wet soils and soils covered by crop residues. Additionally, we found that normalizing the spectra (i.e. dividing the reflectance of each band by the mean reflectance of all spectral bands) allows for cancelling the albedo shift between soil crusts and smooth soils in seed–bed conditions. We then built the exposed soil composite from Sentinel–2 imagery for southern Belgium and part of Noord-Holland and Flevoland in the Netherlands (covering the spring periods of 2016–2021). We used the mean spectra per pixel to predict SOC content by means of a Partial Least Squares Regression Model (PLSR) with 10–fold cross–validation. The uncertainty of the models was assessed via the prediction interval ratio (PIR). The cross validation of the model gave satisfactory results (mean of 100 bootstraps: model efficiency coefficient (MEC) = 0.48 ± 0.07, RMSE = 3.5 ± 0.3 g C kg–1, RPD = 1.4 ± 0.1 and RPIQ = 1.9 ± 0.3). The resulting SOC prediction maps show that the uncertainty of prediction decreases when the number of scenes per pixel increases, and reaches a minimum when at least six scenes per pixel are used (mean PIR of all pixels is 12.4 g C kg–1, while mean SOC predicted is 14.1 g C kg–1). The results of a validation against an independent data set showed a median difference of 0.5 g C kg–1 ± 2.8 g C kg–1 SOC between the measured (average SOC content 13.5 g C kg–1) and predicted SOC contents at field scale. Overall, this compositing method shows both realistic within field and regional SOC patterns.

Pilot studies have demonstrated the potential of remote sensing for soil organic carbon (SOC) mapping in exposed croplands. However, the use of remote sensing for SOC prediction is often hindered by disturbing factors at the soil surface, such as photosynthetic active and non-photosynthetic active vegetation, variation in soil moisture or surface roughness. With the increasing amount of freely available satellite data, recent studies have focused on stabilizing the soil reflectance by building image composites. These composites tend to minimize the disturbing effects by applying sets of criteria. Here, we aim to develop a robust method that allows selecting Sentinel-2 (S-2) pixels with minimal influence of the following disturbing factors: crop residues, surface roughness and soil moisture. We selected all S-2 cloud-free images covering the Belgian Loam Belt from January 2019 to December 2020 (in total 36 images). We then built nine exposed soil composites based on four sets of criteria: (1) lowest Normalized Burn Ratio (NBR2), (2) Normalized Difference Vegetation Index (NDVI) < 0.25, (3–5) NDVI < 0.25 and NBR2 < threshold, (6) the ‘greening-up’ period of a crop and (7–9) the ‘greening-up’ period of a crop and NBR2 < threshold. The ‘greening-up’ period was selected based on the NDVI timeline, where ‘greening-up’ is considered as the last date of acquisition where the soil is exposed (NDVI < 0.25) before the crop develops (NDVI > 0.25). We then built a partial least square regression (PLSR) model with 10-fold cross-validation to estimate the SOC content based on 137 georeferenced calibration samples on the nine composites. We obtained non-satisfactory results (R2 < 0.30, RMSE > 2.50 g C kg–1, and RPD < 1.4, n > 68) for all composites except for the composite in the ‘greening-up’ stage with a NBR2 < 0.07 (R2 = 0.54 ± 0.12, RPD = 1.68 ± 0.45 and RMSE = 2.09 ± 0.39 g C kg–1, n = 49). Hence, the ‘greening-up’ method combined with a strict NBR2 threshold allows selecting the purest exposed soil pixels suitable for SOC prediction. The limit of this method might be its coverage of the total cropland area, which in a two-year period reached 62%, compared to 95% coverage if only the NDVI threshold is applied.

Optical remote sensing and in particular hyperspectral or imaging spectroscopy remote sensing has been long proved to be an adequate method to predict topsoil organic carbon (Corg) content with good accuracy when the soils are well exposed and undisturbed. Several recent studies demonstrated further in science cases the potential of multispectral Copernicus Sentinel-2 data for bare soils Corg prediction, although challenges were reported related to the impact of disturbing factors. Disturbing factors that can affect the prediction and performances of soil surface properties from optical remote sensing are several and can be e.g. due to mixing in the field-of-view with partial vegetation cover depending on the landscape fragmentation. Most pixels at the remote sensing level are composites and in croplands, mixtures of soils with trees or green plants, or mixture with crop residues after harvest are likely. Another factor might be the presence of residual soil moisture or standing water after rain events. Soil reflectance decreases with increasing soil moisture and increasing soil roughness. Soil Surface roughness changes are observed due to variations in soil texture and to variable microtopography. Possible angular and solar illumination changes may affect the soil reflectance as well.In the frame of the ESA WORLDSOILS Project (https://www.world-soils.com) aiming at developing a pre-operational Soil Monitoring System to provide yearly estimations of soil organic carbon at global scale based on space-based EO data, we are working on the development of a spatially upscaled soil spectral library (SUSSL). The SUSSL is based on a sub-selection of the European LUCAS soil database, and includes simulation of realistic scenarios of ‘landscape-like’ cropland reflectance data with effect of mixture with green and dry vegetation, effect of varying soil moisture content, and effect of variable soil roughness. This database is further convoluted to the different spectral response functions of several EO sensors to simulate EO view of surface reflectances in croplands. In a next step, the SUSSL shall be used for the test and validation of different correction, disaggregation and unmixing techniques to assess the capabilities of the retrieval of undisturbed surface reflectance, to which soil prediction models can be applied with increased accuracy. In this talk, we will present the database developed, including methodological choices and parameter selections for the simulation of the different disturbing effects. Further, preliminary assessments will be shown on the uncertainties of the undisturbed vs. disturbed signal and impact on soil properties prediction.

