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122 results on '"Huhn, T."'

1. Data publication: Describing chain-like assembly of ethoxygroup-functionalized organic molecules on Au(111) using high-throughput simulations

Author

(0000-0001-8679-5905) Lokamani, M., (0000-0003-1761-2591) Kelling, J., Ohmann, R., Meyer, J., Kühne, T., Cuniberti, G., Wolf, J., (0000-0002-9935-4428) Juckeland, G., Huhn, T., (0000-0003-4756-5239) Zahn, P., Moresco, F., (0000-0003-0455-1945) Gemming, S., (0000-0001-8679-5905) Lokamani, M., (0000-0003-1761-2591) Kelling, J., Ohmann, R., Meyer, J., Kühne, T., Cuniberti, G., Wolf, J., (0000-0002-9935-4428) Juckeland, G., Huhn, T., (0000-0003-4756-5239) Zahn, P., Moresco, F., and (0000-0003-0455-1945) Gemming, S.

Abstract

Bei diesem Datensatz handelt es sich um die Grundzustandsstruktur von PEEB auf Au(111) und die Inputdatei für DFTB+.

Published
2022

2. Data publication: Describing chain-like assembly of ethoxygroup-functionalized organic molecules on Au(111) using high-throughput simulations

Author

Lokamani, M., Kelling, J., Ohmann, R., Meyer, J., Kühne, T., Cuniberti, G., Wolf, J., Juckeland, G., Huhn, T., Zahn, P., Moresco, F., and Gemming, S.

Subjects
Meta-Structures, STM, DFTB, 1,4-bis(phenylethynyl)-2,5-bis(ethoxy)benzene (PEEB), High-Throughput
Abstract

Bei diesem Datensatz handelt es sich um die Grundzustandsstruktur von PEEB auf Au(111) und die Inputdatei für DFTB+.

Published
2022

3. A combined experimental and theoretical study of 1,4-bis(phenylethynyl)-2,5-bis(ethoxy)benzene adsorption on Au(111)

Author

Lokamani, M., Kelling, J., Ohmann, R., Meyer, J., Kühne, T., Cuniberti, G., Wolf, J., Huhn, T., Zahn, P., Moresco, F., and Gemming, S.

Subjects
1,4-bis(phenylethynyl)-2,5-bis(ethoxy)benzene, STM, Au(111), DFT
Abstract

The electronic and geometrical structure of 1,4-bis(phenylethynyl)-2,5-bis(ethoxy)benzene (PEEB) molecules adsorbed on a Au(111) surface is investigated by low temperature scanning tun- neling microscopy (STM) and scanning tunneling spectroscopy (STS) in conjunction with density- functional-based tight-binding (DFTB) simulations of the density of states and the interaction with the substrate. Our density functional theory calculations indicate that the PEEB molecule is ph- ysisorbed on the Au(111) substrate, with negligible distortion of the molecular geometry and charge transfer between molecule and substrate.

Published
2021

4. Describing chain-like assembly of ethoxygroup-functionalized organic molecules on Au(111) using high-throughput simulations

Author

(0000-0001-8679-5905) Lokamani, M., (0000-0003-1761-2591) Kelling, J., Ohmann, R., Meyer, J., Kühne, T., Cuniberti, G., Wolf, J., (0000-0002-9935-4428) Juckeland, G., Huhn, T., (0000-0003-4756-5239) Zahn, P., Moresco, F., (0000-0003-0455-1945) Gemming, S., (0000-0001-8679-5905) Lokamani, M., (0000-0003-1761-2591) Kelling, J., Ohmann, R., Meyer, J., Kühne, T., Cuniberti, G., Wolf, J., (0000-0002-9935-4428) Juckeland, G., Huhn, T., (0000-0003-4756-5239) Zahn, P., Moresco, F., and (0000-0003-0455-1945) Gemming, S.

Abstract

Due to the low corrugation of the Au(111) surface, 1,4-bis(phenylethynyl)-2,5-bis(ethoxy)benzene (PEEB) molecules can form quasi interlocked lateral patterns, which are observed in scanning tunneling microscopy (STM) experiments at low temperatures. We demonstrate a multi-dimensional clustering approach to quantify the anisotropic pair-wise interaction of molecules and explain these patterns. We perform high-throughput calculations to evaluate an energy function, which incorporates the adsorption energy of single PEEB molecules on the metal surface and the intermolecular interaction energy of a pair of PEEB molecules. The analysis of the energy function reveals, that, depending on coverage density, specific types of pattern are preferred which can potentially be exploited to form one-dimensional molecular wires on Au(111).

Published
2021

5. A combined experimental and theoretical study of 1,4-bis(phenylethynyl)-2,5-bis(ethoxy)benzene adsorption on Au(111)

Author

(0000-0001-8679-5905) Lokamani, M., (0000-0003-1761-2591) Kelling, J., Ohmann, R., Meyer, J., Kühne, T., Cuniberti, G., Wolf, J., Huhn, T., (0000-0003-4756-5239) Zahn, P., Moresco, F., (0000-0003-0455-1945) Gemming, S., (0000-0001-8679-5905) Lokamani, M., (0000-0003-1761-2591) Kelling, J., Ohmann, R., Meyer, J., Kühne, T., Cuniberti, G., Wolf, J., Huhn, T., (0000-0003-4756-5239) Zahn, P., Moresco, F., and (0000-0003-0455-1945) Gemming, S.

Abstract

The electronic and geometrical structure of 1,4-bis(phenylethynyl)-2,5-bis(ethoxy)benzene (PEEB) molecules adsorbed on a Au(111) surface is investigated by low temperature scanning tun- neling microscopy (STM) and scanning tunneling spectroscopy (STS) in conjunction with density- functional-based tight-binding (DFTB) simulations of the density of states and the interaction with the substrate. Our density functional theory calculations indicate that the PEEB molecule is ph- ysisorbed on the Au(111) substrate, with negligible distortion of the molecular geometry and charge transfer between molecule and substrate.

