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The effect of several essential oils, plant extracts and packaging materials on oxidative stability of virgin olive oil during different storage times was investigated. The formation of free radicals, changing of color, development of rancid odor and taste are formed as a result of the oxidation of stored oils due to the effect of oxygen and light in the environment depending on the properties of the packaging materials used. As the storage time progressed, viscosity, color, free fatty acid, peroxide and K232 values were increased. The highest increase in K270 value was found in the first month whereas the value of p-anisidine was found to be maximum in the second and third months of storage. The highest acidity (1.91%) and discoloration were observed in the samples stored in the glass-pet bottle while the highest viscosity (99.80 mPa s), peroxide (12.00 meq O2/kg), K232 (0.73) and K270 (0.11) values are found in the samples stored in the tin. The highest free fatty acid values of samples stored in glass bottles, PET bottles and tin were detected in olive oils added rosemary. The peroxide values of the samples stored in glass and pet bottles decreased at 1st month and increased as the storage process progressed.

The increase in the oil yield of germinated (sprouted) tigernut tubers may be due to the decrease in protein, carbohydrate and mineral contents during the germination process. Antioxidant activity values of both sprouted and raw “Balyumru” tigernut tubers were found higher than those of results of sprouted and raw “Sariseker” tigernut tubers. The phenolic compounds of tigernut tubers changed depending on variety and germination process. Generally, gallic (except raw “Balyumru”), 3,4-dihydroxybenzoic acid, (+)-catechin, 1,2-dihydroxybenzene, syringic acid, caffeic acid, rutin trhydrate, p-coumaric acid, trans-ferulic acid and apigenin-7-glucoside contents of raw “Sariseker” and “Balyumru” tigernut tubers increased compared to sprouted tigernut tubers depending on germination process. The oleic acid amounts of sprouted and raw “Sariseker” and “Balyumru” tigernut tuber oils were determined as 72.47% and 71.36–72.67 and 73.58%, respectively. Ca, K, Mg, Na and P were found at the highest levels in tigernut tubers. The oil and protein contents, fatty acid compositions, total phenol, antioxidant activity, phenolic compounds and the nutrients of raw and sprouted (germinated) “Sariseker” and “Balyumru” tigernut tuber flours were investigated.

The bioactive compounds, antioxidant activity, fatty acid composition, and antimicrobial activity of methanolic extracts of propolis collected from five locations in Turkey were examined. The total...

The bioactive properties of the almond kernel cultivars were determined in the 10 min sonication period with the highest values being observed in the “Ferraduel” almond cultivar. While total phenolic contents of almond kernel extracts obtained by extraction for 10 min change between 10.97 mg GAE/100 g (Texas) and 106.25 mg GAE/100 g (Ferraduel), total phenolic contents of almond kernels extracted for 20 min were determined between 12.57 mg GAE/100 g (Nonpareil) and 103.54 mg GAE/100 g (Ferraduel). Oleic acid amounts of almond kernel oil samples extracted at 10 min changed between 37.84% (Texas) and 75.90% (Ferragnes) while the oleic acid amounts of almond kernel oils obtained by ultrasound-assisted extraction at 20 min sonication period vary between 70.76% (Texas) and 75.91% (Ferragnes). Also, while linoleic acid contents of almond kernel oils at 10 min are identified between 15.78% (Ferragnes) and 21.40% (Texas), linoleic acid amounts of almond kernel oils extracted by ultrasound-assisted extraction at 20 min changed between 16.02% (Ferragnes) and 21.52% (Texas). Gallic acid acid contents of almond kernel extracts at 10 and 20 min sonication period changed between 2.21 mg/100 g (Bitter almond) and 12.90 mg/100 g (Ferragnes), to 3.08 mg/100 g (Nonpareil) and 15.13 mg/100 g (Ferraduel), respectively.

The oil recovery from Alyanak apricot kernel was 36.65% in control (unroasted) and increased to 43.77% in microwave-roasted kernels. The total phenolic contents in extracts from apricot kernel were between 0.06 (oven-roasted) and 0.20 mg GAE/100 g (microwave-roasted) while the antioxidant activity varied between 2.55 (oven-roasted) and 19.34% (microwave-roasted). Gallic acid, 3,4-dihydroxybenzoic acid, (+)-catechin and 1,2-dihydroxybenzene were detected as the key phenolic constituents in apricot kernels. Gallic acid contents varied between 0.53 (control) and 1.10 mg/100 g (microwave-roasted) and 3,4-dihydroxybenzoic acid contents were between 0.10 (control) and 0.35 mg/100 g (microwave-roasted). Among apricot oil fatty acids, palmitic acid contents ranged from 4.38 (oven-roasted) to 4.76% (microwave-roasted); oleic acid contents were between 65.73% (oven-roasted) and 66.15% (control) and linoleic acid contents varied between 26.55 (control) and 27.12% (oven-roasted).

