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1. Microwave assisted cycloaddition of benzonitrile oxides to 1-iodobuta-1,3-diynes.

Author

Efremova, Mariia M., Khashimova, Diana D., Kalinin, Nikita S., Shtyrov, Andrey A., Ryazantsev, Mikhail N., Spiridonova, Dar'ya V., Govdi, Anastasia I., and Balova, Irina A.

Subjects
*COUPLING reactions (Chemistry), *RING formation (Chemistry), *SONOGASHIRA reaction, *BENZONITRILE, *ISOXAZOLES
Abstract

[Display omitted] The microwave-assisted cycloaddition of 2,6-disubstituted benzonitrile oxides to 1-iodobuta-1,3-diynes occurs at the iodo-substituted triple bond giving predominantly 5-alkynyl-4-iodo-1,2,3-isoxazoles. The Suzuki–Miyaura and Sonogashira cross-coupling reactions were used for the modification of the thus obtained 4-iodoisoxazoles. [ABSTRACT FROM AUTHOR]

Published
2024
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