Published
2021

7. Anaerobic Degradation of the Plant Sugar Sulfoquinovose Concomitant With H2S Production : Escherichia coli K-12 and Desulfovibrio sp. Strain DF1 as Co-culture Model

Author

Burrichter, A, Denger, K, Franchini, P, Huhn, T, Müller, N, Spiteller, D, and Schleheck, D

Subjects
Microbiology (medical), ddc:570, Microbiology, anaerobic bacterial metabolism, sulfidogenesis, organosulfonate respiration, sulfoquinovosyldiacylglycerol, plant sulfolipid, biogeochemical carbon and sulfur cycle, gut microbiome, human health and disease, anaerobic bacterial metabolism, sulfidogenesis, organosulfonate respiration, sulfoquinovosyldiacylglycerol, plant sulfolipid, biogeochemical carbon and sulfur cycle, gut microbiome, human health and disease
Abstract

Sulfoquinovose (SQ, 6-deoxy-6-sulfoglucose) is produced by plants and other phototrophs and its biodegradation is a relevant component of the biogeochemical carbon and sulfur cycles. SQ is known to be degraded by aerobic bacterial consortia in two tiers via C3-organosulfonates as transient intermediates to CO2, water and sulfate. In this study, we present a first laboratory model for anaerobic degradation of SQ by bacterial consortia in two tiers to acetate and hydrogen sulfide (H2S). For the first tier, SQ-degrading Escherichia coli K-12 was used. It catalyzes the fermentation of SQ to 2,3-dihydroxypropane-1-sulfonate (DHPS), succinate, acetate and formate, thus, a novel type of mixed-acid fermentation. It employs the characterized SQ Embden-Meyerhof-Parnas pathway, as confirmed by mutational and proteomic analyses. For the second tier, a DHPS-degrading Desulfovibrio sp. isolate from anaerobic sewage sludge was used, strain DF1. It catalyzes another novel fermentation, of the DHPS to acetate and H2S. Its DHPS desulfonation pathway was identified by differential proteomics and demonstrated by heterologously produced enzymes: DHPS is oxidized via 3-sulfolactaldehyde to 3-sulfolactate (SL) by two NAD+-dependent dehydrogenases (DhpA, SlaB); the SL is cleaved by an SL sulfite-lyase known from aerobic bacteria (SuyAB) to pyruvate and sulfite. The pyruvate is oxidized to acetate, while the sulfite is used as electron acceptor in respiration and reduced to H2S. In conclusion, anaerobic sulfidogenic SQ degradation was demonstrated as a novel link in the biogeochemical sulfur cycle. SQ is also a constituent of the green-vegetable diet of herbivores and omnivores and H2S production in the intestinal microbiome has many recognized and potential contributions to human health and disease. Hence, it is important to examine bacterial SQ degradation also in the human intestinal microbiome, in relation to H2S production, dietary conditions and human health. published

Published
2018

8. Design rules for molecular electronics: Theoretical and experimental approach

Author

Lokamani, L., Kilibarda, F., Wolf, J., Zahn, P., Huhn, T., Gemming, S., and Erbe, A.

Subjects
MCBJ, Diarylethenes, photosensitive molecules, break junction, single molecule, photochromism, conductance modulation, molecular design rules, side group, molecular switch, conductance
Abstract

Diarylethenes, a class of photosensitive molecules which exhibit photochromism, can be switched between open- and closed-ring isomers. In break-junction experiments diarylethene derivatives in open and closed-ring forms can be distinguished by a low and high conductance state respectively with a difference in current levels of about one order of magnitude. Here, we explore the underlying design rules for modulating electronic transport in derivatives of diarylethene. In particular, we analyze the effect on molecular orbitals due to various electron accepting and donating groups and in turn the modulation of the conductance properties of single molecules attached to gold electrodes. We have demonstrated that the mechanically controllable break junction (MCBJ) technique can be used to classify and determine the properties of electronic transport through single organic molecules. We present an outlook on experimental methods for exploring the underlying design rules for diarylethene molecules and derivatives. As a result, we show how the addition of different side groups modifies electronic behavior of the molecules.

Published
2017

10. Optically controlled properties of nanoparticles stabilised by photochromic difurylethene-base diarylethenes

Author

Snegir, S., Mukha, I., Sysoiev, D., Lacaze, Emmanuelle, Huhn, T., Pluchery, O., Physico-chimie et dynamique des surfaces (INSP-E6), Institut des Nanosciences de Paris (INSP), Université Pierre et Marie Curie - Paris 6 (UPMC)-Centre National de la Recherche Scientifique (CNRS)-Université Pierre et Marie Curie - Paris 6 (UPMC)-Centre National de la Recherche Scientifique (CNRS), Chuiko Institute of Surface Chemistry, National Academy of Sciences of Ukraine (NASU), and University of Konstanz

Subjects
[PHYS.COND.CM-MS]Physics [physics]/Condensed Matter [cond-mat]/Materials Science [cond-mat.mtrl-sci], ComputingMilieux_MISCELLANEOUS
Abstract

International audience

Published
2016

13. Induced Conductance in Single-Molecule Junctions

Author

Sendler, T., Luka-Guth, K., Wieser, M., Lokamani, J. W., Mortensen, M., Gothelf, K., Helm, M., Gemming, S., Kerbusch, J., Scheer, E., Huhn, T., and Erbe, A.

Abstract

The goal of molecular electronics is the realization of integrated molecular circuits. For this purpose reliable contacts to single molecules have to be built and the characteristics of those junctions need to be investigated. We have demonstrated that the mechanically controllable break junction (MCBJ) technique is a suitable tool to study the electrical transport through molecular junctions and to analyze the electronic structure of the molecules. Furthermore, based on the use of complex molecules, we are able to control the conductance of single molecular junctions. On the one hand, molecular switches are transformed in-situ from a non-conductive “off”- to a conductive ”on”-state via light-irradiation of a well-defined wavelength. On the other hand molecule-metal complexes are turned from an isolating to a conductive state by introducing metal centers into the molecular structures. The findings provide a significant contribution to the development of functional molecular junctions.