Pilot studies have demonstrated the potential for remote sensing techniques for soil organic carbon (SOC) mapping in exposed croplands. However, the use of remote sensing for SOC prediction is often hindered by disturbing factors at the soil surface such as photosynthetic active and nonphotosynthetic active vegetation, variation in soil moisture or surface roughness. With the increasing amount of freely available satellite data, many studies have focused on stabilizing the soil reflectance by building image composites that are generated using a set of criteria. These composites tend to minimize and cancel out the disturbing effects. Here we aim to develop a robust method that allows selecting Sentinel-2 (S-2) pixels that are not affected by the following disturbing factors: crop residues, surface roughness and soil moisture. We selected all S-2 cloud-free images covering the Loam Belt of Belgium from January 2019 to December 2020 (in total 38 images). We then built four exposed soil composites based on four sets of criteria: (1) NDVI < 0.25, (2) NDVI < 0.25 & Normalized Burn Ratio (NBR2) < 0.07, (3) the ‘greening-up’ period of a crop and (4) the ‘greening-up’ period of a crop & NBR2 < 0.07. The ‘greening-up’ period was selected based on the NDVI timeline, where ‘greening-up’ is considered as the last date of acquisition where the soil is bare (NDVI < 0.25) before the crop develops (NDVI > 0.6).,We then built a partial least square regression (PLSR) model with 10-fold cross-validation to estimate the SOC content based on 137 georeferenced calibration samples on the four above described composites. We obtained a non-satisfactory result for composites (1) to (3): R² = 0.22, RMSE = 3.46 g C kg-1 and RPD 1.12 for (1), R² = 0.19, RMSE = 3.43 g C kg-1 and RPD 1.10 for (2) and R² = 0.15, RMSE = 2.74 g C kg-1 and RPD 1.06 for (3). We, however, obtained a satisfactory result for composite (4): R² = 0.54, RMSE = 2.09 g C kg-1 and RPD 1.68. Hence, the ‘greening-up’ method combined with a strict NBR2 threshold allows selecting the purest exposed soil pixels suitable for SOC prediction. The limit of this method might be the surface coverage, which for a two-year period reached 47% of croplands, compared to 89% exposure if only the NDVI threshold is applied.

Intra-field heterogeneity of soil properties is function of complex interaction between biological, physical factors and historic agricultural management. Quantifying the spatial patterns of soil properties such as soil organic carbon (SOC), nitrogen (N), phosphorous, exchangeable cations, pH, soil texture will contribute to an optimization of fertilizer application and crop yields. We tested the capacity of the multispectral Micasense rededge camera mounted on a UAV in order to map the development of winter wheat and related the Red-Edge NDVI (RENDVI) from the sensor to the Plant Area Index (PAI) measured in the field. The geo-referenced grain yield of the winter wheat was measured by a combine harvester and the top soil characteristics analysed by a grid based sampling. The spatial patterns in RENDVI at three phenological stages were mapped together with the yields. For each of these images conditional inference trees were used to derive the soil properties that significantly influenced these spatial patterns. Within-field variation in PAI (cv 41 % in March, 27% in April and 9 % in May) and yield (cv 4%) can be observed. The spatial patterns of RENDVI are rather constant and their correlation with yields is highest in March and April (r=0.64). Soil properties explain between 67 to 79 % of the variance in vegetation index throughout the growing season as well as 67 % of the variance in yield. Legacy effects of land consolidation two years earlier reflected in the field lay-out, pH and exchangeable K are significant factors explaining around 12-18 % of the variance in crop yield each. The SOC contents were overall low (8-15 g kg-1). Hence, the N supply resulting from SOC mineralization throughout the growing season covered less than 10% of the crop needs and the yield patterns did not reflect the variation in SOC contents.

During the surface mount technological process the assembled PCB is exposed to heat when molten solder alloy wets the surfaces and creates future solder joints. The PCB with all components should ideally be exposed to the same temperature profile during the soldering process. The temperatures differ throughout the PCB due to different thermal capacities of used materials and components even though the temperature profile is stable. The aim of the study was to assess the solderability of the copper material with different thermal capacity and to consider the effect of different types of fluxes. The measurement was done by wetting balance method, where the wetting force is measured as a function of time during which the test specimen is immersed into, remains immersed and then it is pulled out from the solder bath. In our experiments we used copper wire of four different diameters (0.7 mm, 1 mm, 1.5 mm), three types of solders - one lead (Sn63Pb37) and two lead free (Sn99Cu1, Sn97Cu3) solders and three types of fluxes.