The tocopherol contents of unripe and ripe avocado fruit oil extracted from Pinkerton, Hass and Fuerte varieties were determined after drying fruit using air, microwave or oven drying methods. The α-tocopherol content changed between 13.70 mg/100 g (microwave-dried) and 28.06 mg/100 g (air-dried) in oil from unripe Pinkerton fruit; between 14.86 mg/100 g (microwave-dried) and 88.12 mg/100 g (fresh) in oil from unripe Hass fruit and between 13.31 mg/100 g (microwave-dried) and 17.35 mg/100 g (oven-dried) in oil from unripe Fuerte fruit. The α-tocopherol contents in oil from ripe Fuerte fruit changed between 13.21 mg/100 g (fresh) and 17.61 mg/100 g (oven-dried). In addition, γ-tocopherol contents varied between 11.55 mg/100 g (air-dried) and 14.61 mg/100 g (microwave-dried) unripe "Pinkerton" fruit; between 11.52 mg/100 g (air-dried) and 15.01 mg/100 g (fresh) in unripe Hass fruit and between 12.17 mg/100 g (air-dried) and 15.27 mg/100 g (microwave-dried) unripe Fuerte fruit. The γ-tocopherol contents ranged from 12.71 mg/100 g (fresh) to 17.40 mg/100 g (oven-dried) in ripe Hass fruit; from 10.29 mg/100 g (fresh) and 17.20 mg/100 g (microwave-dried) ripe Fuerte fruit. α-, β-, γ- and δ-tocopherols could not be detected in ripe fresh Pinkerton fruit. In general, β- and δ-tocopherol could not be detected in most of the unripe and ripe avocado fruit oils. α-Tocopherol and γ-tocopherol contents of dried ripe Fuerte fruit oils were found to be higher compared to those of dried unripe Fuerte fruits.

All drying processes increased oil content, antioxidant activity, total phenolic contents, and most of the phenolic compounds in the pulp, peel and seeds of both ripe fruits with varied degrees (p < 0.05). In addition, the processes reduced the oil contents, linoleic acids, 3,4-dihydroxybenzoic acid, (+)-catechin, and naringenin of the pulp, antioxidant activity of the peels and seeds, and 3,4-dihydroxybenzoic acid, (+)-catechin of the seeds and it enhanced all other parameters in the pulp, peel, and seeds of unripe fruits (p < 0.05). Comparing the phenolic profiles of avocado pulp, peels, and seeds of ripe and unripe fruits indicated that the peel and seeds are richer than the pulp and that is superior in unripe fruits than ripe ones. In addition, drying processes particularly microwave and air drying greatly enhanced the bioactive properties of ripe and unripe avocado fruits and could thus be used to elongate the shelf-life of avocado fruit products without major impact on the overall quality.

In this study, the combined effect of different packaging materials (transparent PET, transparent glass, glass-PET bottle and tin), some aromatic herbs (thyme, rosemary, sage and olive leaf) and also their essential oils (thyme, rosemary and sage) on fatty acid composition of virgin olive oil was investigated during storage period. The initial amounts of the main fatty acids as oleic, palmitic and linoleic acids were determined as 72.89%, 11.89% and 8.96%, respectively. The addition of aromatic plants and essential oils did not effect the fatty acid profile. Also, packaging materials had a minor influence on fatty acids. In the 6th month of storage, the oleic acid contents of olive oils showed the increase in all of samples. The highest increase was observed in olive oil stored in glass-PET (74.30-75.01%), followed by stored in glass bottle (73.41-74.82%). Generally, during the storage, the differences of fatty acid contents were in minor level. The fatty acid composition of olive oils stored under different essential oil and extract concentrations showed partial differences depending on the extract type and concentration.