Published
2015

15. Role of solvents in the electronic transport properties of single-molecule junctions

Author

Luka-Guth, K., Hambsch, S., Bloch, A., Ehrenreich, P., Briechle, B. M., Kilibarda, F., Sendler, T., Sysoiev, D., Huhn, T., Erbe, A., Scheer, E., Luka-Guth, K., Hambsch, S., Bloch, A., Ehrenreich, P., Briechle, B. M., Kilibarda, F., Sendler, T., Sysoiev, D., Huhn, T., Erbe, A., and Scheer, E.

Abstract

We report on an experimental study of the charge transport through tunnel gaps formed by adjustable gold electrodes immersed into different solvents which are commonly used in the field of molecular electronics (ethanol, toluene, mesitylene, 1,2,4-trichlorobenzene, isopropanol, toluene/tetrahydrofuran mixtures) for the study of single-molecule contacts of functional molecules. We present measurements of the conductance as a function of gap width, conductance histograms as well as current-voltage characteristics of narrow gaps and discuss them in terms of the Simmons model, which is the standard model for describing transport via tunnel barriers, and the resonant single-level model, often applied to single-molecule junctions. One of our conclusions is that stable junctions may form from solvents as well and that both conductance-distance traces and current-voltage characteristics have to be studied to distinguish between contacts of solvent molecules and of molecules under study.

Published
2016

16. In Situ Tuning the Conductance of Single Molecular Diarylethene Switches

Author

Sendler, T., Luka-Guth, K., Wieser, M., Lokamani, M., Wolf, J., Huhn, T., Scheer, E., Kerbusch, J., Gemming, S., and Erbe, A.

Abstract

A major goal of molecular electronics is the development and implementation of molecular electronic devices such as single molecular switches. In this work we present a detailed study of single diarylethene molecules that were in situ switched from their non-conductive to conductive state in the presence of gold nanoelectrodes via controlled light irradiation. The molecules were dissolved in two different solvents and measured with two different side-groups. Histograms of conductance traces were taken and complemented by extracting the relative position of the current carrying molecular level and its level broadening from current-voltage characteristics by means of the single level transport model. The obtained results show a clear light-induced ring forming isomerization, which is almost independent of the side-groups, while electron withdrawing side groups lead to a reduction of conductance, a decrease of the level broadening and an increased difference between the molecular level and the Fermi energy of the metals. Quantum chemical calculations of the light-induced switching processes correlate these observations with the fundamentally different low-lying electronic states of the opened and closed forms and their comparably small modification by the electron-withdrawing substituents.

Published
2014

17. Electrical Characterization of a Switchable Molecular Wire via Mechanically Controllable Break Junctions

Author

Sendler, T., Wieser, M., Wolf, J., Huhn, T., Scheer, E., Moresco, F., Grebing, J., Gemming, S., and Erbe, A.

Subjects
MCBJ, Molecular Electronics, Switchable Molecular Wire
Abstract

Molecular electronics has been a eld of big interest for the last years. Using the technique of mechanically controllable break junctions we characterize the Switchable Molecular Wire Oligo(phenylene ethynylene)-embedded Difurylperuorocyclopentenes (SMW) in liquid environment. Via light irradiation the SMW can be switched between two well-defined conductance states. Conductance and hysteresis measurements allow us to identify the two states providing the basis for a comprehensive study of the in situ switching process. Based on the analysis with the transport model assuming transport through a single molecular level, we confirm that a reliable contact of the molecules to the gold contacts is formed and extract the energy of the molecular levels and the coupling constants between molecule and electrodes.

Published
2014

19. Electrical Characterization of Single Organic Molecules via Mechanically Controllable Break Junctions

Author

Sendler, T., Wieser, M., Liu, S.-P., Weisbrod, S., Tang, Z., Marx, A., Wolf, J., Huhn, T., Scheer, E., Moresco, F., Grebing, J., and Erbe, A.

Subjects
Molecular Electronics, Electronic Transport
Abstract

Molecular electronics has been of big interest for the last years. To allow an electrical characterization of single molecules a reliable contact to gold atoms is required. We ensure this by using single organic molecules with a plain structure, in particular 1,4-Diethoxy-2,5-bis (4-sulfanyl-phenylethynyl)-benzene and single stranded DNA fragments, dissolved in an organic non-polar solvent. For measurements we use the technique of mechanically controllable break junctions. IV-curves taken from single molecules connected to single gold atom contacts show the expected tunneling behavior, from which we gain the energy of the molecular level and the coupling between electrode and molecule.

Published
2013

20. Electrical Characterization of Single Molecules via Mechanically Controllable Break Junctions

Author

Wieser, M., Sendler, T., Weisbrod, S., Tang, Z., Marx, A., Wolf, J., Huhn, T., Scheer, E., Moresco, F., Grebing, J., and Erbe, A.

Subjects
Molecular Electronics, Electronic Transport
Abstract

Molecular electronics has been a field of big interest for the last years. Using the technique of mechanically controllable break junctions we characterize different organic molecules, e.g. 1,4-Diethoxy-2,5-bis(4-sulfanyl-phenylethynyl)-benzene (PEEB) and switchable molecular wires, dissolved in an organic non-polar solvent. IV-curves taken from the molecules connected to single gold atom contacts show the expected tunneling behavior described by the single-level model: weak coupling of the molecules to the gold atoms implies an off-resonant tunneling process and a transport through a single channel. Varying the end-groups of the molecules leads to a different transport behavior. Figure 1 shows a 2D histogram of IV-curves of PEEB with amino end-groups. Based on the single-level transport model the analysis of the current-voltage characteristics delivers the energy of the molecular level and the coupling between electrode and molecule. It also indicates a reliable contact of the molecules to the gold atoms. A further goal is the investigation of an electric gate effect on the transport behavior through the molecules.

Published
2013

21. Current-voltage characteristics of single-molecule diarylethene junctions measured with adjustable gold electrodes in solution

Author

Briechle, B. M., Kim, Y., Ehrenreich, P., Erbe, A., Sysoiev, D., Huhn, T., Groth, U., Scheer, E., Briechle, B. M., Kim, Y., Ehrenreich, P., Erbe, A., Sysoiev, D., Huhn, T., Groth, U., and Scheer, E.

