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The aim of the present paper was to investigate microstructure and texture evolution of two single crystals and polycrystal of Cu-8.5%at.Al material. All of mentioned samples were deformed by HE to achieve true strain ε = 1.17. For microstructure analyzes observations by transmission electron microscope (STEM) were done. Crystalline size for samples after SPD were determine using XRD method. The global texture measurements were done using Bruker D8 Discover diffractometer equipped in Cr radiation. Microstructure investigations revealed nanocrystalline structure in single crystals with initial orientations and and polycrystalline Cu-8.5%at.Al material after SPD. The global texture measurements have shown the stability of initial orientation of Cu-8.5%at.Al single crystal after HE, whereas the same SPD process strongly brakes up the orientation Cu-8.5%at. Al single crystal.

The presented results describe the effect of severe plastic deformation on the structure and mechanical properties of AA5083 and AA5754 alloys. Both materials were subjected to single hydrostatic extrusion (HE) and cumulative hydrostatic extrusion in the case of AA5083 and a combination of plastic deformation by equal-channel angular pressing (ECAP) with the next HE for AA5754. After the deformation, both alloys featured a homogeneous and finely divided microstructure with average grain size deq = 140 nm and 125 nm for AA5083 and AA5754, respectively. The selection of plastic forming parameters enabled a significant increase in the UTS tensile strength and YS yield stress in both alloys - UTS = 510 MPa and YS = 500 MPa for alloy AA5083 after cumulative HE, and 450 MPa and 440 MPa for alloy AA5754 after the combination of ECAP and HE, respectively. It has been shown on the example of AA5083 alloy that after the deformation the threads of the fasteners made of this material are more accurate and workable at lower cutting speeds, which saves the cutting tools. The resultant properties of AA5083 and AA5754 alloys match the minimum requirements for the strongest Al-Zn alloys of the 7xxx series, which, however, due to the considerably lower corrosion resistance, can be replaced in many responsible structures by the AA5xxx series Al-Mg alloys presented in this paper. [ABSTRACT FROM AUTHOR]

The study attempts to investigate the influence of severe plastic deformation (SPD in the hydrostatic extrusion (HE) process on the anisotropy of the structure and mechanical properties of the AA 6060 alloy. Material in isotropic condition was subjected to a single round of hydrostatic extrusion with three different degrees of deformation ( ε = 1.23, 1.57, 2.28). They allowed the grain size to be fragmented to the nanocrystalline level. Mechanical properties of the AA 6060 alloy, examined on mini-samples, showed an increase in ultimate tensile strength (UTS) and yield strength (YS) as compared to the initial material. Significant strengthening of the material results from high grain refinement in transverse section, from »220 μm in the initial material to »300 nm following the HE process. The material was characterized by the occurrence of structure anisotropy, which may determine the potential use of the material. Static tensile tests of mini-samples showed »10% anisotropy of properties between longitudinal and transverse cross-sections. In the AA6060 alloy, impact anisotropy was found depending on the direction of its testing. Higher impact toughness was observed in the cross-section parallel to the HE direction. The results obtained allow to analyze the characteristic structure created during the HE process and result in more efficient use of the AA 6060 alloy in applications. [ABSTRACT FROM AUTHOR]

The broad range applications of Ultra-Fine Grained metals is substantially limited by the lack of a welding method that allows them to be joined without losing the strong refinement of structure. From this point of view, the solid state welding processes are privileged. Friction welding tests were carried out on UFG 316L stainless steel. A joining process at high temperature activates the recrystallization, therefore the friction welding parameters were selected according to the criterion of the lowest degree of weakness due to recrystallization in the heat affected zone. In order to characterize the structure of basic material and selected areas of the obtained joint, were performed SEM, TEM and metallographic examinations in terms of hardness and range of softening of the material and tensile test. Despite the short time and relatively low welding temperature, results of the test by scanning electron microscopy and transmission electron microscopy confirmed the loss of the primary ultrafine structure in the Heat Affected Zone of welded joint. [ABSTRACT FROM AUTHOR]

Nickel and copper were subject to severe plastic deformation at room temperature, using hydrostatic extrusion (HE) and equal-channel angular pressing (ECAP). The maximum deformation was 13.5 in nickel and 22.3 in copper. These deformations were obtained by each of the techniques separately and by their combination. It has been found that the combined HE and ECAP deformation greatly increases the homogeneity of the microstructure and improves considerably its mechanical properties comparing with a single technique. After the combined treatment, the grain size of both copper and nickel was of the order of 100 nm. The experiments have shown that the combination of HE and ECAP techniques permits producing homogeneous nanocrystalline materials of large volumes. [ABSTRACT FROM AUTHOR]

The goal of the present work is to demonstrate that a bulk, ultra-fine grained microstructure can be obtained by the hydrostatic extrusion process of a 99.5% technical purity of nickel. Deformation with the total true strain of 3.8 was performed at room temperature to a wire 3 mm in diameter. Microstructure was characterized by light microscopy, TEM, XRD and mechanical properties. Hydrostatic extrusion was shown to be an effective method of severe plastic deformation, which allows ultra-fine grained structures to be obtained within the deformed material. After cumulative hydrostatic extrusion, the yield stress tripled, reaching a maximum of 812 MPa with a moderate elongation of 13%. A mean subgrain size of 200 nm was observed, with a considerable diversity in the size of individual grains. For the final passes of hydrostatic extrusion, a slight decrease in the mechanical properties was observed, accompanied with an increase in crystallite size. This is explained in terms of thermal softening processes activated by the heat generated during hydrostatic extrusion. [ABSTRACT FROM AUTHOR]