Oil contents of seeds changed between 15.89 g/100 g (purslane) and 38.97 g/100 g (black radish). Palmitic acid contents of oil samples were found between 2.2 g/100 g (turnip) and 15.0 g/100 g (purslane). While oleic acid contents of oil samples change between 12.1% (turnip) and 69.8% (purple carrot), linoleic acid contents of oils were determined between 8.9% (black radish) and 57.0% (onion). The highest linolenic acid was found in purslane oil (26.7%). While α-tocopherol contents of oil samples range from 2.01 mg/kg (purple carrot) to 903.01 mg/kg (onion), γ-tocopherol contents of vegetable seed oils changed between 1.14 mg/kg (curly lettuce) and 557.22 mg/kg (purslane). While campesterin contents of seed oils change between 203.2 mg/kg (purple carrot) and 2808.5 mg/kg (cabbage Yalova), stosterin contents of oil samples varied from 981.5 (curly lettuce) to 4843.3 mg/kg (purslane). The highest brassicasterin and δ5-avenasterin were found in red cabbage oil (894.5 mg/kg) and purslane seed oils (971.3 mg/kg), respectively. Total sterol contents of seed oils changed between 2960.4 mg/kg (purple carrot) and 9185.1 mg/kg (purslane). According to the results, vegetable seeds have different bioactive compound such as fatty acid, tocopherol and phytosterol.

Lemon peel powder (LPP) obtained after drying (microwave, infrared, and oven) showed the lowest (58.72%) DPPH-radical scavenging activity in oven-dried and the highest (67.84%) in infrared-dried LPP while that of fresh lemon peel remained 63.22%. Orange peel powder (OPP) showed the lowest DSA (61.65) after microwave and the lowest (63.54%) after infrared-drying while that of fresh orange peel was 63.48%. Total phenolics were between 114.58 (fresh) and 179.69 mgGAE/100 g (oven) in LPP and between 158.54 (fresh) and 177.92 mgGAE/100 g (infrared) in OPP. The total flavonoid contents were 380.44 (fresh)–1043.04 mg/100 g (oven) in case of LPP and 296.38 (fresh)–850.54 mg/100 g (oven) in case of OPP. The gallic acid contents were 2.39 (fresh)–14.02 mg/100 g (oven) in LPP. The (+)-catechin contents were 1.10 (fresh)–49.57 mg/100 g (oven) for LPP and 0.82 (fresh)–7.63 mg/100 g (infrared) in case of OPP. The oleic acid content was 22.99 (infrared)–58.85% (fresh) in LPP-oil and 28.59 (microwave)–61.65% (fresh) in OPP-oil. The linoleic acid contents were 13.76 (fresh)–36.90% (oven) in LPP-oil and 14.14 (fresh)–37.08% (infrared) in case of OPP-oil. The drying techniques showed profound but variable effects on radical scavenging activity, total phenolics, flavonoid, carotenoids, phenolic compounds and fatty acid composition of both LPP and OPP and oven-drying (60 °C) was the most effective in improving these bioactive constituents.

Oil content of almond kernels ranged from 36.7% in the cultivar T12 to 79.0% in genotype T27. The major fatty acid in almond oil is oleic (62.43% in T7-76.34% in T4) followed by linoleic (13.97% in T4-29.55% in T3) and palmitic (4.97% in T2-7.51% inT3). The main tocopherol in almond oil was α-tocopherol (44.25 mg/100 g in T25-75.56 mg/100 g in T13) that was 44 folds higher than other tocopherols in the oil. Total tocopherol contents of almond oils ranged between 47.42 mg/100 g (T14) and 80.15 mg/100 g (T16). Among macro minerals, K was the highest (5238–14,683 mg/kg), followed by P (3475–11,123 mgkg), Ca (1798–5946 mg/kg), and Mg (2192–3591 mg/kg), whereas Na was the least (334–786 mg/kg) in almond kernel. The total polyphenol was observed in T16 (98.67 mg GAE/100 g), while the least was found in T24 (23.75 mg GAE/100 g). Antioxidant activity was high in T7 (91.18%) and low in T12 (44.59%).

In this study, phenolic compounds were extracted from Argel leaves using an ultrasound-assisted extraction (UAE) method. The extraction parameters (sonication temperature, time, and ethanol concentration) were optimized using a response surface methodology (Box-Behnken design), in order to maximize the total phenolic content (TPC) and 1,1-diphenyl-2-picrylhydrazyl (DPPH) scavenging activity of Argel leaf extracts (ALEs). The phenolic compounds of the ALEs obtained under optimized conditions were also identified. The optimum UAE conditions for achieving maximum TPC (72.27 g gallic acid equivalents kg−1 DW) and DPPH scavenging activity (86.15%) were a 60 °C temperature, a 37.07 min duration, and a 39.14% ethanol concentration. Under these conditions, the experimental values of TPC and DPPH scavenging activity were 73.02 g GAE kg−1 and 85.56%, respectively, which agreed with the predicted values. In addition, the major phenolic acids found in ALEs under the optimized extraction conditions were sinapic, p-coumaric, and ferulic acid. Overall, the findings of this study demonstrated the suitability of UAE and the success of RSM in optimizing the extraction conditions of bioactive compounds from ALEs.