Abstract

We report on an experimental analysis of the charge transport through sulfur-free photochromic molecular junctions. The conductance of individual molecules contacted with gold electrodes and the current-voltage characteristics of these junctions are measured in a mechanically controlled break-junction system at room temperature and in liquid environment. We compare the transport properties of a series of molecules, labeled TSC, MN, and 4Py, with the same switching core but varying side-arms and end-groups designed for providing the mechanical and electrical contact to the gold electrodes. We perform a detailed analysis of the transport properties of TSC in its open and closed states. We find rather broad distributions of conductance values in both states. The analysis, based on the assumption that the current is carried by a single dominating molecular orbital, reveals distinct differences between both states. We discuss the appearance of diode-like behavior for the particul! ar species 4Py that features end-groups, which preferentially couple to the metal electrode by physisorption. We show that the energetic position of the molecular orbital varies as a function of the transmission. Finally, we show for the species MN that the use of two cyano end-groups on each side considerably enhances the coupling strength compared to the typical behavior of a single cyano group.

Published
2012

22. Revealing the role of anchoring groups in the electrical conduction through single-molecule junctions

Author

Zotti, L. A., Kirchner, T., Cuevas, J.-C., Pauly, F., Huhn, T., Scheer, E., Erbe, A., Zotti, L. A., Kirchner, T., Cuevas, J.-C., Pauly, F., Huhn, T., Scheer, E., and Erbe, A.

Abstract

A combined experimental and theoretical study is presented revealing the influence of metal-molecule coupling on electronic transport through single-molecule junctions. Transport experiments through tolane molecules attached to gold electrodes via thiol, nitro, and cyano anchoring groups are performed. By fitting the experimental current-voltage characteristics to a single-level tunneling model, we extract both the position of the molecular orbital closest to the Fermi energy and the strength of the metal-molecule coupling. The values found for these parameters are rationalized with the help of density-functional-theory-based transport calculations. In particular, these calculations show that the anchoring groups determine the junction conductance by controlling not only the strength of the coupling to the metal but also the position of the relevant molecular energy levels.

Published
2010

31. Design Challenges and Activation Concerns for ARIES Vacuum Vessel

Author

El-Guebaly, L., Huhn, T., Rowcliffe, A., and Malang, S.

Abstract

AbstractResearch has been conducted to find the optimal steel to use in the vacuum vessel (VV) of ARIES power plants. The VV should meet several design criteria, including activation and fabrication requirements. Seven different types of steel were examined in order to determine which steel would be the best candidate for the ARIES VV. The main concerns are related to activation, properties under irradiation, and fabrication of a sizable VV. Steels generating high-level waste (such as 316-SS) were excluded from possible material choices. As a VV material, there is the necessity for a carefully controlled the post-weld-heat-treatment at ~750°C after assembly, welding, and rewelding. For this particular reason, the F82H FS is not suitable for the ARIES VV. The newly developed 3Cr-3WV bainitic FS meets the activation requirements and has the potential to satisfy the fabrication requirements for the ARIES VV. It is recommended for further consideration because of several advantages over other candidate steels.

Published
2013
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32. Cyanopeptolin 954, a Chlorine-Containing Chymotrypsin Inhibitor of Microcystis aeruginosa NIVA Cya 43

Author

Elert, E. von, Oberer, L., Merkel, P., Huhn, T., and Blom, J. F.

Abstract

A new depsipeptide, cyanopeptolin 954 (1), was isolated from the freshwater cyanobacterium Microcystis aeruginosa NIVA Cya 43. The structure of the compound was elucidated by chemical and spectroscopic analyses, including 2D NMR and GC-MS of the hydrolysate. The major structural differences compared to previously characterized heptadepsipeptides of Microcystis are the replacement of the basic amino acid in position 4 by l-leucine, the presence of l-phenylalanine in position 6, and the uncommon residue 3‘-chloro-N-Me-l-tyrosine in position 7. Cyanopeptolin 954 inhibited chymotrypsin with an IC50 value of 45 nM. Nostopeptin BN920, formerly isolated from the cyanobacterium Nostoc,1 was isolated from the same strain of Microcystis, and a cis amide bond between Phe (6) and N-Me-Tyr (7) was shown. Nostopeptin BN920 inhibited chymotrypsin with an IC50 value of 31 nM.

Published
2005

33. Search for pair-production of long-lived heavy charged particles in $e^+ e^-$ annihilation

Author

Barate, R., Buskulic, D., Decamp, D., Ghez, P., Goy, C., Lees, J P., Lucotte, A., Minard, M N., Nief, J Y., Pietrzyk, B., Casado, M P., Chmeissani, M., Comas, P., Crespo, J M., Delfino, M., Fernandez, E., Fernandez-Bosman, M., Garrido, L., Juste, A., Martinez, M., Miquel, R., Mir, L M., Orteu, S., Padilla, C., Park, I C., Pascual, A., Perlas, J A., Riu, I., Sanchez, F., Teubert, F., Colaleo, A., Creanza, D., de Palma, M., Gelao, G., Iaselli, G., Maggi, G., Maggi, M., Marinelli, N., Nuzzo, S., Ranieri, A., Raso, G., Ruggieri, F., Selvaggi, G., Silvestris, L., Tempesta, P., Tricomi, A., Zito, G., Huang, X., Lin, J., Ouyang, Q., Wang, T., Xie, Y., Xu, R., Xue, S., Zhang, J., Zhang, L., Zhao, W., Abbaneo, D., Alemany, R., Bazarko, A O., Becker, U., Bright-Thomas, P., Cattaneo, M., Cerutti, F., Dissertori, G., Drevermann, H., Forty, R W., Frank, M., Hagelberg, R., Hansen, J B., Harvey, J., Janot, P., Jost, B., Kneringer, E., Knobloch, J., Lehraus, I., Lutters, G., Mato, P., Minten, A., Moneta, L., Pacheco, A., Pusztaszeri, J F., Ranjard, F., Rizzo, G., Rolandi, L., Schlatter, D., Schmitt, M., Schneider, O., Tejessy, W., Tomalin, I R., Wachsmuth, H., Wagner, A., Ajaltouni, Z., Barres, A., Boyer, C., Falvard, A., Ferdi, C., Gay, P., Guicheney, C., Henrard, P., Jousset, J., Michel, B., Monteil, S., Montret, J C., Pallin, D., Perret, P., Podlyski, F., Proriol, J., Rosnet, P., Rossignol, J M., Fearnley, T., Hansen, J D., Hansen, J R., Hansen, P H., Nilsson, B S., Rensch, B., Waananen, A., Daskalakis, G., Kyriakis, A., Markou, C., Simopoulou, E., Vayaki, A., Blondel, A., Brient, J C., Machefert, F., Rouge, A., Rumpf, M., Valassi, A., Videau, H., Focardi, E., Parrini, G., Zachariadou, K., Cavanaugh, R., Corden, M., Georgiopoulos, C., Huhn, T., Jaffe, D E., Antonelli, A., Bencivenni, G., Bologna, G., Bossi, F., Campana, P., Capon, G., Casper, D., Chiarella, V., Felici, G., Laurelli, P., Mannocchi, G., Murtas, F., Murtas, G P., Passalacqua, L., Pepe-Altarelli, M., Curtis, L., Dorris, S J., Halley, A W., Knowles, I G., Lynch, J G., O'Shea, V., Raine, C., Scarr, J M., Smith, K., Teixeira-Dias, P., Thompson, A S., Thomson, E., Thomson, F., Turnbull, R M., Geweniger, C., Graefe, G., Hanke, P., Hansper, G., Hepp, V., Kluge, E E., Putzer, A., Schmidt, M., Sommer, J., Tittel, K., Werner, S., Wunsch, M., Beuselinck, R., Binnie, D M., Cameron, W., Dornan, P J., Girone, M., Goodsir, S., Martin, E B., Morawitz, P., Moutoussi, A., Nash, J., Sedgbeer, J K., Stacey, A M., Williams, M D., Girtler, P., Kuhn, D., Rudolph, G., Betteridge, A P., Bowdery, C K., Colrain, P., Crawford, G., Finch, A J., Foster, F., Hughes, G., Jones, R W L., Sloan, T., Whelan, E P., Williams, M I., Hoffmann, C., Jakobs, K., Kleinknecht, K., Quast, G., Renk, B., Rohne, E., Sander, H G., Van Gemmeren, P., Zeitnitz, C., Aubert, J.J., Benchouk, C., Bonissent, A., Bujosa, G., Calvet, D., Carr, J., Coyle, P., Diaconu, C., Konstantinidis, N., Leroy, O., Motsch, F., Payre, P., Rousseau, D., Talby, M., Sadouki, A., Thulasidas, M., Tilquin, A., Trabelsi, K., Aleppo, M., Ragusa, F., Berlich, R., Blum, W., Buscher, V., Dietl, H., Ganis, G., Gotzhein, C., Kroha, H., Lutjens, G., Lutz, G., Manner, W., Moser, H G., Richter, R H., Rosado-Schlosser, A., Schael, S., Settles, R., Seywerd, H C J., Stenzel, H., Wiedenmann, W., Wolf, G., Boucrot, J., Callot, O., Chen, S., Cordier, A., Davier, M., Duflot, L., Grivaz, J F., Heusse, P., Hocker, A., Jacholkowska, A., Jacquet, M., Kim, D W., Le Diberder, F., Lefrancois, J., Lutz, A M., Nikolic, I., Schune, M H., Simion, S., Tournefier, E., Veillet, J J., Videau, I., Zerwas, D., Azzurri, P., Bagliesi, G., Batignani, G., Bettarini, S., Bozzi, C., Calderini, G., Carpinelli, M., Ciocci, M A., Ciulli, V., Dell'Orso, R., Fantechi, R., Ferrante, I., Giassi, A., Gregorio, A., Ligabue, F., Lusiani, A., Marrocchesi, P S., Messineo, A., Palla, F., Sanguinetti, G., Sciaba, A., Spagnolo, P., Steinberger, J., Tenchini, R., Tonelli, G., Vannini, C., Venturi, A., Verdini, P G., Blair, G A., Bryant, L M., Chambers, J T., Gao, Y., Green, M G., Medcalf, T., Perrodo, P., Strong, J A., Von Wimmersperg-Toeller, J H., Botterill, D R., Clifft, R W., Edgecock, T R., Haywood, S., Maley, P., Norton, P R., Thompson, J C., Wright, A E., Bloch-Devaux, B., Colas, P., Fabbro, B., Kozanecki, W., Lancon, E., Lemaire, M C., Locci, E., Perez, P., Rander, J., Renardy, J F., Rosowsky, A., Roussarie, A., Schuller, J P., Schwindling, J., Trabelsi, A., Vallage, B., Black, S N., Dann, J H., Kim, H Y., Litke, A M., McNeil, M A., Taylor, G., Booth, C N., Boswell, R., Brew, C A J., Cartwright, S L., Combley, F., Kelly, M S., Lehto, M H., Newton, W M., Reeve, J., Thompson, L F., Affholderbach, K., Bohrer, A., Brandt, S., Cowan, G D., Foss, J., Grupen, C., Saraiva, P., Smolik, L., Stephan, F., Apollonio, M., Bosisio, L., Della Marina, R., Giannini, G., Gobbo, B., Musolino, G., Putz, J., Rothberg, J E., Wasserbaech, S., Williams, R W., Armstrong, S R., Charles, E., Elmer, P., 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Abstract

A search for pair-production of long-lived, heavy, singly-charged particles has been performed with data collected by the ALEPH detector at a centre-of-mass energy of 172 GeV. Data at \sqrt{s} = 161, 136, and 130 GeV are also included to improve the sensitivity to lower masses. No candidate is found in the data. A model-independent 95 % confidence level upper limit on the production cross section at 172 GeV of 0.2-0.4 pb is derived for masses between 45 and 86 GeV/c^2. This cross section limit implies, assuming the MSSM, a lower limit of 67 (69) GeV/c^2 on the mass of right- (left-) handed long-lived scalar taus or scalar muons and of 86 GeV/c^2 on the mass of long-lived charginos.