WOS: 000517708300002, The impact of fermentation and bud size on the antioxidant activity, total phenolic content (TPC), and bioactive compounds of caper buds were investigated. The results showed significant differences in the bioactive properties depending on bud sizes and fermentation process. Antioxidant activity values of fresh caper buds were ranged between 69.61% (bid size) and 72.78% (small size), whereas the values of fermented ones varied between 12.50% (big size) and 39.09% (small size). TPC of fresh caper buds were found in the range of 357.81 mg GAE/100 g (medium size) and 372.22 mg GAE/100 g (small size), while those of fermented buds were ranged from 167.53 mg GAE/100 g (medium) to 246.01 mg GAE/100 g (small). Apigenin-7-glucoside, (+)-catechin, 1,2-dihydroxybenzene, and 3,4-dihydroxybenzoic, syringic, and gallic acids were the major phenolic compounds in both fresh and fermented caper buds. Overall, this study clearly demonstrated that both fermentation process and bud size significantly affected the antioxidant activity, TPC, and phenolic compounds of caper buds., Deanship of Scientific Research at King Saud UniversityDeanship of Scientific Research at King Saud University [RG-1439-080], The authors would like to extend their sincere appreciation to the Deanship of Scientific Research at King Saud University for its funding the Research group no (RG-1439-080). Technical support of RSSU at King Saud University is also well appreciated.

The effects of Moringa leaves as a partial replacer of alfalfa hay on oxidative status of goats' blood and milk were investigated in this study. Three dietary treatments including alfalfa (AHD), 25% Moringa oleifera Lam. (MOD) or 25% Moringa peregrina Forssk. (MPD) diets were used in this study. Thirty goats were randomly assigned into 3 experimental groups with 10 experiment units (10 goats) each using completely randomized design. The experiment consisted of 2-week adaptation and 6-week collection data. Both MPD and MOD showed higher fat, nitrogen free extract, total phenolics, antioxidant activity than AHD. Malondialdehyde concentration of milk and serum was lower in goats fed MPD and MOD. Catalase activity, vitamin C contents and total antioxidant capacity were higher in the milk and serum of goats fed diets containing MOD or MPD than that fed AHD. Replacement of alfalfa hay in goats' diet with M. oleifera or peregrina leaves resulted in reduction of serum cholesterol and glucose levels. The results suggest that utilization of M. oleifera or peregrina leaves as a non-traditional fodder could improve both animal and consumer oxidative status and immune systems through the transfer of bioactive compounds, particularly antioxidants and vitamin C from fodder to milk.

In this study, the effect of altitude on oil amounts, antioxidant activity, polyphenol content and mineral contents of Acacia seeds collected from two different locations (up to 1100 m above sea level) was investigated. Total carotenoid and flavonoid contents of Acacia seeds were detected as 0.76 (Konya) and 1.06 µg/g (Tasucu-Mersin) to 1343.60 (Konya) and 184.53 mg/100 g (Tasucu-Mersin), respectively. Total phenol contents and antioxidant activity values of Acacia seeds were identified as 255.11 (Konya) and 190.00 mgGAE/Tasucu-Mersin) to 64.18% (Konya) and 75.21% (Tasucu-Mersin), respectively. The oils extracted from Acacia seeds in Konya and Mersin province contained 62.70% and 70.39% linoleic, 23.41% and 16.03% oleic, 6.45%and 6.04% palmitic and 2.93% and 4.94% stearic acids, respectively. While 3,4-dihydroxybenzoic acid amounts of seeds are determined as 3.89 (Konya) and 4.83 mg/100 g (Tasucu-Mersin), (+)-catechin contents of Acacia seeds were identified as 3.42 (Konya) and 9.51 mg/100 g (Tasucu-Mersin). Also, rutintrihydrate and ferulic contents of Acacia seeds were found as 23.37 (Konya) and 11.87 mg/100 g (Tasucu-Mersin) to 14.74 mg/100 g (Konya) and 1.12 mg/100 g (Tasucu-Mersin), respectively. Acacia seeds collected from Konya and Mersin contained 4003.75 and 3540.89 mg/kg P, 9819.12 and 16175.69 mg/kg K, 4347.47 and 5078.81 mg/kg P, 2195.77 and 2317.90 mg/kg Mg, 1015.75 and 2665.60 mg/kg S and 187.53 and 905.52 mg/kg Na, respectively.

Ultrasound-assisted extraction (UAE) was optimized for the collection of phenolic compounds and determination of antioxidant activity of watermelon peel (WMP) and watermelon seed (WMS) using Box-Behnken design and response surface methodology. UAE process variables (sonication temperature, sonication time, and ethanol concentration) had a significant impact on the total phenolic content (TPC) and antiradical activity of WMP and WMS. The optimum conditions for WMP extraction (sonication temperature = 47.82 °C, sonication time = 31.63 min, and ethanol concentration = 42.84%) yielded maximum TPC (7.944 mg GAE/100 mL) and antiradical activity (85.150%) while UAE at 50.32 °C, 37.60 min, and 39.18% ethanol yielded maximum TPC (32.152 mg GAE/100 mL) and antiradical activity (85.947%) for WMS. The experimental values obtained matched well with the predicted values. Furthermore, of the nine phenolic acids studied, eight were identified and quantified by GC–MS analysis in WMS extracts while none were identified in WMP extracts.

The results showed significant (P

WOS: 000509151900003, The current study investigated the impact of sonication process on antioxidant activity, phenolic compounds, total phenolic, total flavonoid, oil contents, fatty acids profile, and tocopherols of terebinth (Pistacia terebinthus) fruits. The highest antioxidant activity (87.32%), total phenolic (251.25 mg/100 g) and flavonoid (3413.72 mg/100 g) contents were observed in terebinth fruits sonicated for 30 min. The oil contents of terebinth increased from 38.93% (control) to 42.60% (sonicated for 15 min) after sonication process. The quercetin and catechin were the chief phenolic compounds in P. terebinthus extracts and their values were increased from 129.09 to 467.28 mg/100 g (quercetin) and from 5.58 to 21.33 mg/100 g (catechin) in fruits sonicated for 30 min. The major fatty acids of terebinth fruit oil were oleic (48.02-49.15%), linoleic (22.28-23.48%) and palmitic (22.10-23.67%) and sonication processes did not affect the quantities of these fatty acids. gamma-Tocopherol was the most abundant isomer with the value of 63.95-122.03 mg/100 g in terebinth fruit oil. It could be concluded that pre-sonication for 30 min was more suitable for enhancing the antioxidants and phenolic compounds of P. terebinthus fruit., Deanship of Scientific Research at King Saud UniversityDeanship of Scientific Research at King Saud University [RG-1439-80], The authors extend their appreciation to the Deanship of Scientific Research at King Saud University for funding this work through research Group No (RG-1439-80).

The oil content of both 'raw' and hazelnut kernels was significantly (p < 0.05) reduced as the microwave power increased from 180 W to 360 W. The contents of fatty acids flucuated for all varieties with microwave power, with a significant (p < 0.05) increment observed for 'Sivri' hazelnut at 180 and 720 W. The maximum linoleic acid contents for 'Raw', 'Sivri' and 'Tombul' hazelnuts were found as 11.87%, 12.61% and 17.68% for nuts roasted at 540 W, unroasted and those roasted at 720 W, respectively. It was observed that K (9735.1 mg/kg) and Mg (2343.7 mg/kg) contents of the investigated samples were found at the maximum levels in unroasted 'Tombul' hazelnut, while the highest P (2845.0 mg/kg) and S (1795.3 mg/kg) contents are determined for hazelnut roasted at 720 W (p < 0.05). The highest Ca content in hazelnut kernel was also observed at 360 W with 2400.9 mg/kg. However, roasting process did not dramatically affect the mineral contents of samples.