38. Unveiling the strong interaction among hadrons at the LHC

Author

Acharya, Shreyasi, Adamova, Dagmar, Ahn, Sang Un, Bhattacharjee, Buddhadeb, Yurchenko, Volodymyr, Zaccolo, Valentina, Zaman, Ali, Zampolli, Chiara, Correia Zanoli, Henrique Jose, Zardoshti, Nima, Zarochentsev, Andrey, Zavada, Petr, Zavyalov, Nikolay, Zbroszczyk, Hanna Paulina, Bianchi, Antonio, Zhalov, Mikhail, Zhang, Song, Zhang, Xiaoming, Zhang, Zuman, Zherebchevskii, Vladimir, Yu, Zhi, Zhou, Daicui, Zhou, You, Zhou, Zhuo, Zhu, Jianhui, Bianchi, Livio, Zhu, Ya, Zichichi, Antonino, Zinovjev, Gennady, Zurlo, Nicola, ALICE Collaboration, Bianchi, Nicola, Bielcik, Jaroslav, Bielcikova, Jana, Bilandzic, Ante, Biro, Gabor, Biswas, Rathijit, Biswas, Saikat, Akbar, Zaenal, Blair, Justin Thomas, Blau, Dmitry, Blume, Christoph, Boca, Gianluigi, Bock, Friederike, Bogdanov, Alexey, Boi, Stefano, Bok, Jeongsu, Boldizsar, Laszlo, Bolozdynya, Alexander, Akindinov, Alexander, Bombara, Marek, Bonomi, Germano, Borel, Herve, Borissov, Alexander, Bossi, Hannah, Botta, Elena, Bratrud, Lars, Braun-munzinger, Peter, Bregant, Marco, Broz, Michal, Al-turany, Mohammad, Bruna, Elena, Bruno, Giuseppe Eugenio, Buckland, Matthew Daniel, Budnikov, Dmitry, Buesching, Henner, Bufalino, Stefania, Bugnon, Ophelie, Buhler, Paul Alois, Buncic, Predrag, Buthelezi, Edith Zinhle, Alam, Sk Noor, Bashir Butt, Jamila, Bysiak, Sebastian Adam, Caffarri, Davide, Caliva, Alberto, Calvo Villar, Ernesto, Mejia Camacho, Juan Manuel, Soto Camacho, Rabi, Camerini, Paolo, De Moraes Canedo, Fabio, Capon, Aaron Allan, Silva De Albuquerque, Danilo, Carnesecchi, Francesca, Caron, Robin Albert Andre, Castillo Castellanos, Javier Ernesto, Castro, Andrew John, Casula, Ester Anna Rita, Catalano, Fabio, Ceballos Sanchez, Cesar, Chakraborty, Pritam, Chandra, Sinjini, Chang, Wan, Aleksandrov, Dmitry, Chapeland, Sylvain, Chartier, Marielle, Chattopadhyay, Subhasis, Chattopadhyay, Sukalyan, Chauvin, Alex Henri Jean, Cheshkov, Cvetan Valeriev, Cheynis, Brigitte, Chibante Barroso, Vasco Miguel, Dobrigkeit Chinellato, David, Cho, Soyeon, Alessandro, Bruno, Chochula, Peter, Chowdhury, Tasnuva, Christakoglou, Panagiotis, Christensen, Christian Holm, Christiansen, Peter, Chujo, Tatsuya, Cicalo, Corrado, Cifarelli, Luisa, De Cilladi, Lorenzo, Cindolo, Federico, Alfanda, Haidar Mas'ud, Ciupek, Michael Rudolf, Clai, Giulia, Cleymans, Jean Willy Andre, Colamaria, Fabio Filippo, Colella, Domenico, Collu, Alberto, Colocci, Manuel, Concas, Matteo, Conesa Balbastre, Gustavo, Conesa Del Valle, Zaida, Alfaro Molina, Jose Ruben, Contin, Giacomo, Contreras Nuno, Jesus Guillermo, Cormier, Thomas Michael, Corrales Morales, Yasser, Cortese, Pietro, Cosentino, Mauro Rogerio, Costa, Filippo, Costanza, Susanna, Crochet, Philippe, Cuautle Flores, Eleazar, Adler, Alexander, Ali, Bushra, Cui, Pengyao, Cunqueiro Mendez, Leticia, Dabrowski, Daniel, Dahms, Torsten, Dainese, Andrea, Damas, Florian Paul Andre, Danisch, Meike Charlotte, Danu, Andrea, Das, Debasish, Das, Indranil, Ali, Yasir, Das, Prottay, Das, Prottoy, Das, Supriya, Dash, Ajay Kumar, Dash, Sadhana, De, Sudipan, De Caro, Annalisa, De Cataldo, Giacinto, De Cuveland, Jan, De Falco, Alessandro, Alici, Andrea, De Gruttola, Daniele, De Marco, Nora, De Pasquale, Salvatore, Deb, Suman, Franz Degenhardt, Hermann, Deja, Kamil Rafal, Deloff, Andrzej, Delsanto, Silvia, Deng, Wenjing, Dhankher, Preeti, Alizadehvandchali, Negin, Di Bari, Domenico, Di Mauro, Antonio, Arteche Diaz, Raul, Dietel, Thomas, Raisig, Pascal, Ding, Yanchun, Divia, Roberto, Dixit, Dhruv Utpalkumar, Djuvsland, Oeystein, Dmitrieva, Uliana, Alkin, Anton, Dobrin, Alexandru Florin, Donigus, Benjamin, Dordic, Olja, Dubey, Anand Kumar, Dubla, Andrea, Dudi, Sandeep, Mallick, Dukhishyam, Dupieux, Pascal, Ehlers Iii, Raymond James, Eikeland, Viljar Nilsen, Alme, Johan, Elia, Domenico, Erazmus, Barbara Ewa, Erhardt, Filip, Erokhin, Andrey, Ersdal, Magnus