The acidity values changed between 1.03 mgKOH/100g (control) and 1.11 mgKOH/100g (0.1% extract) for orange oil, 1.06 mgKOH/100g (0.5% extract) and 1.13 mgKOH/100g (0.1% extract) and 1.25 mgKOH/100g (0.5% extract) and 1.31 mgKOH/100g (control) for mandarin oil. The peroxide values were determined between1.37 meqO2/kg (0.5% extract) and 1.43 meqO2/kg (0.1% extract) for orange oil, between 1.24 meqO2/kg (control) and 1.27 meqO2/kg (0.1% extract) for lemon and 1.60 meqO2/kg (0.5% extract) and 1.71 meqO2/kg (control) in mandarin oil samples. The viscosity values of samples changed between 0.051 Pa.S (control) and 0.065 Pa.S (0.5% extract) for orange, 0.051 Pa.S (control) and 0.067 Pa.S (0.5% extract) lemon and 0.044 Pa.S (control) and 0.057 Pa.S (0.5% extract) in mandarin oil samples. At the end of storage study (28th day), the acidity values significantly changed, and their values ranged between 2.28 mgKOH/100g (0.5% extract) and 3.64 mgKOH/100g (control) in orange, 1.67 mgKOH/100g (0.5% extract) and 2.28 mgKOH/100g (control) in lemon and 1.74 mgKOH/100g (0.5% extract) and 2.36 mgKOH/100g (control) in mandarin oil samples. While peroxide values vary between 11.68 meqO2/kg (0.5% extract) and 32.57 meqO2/kg (control) for orange, 12.55 meqO2/kg (0.5% extract) and 34.63 meqO2/kg (control) for lemon and between 17.56 meqO2/kg (0.5% extract) and 37.81 meqO2/kg (control) for mandarin oils, viscosity values after 28 day storage changed between 0.123 Pa.S (0.5% extract) and 0.675 Pa.S (control) in orange, 0.257 Pa.S (0.5% extract) and 0.697 Pa.S (control) in lemon and 0.215 Pa.S (0.5% extract) and 0.728 Pa.S (control) in mandarin oil samples.

In this study, bioactive lipid components such as fatty acid composition, tocopherol and total phenolics content and antioxidant activity of few wild plant seed extracts were determined. The oil contents of seed samples changed between 3.75 g/100 g (Onobrychis viciifolia Scop) and 17.94 g/100 g (Pimpinella saxifrage L.). While oleic acid contents of seed oils change between 10.4% (Trifolium repens) and 29.5% (Onobrychis viciifolia Scop), linoleic acid contents of oil samples varied from 16.3% (Onobrychis viciifolia Scop) and 64.2% (Trifolium repens) (p < 0.05). While α-tocopherol contents of oil samples change between 2.112 (Pimpinella saxifrage L.) and 228.279 mg/100 g (Trifolium pratense), ɣ-tocopherol contents ranged from 0.466 (Phleum pratense) to 67.128 mg/100 g (Onobrychis viciifolia Scop). Also, α-tocotrienol contents of Onobrychis viciifolia Scop and Phleum pratense were 30.815 and 23.787 mg/100 g, respectively. Results showed some differences in total phenol contents and antioxidant activity values of extracts depending on plant species. The present study indicates that this seed oils are rich in fatty acid and tocopherol.

The oxidative stability of sunflower oil containing rosemary essential oil and extracts in the oil during frying were followed by measuring peroxide value. Variation in the values of L* of the frying oil containing extract was less than that of frying oil containing essential oil. a*-Value of the fried oil containing extract highly significant decreased. Increase in the value of b* of 1. and 2. frying oil with 0.5 % rosemary essential oil was less. b* Value of the frying oils containing rosemary extract increased compared to b* values of frying oils containing essential oil. b* Value of the frying oil that the essential oil of rosemary added showed less increase than b* value of the frying oil that extract of rosemary. The viscosity values of frying oils containing rosemary extract changed between 30.3 mPas (1. frying oil containing 0.5% extract) and 35.5 mPas (2. frying oil containing 0.5% extract). In addition, free fatty acidity values of frying oils containing essential oil at 0.1, 0.3 and 0.5% levels ranged from 0.160% (1. frying oil containing 0.5% essential oil) to 0.320% (1. frying oil containing 0.3% essential oil). Peroxide values of frying oils containing rosemary extracts were determined between 12.84 meq O2/kg (1. frying oil containing 0.1% extract) and 28.98 meq O2/kg (2. frying oil containing 0.1% extract). Peroxide value of frying made with 0.3 % the rosemary essential oil increased less than that of made with the raw sunflower oil (control) (p < 0.05). Whenever rosemary essential oil and rosemary extract compare, the essential oil seems to be more effective on the peroxide value of the frying oil. The essential oil of rosemary have been effected more from the extracts of rosemary on the oxidative stability of sunflower oil.