Rentsch, Espagnon, Bruno, Eulisse, Giulio, Evans, David, Evdokimov, Sergey, Fabbietti, Laura, Alt, Torsten, Faggin, Mattia, Faivre, 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Vladimir, Izucheev, Vladimir, Jacak, Barbara, Aggarwal, Madan Mohan, Aphecetche, Laurent Bernard, Jacazio, Nicolo, Jacobs, Peter Martin, Jadlovska, Slavka, Jadlovsky, Jan, Jaelani, Syaefudin, Jahnke, Cristiane, Jakubowska, Monika Joanna, Janik, Malgorzata Anna, Janson, Thomas, Jercic, Marko, Appelshaeuser, Harald, Jevons, Oliver Thomas, Jin, Muqing, Jonas, Florian, Jones, Peter Graham, Jung, Jerome, Jung, Michael, Jusko, Anton, Kalinak, Peter, Kalweit, Alexander Philipp, Kaplin, Vladimir, Arcelli, Silvia, Kar, Somnath, Karasu Uysal, Ayben, Karatovic, David, Karavichev, Oleg, Karavicheva, Tatiana, Karczmarczyk, Przemyslaw, Karpechev, Evgeny, Kazantsev, Andrey, Kebschull, Udo Wolfgang, Keidel, Ralf, Arnaldi, Roberta, Keil, Markus, Ketzer, Bernhard Franz, Khabanova, Zhanna, Khan, Ahsan Mehmood, Khan, Shaista, Khanzadeev, Alexei, Kharlov, Yury, Khatun, Anisa, Khuntia, Arvind, Kileng, Bjarte, Arratia Munoz, Miguel Ignacio, Kim, Beomkyu, Kim, Byungchul, Kim, Daehyeok, Kim, Dong Jo, Kim, Eun Joo, Kim, Hyeonjoong, Kim, Jaehyun, Kim, Jinsook, Kim, Jiyoung, Kim, Jungeol, Arsene, Ionut Cristian, Kim, Junlee, Kim, Minjung, Kim, Se Yong, Kim, Taejun, Kim, Taesoo, Kirsch, Stefan, Kisel, Ivan, Kiselev, Sergey, Kisiel, Adam Ryszard, Klay, Jennifer Lynn, Arslandok, Mesut, Klein, Carsten, Klein, Jochen, Klein, Spencer Robert, Klein-boesing, Christian, Kleiner, Matthias, Kluge, Alexander, Knichel, Michael Linus, Knospe, Anders Garritt, Kobdaj, Chinorat, Kohler, Markus Konrad, Augustinus, Andre, Kollegger, Thorsten Sven, Kondratyev, Andrey, Kondratyeva, Natalia, Kondratyuk, Evgeny, Konig, Joshua Leon, Konigstorfer, Stephan Alexander, Konopka, Piotr Jan, Kornakov, Georgui, Koska, Lukas, Kovalenko, Oleksandr, Averbeck, Ralf Peter, Kovalenko, Vladimir, Kowalski, Marek, Kralik, Ivan, Kravcakova, Adela, Kreis, Lukas, Krivda, Marian, Krizek, Filip, Krizkova Gajdosova, Katarina, Kruger, Mario, Kryshen, Evgeny, Aziz, Sizar, Krzewicki, Mikolaj, Kubera, Andrew Michael, Kucera, Vit, Kuhn, Christian Claude, Kuijer, Paulus Gerardus, Kumar, Lokesh, Kundu, Sourav, Kurashvili, Podist, Kurepin, Alexander, Kurepin, Alexey, Aglieri Rinella, Gianluca, Azmi, Mohd Danish, Kuryakin, Alexey, Kushpil, Svetlana, Kvapil, Jakub, Kweon, Min Jung, Kwon, Jiyeon, Kwon, Youngil, La Pointe, Sarah Louise, La Rocca, Paola, Lai, Yue Shi, Lamanna, Massimo, Badala, Angela, Langoy, Rune, Lapidus, Kirill, Lardeux, Antoine Xavier, Larionov, Pavel, Laudi, Elisa, Lavicka, Roman, Lazareva, Tatiana, Lea, Ramona, Leardini, Lucia, Lee, Joonil, Baek, Yongwook, Lee, Seongjoo, Lehner, Sebastian, Lehrbach, Johannes, Lemmon, Roy Crawford, Leon Monzon, Ildefonso, Lesser, Ezra Douglas, Lettrich, Michael, Levai, Peter, Li, Xiaomei, Li, Xing Long, Bagnasco, Stefano, Lien, Jorgen Andre, Lietava, Roman, Lim, Bong-hwi, Lindenstruth, Volker, Lindner, Amelia, Lippmann, Christian, Lisa, Michael Annan, Liu, Alwina Ruixin, Liu, Jian, Liu, Suyuan, Bai, Xiaozhi, Llope, William Joseph, Lofnes, Ingrid Mckibben, Loginov, Vitaly, Loizides, Constantinos, Loncar, Petra, Lopez Lopez, Jorge Andres, Lopez, Xavier Bernard, Lopez Torres, Ernesto, Luhder, Jens Robert, Lunardon, Marcello, Bailhache, Raphaelle Marie, Luparello, Grazia, Ma, Yugang, Maevskaya, Alla, Mager, Magnus, Mahmood, Sohail Musa, Mahmoud, Tariq, Maire, Antonin, Majka, Richard Daniel, Malaev, Mikhail, Malik, Qasim Waheed, Bala, Renu, Malinina, Liudmila, Mal Kevich, Dmitry, Malzacher, Peter, Mandaglio, Giuseppe, Manko, Vladislav, Manso, Franck, Manzari, Vito, Mao, Yaxian, Marchisone, Massimiliano, Mares, Jiri, Balbino, Alessandro, Margagliotti, Giacomo Vito, Margotti, Anselmo, Marin, Ana Maria, Markert, Christina, Marquard, Marco, De Martin, Chiara, Martin, Nicole Alice, Martinengo, Paolo, Martinez, Jacobb Lee, Martinez Hernandez, Mario Ivan, Baldisseri, Alberto, Martinez-garcia, Gines, Masciocchi, Silvia, Masera, Massimo, Masoni, Alberto, Massacrier, Laure