WOS: 000511905500025, PubMed: 31975726, Kiwi and pepino fruits are most valuable fruits as they contains substantial amounts of nutrients and bioactive compounds. These fruits exhibited several health potentials such as antioxidant, antiinflammatory, antiobesity, antihyperlipidemia, and anticancer properties. However, studies on the effect of microwave and conventional drying methods on the antioxidant activity and bioactive compounds of kiwi and pepino fruits are limited. Therefore, this study was conducted to assess the effect of microwave and oven drying methods on antioxidant activity, total phenolic, and phenolic compounds of kiwi and pepino fruits. Drying of the fruit samples was carried out using conventional (70 degrees C for 20 h) and microwave (720 W for 3 min) ovens. 1,1-diphenyl-2-picrylhydrazyl scavenging and colorimetric Folin-Ciocalteu assays were used to assess the antioxidant activity and total phenolic contents, respectively, of fresh and dried fruits. Both drying methods significantly (p < 0.05) decreased the moisture contents of both fruits compared to untreated controls. Concomitantly, drying methods also enhanced (p < 0.05) antioxidant activity and total phenolic content of both fruits with the highest improvement being observed for microwave-dried fruits compared to untreated controls. In addition, a significant increase was observed in catechin and 1,2-dihydroxybenzene content of kiwi and pepino after drying process. However, microwave drying method reduced the amount of 3,4-dihydroxybenzoic acid in kiwi (ranging from 34.120 to 9.350 mg/100 g) and pepino (varied from 33.414 to 15.445 mg/100 g). Generally, the highest antioxidant activity and phenolic contents were reported in microwave oven dried samples, followed by samples dried in oven and fresh fruits. The results revealed that microwave drying could be more useful in fruit drying than conventional drying. In addition, dried kiwi and pepino fruits contains substantial quantities of phenolic compounds with high antioxidant activity compared to fresh fruits, and thus they are considered as healthy food.

WOS: 000478678800043, The current study presents physico-chemical attributes, fatty acid, sterol and tocopherol compositions in oils obtained from Moringa seed using either cold-press or Soxhlet extraction systems. Moringa oleifera and M. peregrina seed oils, recovered using cold press (CP) and Soxhlet extraction (SE) techniques, contained substantial amount of oleic acid (75.49 and 74.62% in CP 73.83 and 71.67% in SE) showing significant (p < .05) differences. Palmitic acid contents of M. oleifera and M. peregrina oils were 9.58 and 11.74% in case of CP and 12.27 and 12.84% in SE. The alpha-tocopherol contents of M. oleifera and M. peregrina oils obtained using these two techniques were 139.61 and 137.89 mg/kg in CP and 142.74 and 151.67 mg/kg in SE systems. Stigmasterol contents of M. oleifera and M. peregrina oils obtained with cold press and Soxhlet extraction system were found as 19.62 and 17.84% to 18.54 and 15.41%, respectively. (C) 2019 SAAB. Published by Elsevier B.V. All rights reserved., Deanship of Scientific Research at King Saud UniversityDeanship of Scientific Research at King Saud University [RG-1439-016], The authors would like to extend their sincere appreciation to the Deanship of Scientific Research at King Saud University for its funding this work through research group no. RG-1439-016.

WOS: 000490028900058, PubMed: 31368072, While Cd contents of cigarettes are determined between 0.44 (C8) and 1.55 mg/kg (C7), Co contents of cigarette samples varied between 0.26 (B5) and 2.19 mg/kg (B3). Also, while Cr contents of tested cigarettes are determined between 0.88 mg/kg (C5) and 1.72 mg/kg (B2), Mo contents of cigarettes ranged from 0.39 (C7) to 1.13 mg/kg (B2). In addition, Cu contents of cigarettes varied between 10.36 (C11) and 30.47 mg/kg (C18), while Fe contents of cigarette samples range between 306.03 (C5) and 595.42 mg/kg (C16). In addition, while Ni contents of cigarettes vary between 1.00 (C7) and 3.17 mg/kg (C1), Pb contents of brands varied between 0.16 (B4) and 7.37 mg/kg (B1). In general, Indian and imported cigarette samples used in Turkey are rich in Ca, K, Mg, P, and S. In Indian samples, B4 and B5 cigarette samples contained lower heavy metals compared with other cigarettes., Deanship of Scientific Research at King Saud UniversityDeanship of Scientific Research at King Saud University [RG-1435-049], The authors would like to extend their sincere appreciation to the Deanship of Scientific Research at King Saud University for funding the research group (no. RG-1435-049).

WOS: 000473260500006, The objective of the present work was to investigate the influence of locations on bioactive propertiest, phenolic compounds and mineral contents of bee pollens. The oil content of pollen grains changed between 3.50% (Alanya) and 6.85% (Russia-Perm Region). The highest total phenolic content (720 mg/100g) and antioxidant activity values (81.4%) were observed in pollens obtained from the Russia-Perm Region and Alanya districts, respectively. Additionally, the highest carotenoid was found in a pollen sample collected from Karaman (Sanveliler) (98.6 mg/g). The major phenolic compounds were (+)-catechin (66.75-337.39 mg/100g) and quercetin (61.2-1221.7 mg/100g) in all pollen samples. The pollen samples were observed to be a significant source of potassium (3846-6287 mg/kg), phosphorus (2947-5010 mg/kg), calcium (1022-2424 mg/kg) and sulfur (1744-2397 mg/kg). All of the analysis results were significantly affected by supplying locations. The antioxidant activity values of pollens were found partly similar and varied depending on locations. The content of saturated fatty acid (palmitic) was high (20-30%) in the tested pollen samples but did not exceed the content of linoleic acid., Deanship of Scientific Research at King Saud UniversityDeanship of Scientific Research at King Saud University [RG-1435-049], The authors would like to sincerely appreciate the Deanship of Scientific Research at King Saud University for funding this Research group No (RG-1435-049).

WOS: 000468273400005, PubMed: 31168120, The effect of harvest periods on total phenol, antioxidant activity, individual phenolic compounds of fruit and leaves of Tavan Yurei, Memecik, Edremit, Ayvalk and Gemlik olive varieties grown in Turkey were investigated. The highest total phenol (317.70mg/100g and 2657.81mg/100g) were observed in Tavan Yurei olive fruit and Ayvalk leaves harvested in December, respectively. The highest antioxidant activities (83.84%) were determined in Edremit fruit harvested in August and 83.33% in either Edremit olive leaves harvested in November and Tavan Yurei leaves harvested in December. The olive fruit contained gallic acid ranging from 7.18mg/100g (August) to 35.85mg/100g (December) in case of Ayvalk and 2.09mg/100g (November) to 21.62mg/100g (December) in Edremit. Gemlik olives showed higher gallic acid contents compared to the other varieties, however it depended significantly on harvest time in all cases. 3,4-Dihydroxybenzoic acid contents ranged from 33.11mg/100g (October) to 25.17mg/100g (September) in Memecik olives; 12.17mg/100g (August) to 33.11mg/100g (December) in case of Tavan Yurei olives depending on harvest time. The 3,4-dihydroxybenzoic acid contents of Memecik leaves ranged between 122.25mg/100g (September) to 196.58mg/100g (August) and that of Tavan Yurei leaves changed between 99.38mg/100g (November) and 179.90mg/100g (August). The leaves of these two varieties contained significantly (p, Deanship of Scientific Research at King Saud UniversityDeanship of Scientific Research at King Saud University [RG-1435-049], The authors would like to extend their sincere appreciation to the Deanship of Scientific Research at King Saud University for its funding the Research Group No. (RG-1435-049).

Saudi Arabia is one of the major producers of date (Phoenix dactylifera) fruit. Date fruit flesh is considered a healthy food due to the presence of natural antioxidants. Green and innovative supercritical fluid (SFE, 52.5 °C temperature, 27.50 MPa pressure, 5 mL CO2/min flow rate) and subcritical (SubCO2, 250 extraction cycles, 29 °C temperature, 6.8 MPa, 12 h, ethanol solvent) extraction techniques were used to produce flesh extracts from four Saudi date fruits (Sukari (SKFE), Ambara (AMFE), Majdool (MJFE) and Sagai (SGFE)), and extracts prepared using 6 h Soxhlet extraction at 70 °C for 16 h using n-hexane as solvent, were taken as control. SFE produced the highest (p < 0.05) extract yields, whereas the SubCO2 method recovered significantly higher (p < 0.05) amounts of phytochemicals. Total phenolics (186.37–447.31 mg GAE/100 g), total flavonoids (82.12–215.28 mg QE/100 g), total anthocyanins (0.41–1.34 mg/100 g), and total carotenoid (1.24–2.85 mg BCE/100 g) were quantified in all the flesh extracts. The biological properties evaluation showed that flesh extracts had high antioxidant (17.79–45.08 µg AAE/mL), antiradical (191.36–34.66 µg/mL DPPH IC50), ferric-reducing (2.18–5.01 mmol TE/100 g) and ABTS-scavenging (444.75–883.96 µmol TE/100 g) activities. SubCO2 was the best technique and Majdool the best date variety, in terms of both phytochemicals and biological properties.

Caper seed oil obtained by the soxhlet extraction had significantly (p