Marie, Masson, Erwann, Mastroserio, Annalisa, Mathis, Andreas Michael, Matonoha, Oliver, 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Murakami, Hikari, Murray, Sean, Musa, Luciano, Musinsky, Jan, Myers, Corey James, Myrcha, Julian Wojciech, Naik, Bharati, Nair, Rahul Ramachandran, Nandi, Basanta Kumar, Barnafoldi, Gergely Gabor, Nania, Rosario, Nappi, Eugenio, Naru, Muhammad Umair, Nassirpour, Adrian Fereydon, Nattrass, Christine, Nayak, Ranjit, Nayak, Tapan Kumar, Nazarenko, Sergey, Neagu, Alexandra, Negrao De Oliveira, Renato Aparecido, Barnby, Lee Stuart, Nellen, Lukas, Nesbo, Simon Voigt, Neskovic, Gvozden, Nesterov, Dmitrii, Neumann, Lukasz Tomasz, Nielsen, Borge Svane, Nikolaev, Sergey, Nikulin, Sergey, Nikulin, Vladimir, Noferini, Francesco, Ramillien Barret, Valerie, Nomokonov, Petr, Norman, Jaime, Novitzky, Norbert, Nowakowski, Piotr, Nyanin, Alexander, Nystrand, Joakim Ingemar, Ogino, Masanori, Ohlson, Alice Elisabeth, Oleniacz, Janusz, Oliveira Da Silva, Antonio Carlos, Bartalini, Paolo, Oliver, Michael Henry, Oppedisano, Chiara, Ortiz Velasquez, Antonio, Oskarsson, Anders Nils Erik, Otwinowski, Jacek Tomasz, Oyama, Ken, Pachmayer, Yvonne Chiara, Pacik, Vojtech, Padhan, Sonali, Pagano, Davide, Bartels, Clara, Paic, Guy, Pan, Jinjin, Panebianco, Stefano, Pareek, Pooja, Park, Jonghan, Parkkila, Jasper Elias, Parmar, Sonia, Pathak, Surya Prakash, Paul, Biswarup, Pazzini, Jacopo, Barth, Klaus, Pei, Hua, Peitzmann, Thomas, Peng, Xinye, Pereira, Luis Gustavo, Pereira Da Costa, Hugo Denis Antonio, Peresunko, Dmitry Yurevich, Mesa Perez, Guillermo, Perrin, Sebastien, Pestov, Yury, Petracek, Vojtech, Agrawal, Neelima, Bartsch, Esther, Petrovici, Mihai, Peretti Pezzi, Rafael, Piano, Stefano, Pikna, Miroslav, Pillot, Philippe, Pinazza, Ombretta, Pinsky, Lawrence, Pinto, Chiara, Pisano, Silvia, Pistone, Daniele, Baruffaldi, Filippo, Ploskon, Mateusz Andrzej, Planinic, Mirko, Pliquett, Fabian, Poghosyan, Martin, Polishchuk, Boris, Poljak, Nikola, Pop, Amalia, Porteboeuf, Sarah Julie, Pozdniakov, Valeriy, Prasad, Sidharth Kumar, Bastid, Nicole, Preghenella, Roberto, Prino, Francesco, Pruneau, Claude Andre, Pshenichnov, Igor, Puccio, Maximiliano, Putschke, Jorn Henning, Qiu, Shi, Quaglia, Luca, Quishpe Quishpe, Raquel Estefania, Ragoni, Simone, Basu, Sumit, Raha, Sibaji, Rajput, Sonia, Rak, Jan, Rakotozafindrabe, Andry Malala, Ramello, Luciano, Rami, Fouad, Rodriguez Ramirez, Saul Anibal, Raniwala, Rashmi, Raniwala, Sudhir, Rasanen, Sami Sakari, Batigne, Guillaume, Rath, Rutuparna, Ratza, Viktor, Ravasenga, Ivan, Read, Kenneth Francis, Redelbach, Andreas Ralph, Redlich, Krzysztof, Rehman, Attiq Ur, Reichelt, Patrick Simon, Reidt, Felix, Ren, Xiaowen, Batyunya, Boris, Renfordt, Rainer Arno Ernst, Jakubcinova, Zuzana, Reygers, Klaus Johannes, Riabov, Andrei, Riabov, Viktor, Richert, Tuva Ora Herenui, Richter, Matthias Rudolph, Riedler, Petra, Riegler, Werner, Riggi, Francesco, Bauri, Dibakar, Ristea, Catalin-lucian, Rode, Sudhir Pandurang, Rodriguez Cahuantzi, Mario, Roeed, Ketil, Rogalev, Roman, Rogochaya, Elena, Rohr, David Michael, Roehrich, Dieter, Fierro Rojas, Pablo, Rokita, Przemyslaw Stefan, Bazo Alba, Jose Luis, Ronchetti, Federico, Rosano, Antonina, Dominguez Rosas, Edgar, Roslon, Krystian, Rossi, Andrea, Rotondi, Alberto, Roy, Ankhi, Roy, Pradip Kumar, Vazquez Rueda, Omar, Rui, Rinaldo, Bearden, Ian Gardner, Rumyantsev, Boris, Rustamov, Anar, Ryabinkin, Evgeny, Ryabov, Yury, Rybicki, Andrzej, Rytkonen, Heidi Maria, Saarimaki, Oskari Antti Matti, Sadek, Rita, Sadhu, Samrangy, Sadovskiy, Sergey, Beattie, Caitlin, Safarik, Karel, Saha, Sumit Kumar, Sahoo, Baidyanath, Sahoo, Pragati, Sahoo, Raghunath, Sahoo, Sarita, Sahu, Pradip Kumar, Saini, Jogender, Sakai, Shingo, Sambyal, Sanjeev Singh, Ahammed, Zubayer, Bedda, Cristina, Samsonov, Vladimir, Sarkar, Debojit, Sarkar, Nachiketa, Sarma, Pranjal, Mantovani Sarti, Valentina, Sas, Mike Henry Petrus, Scapparone, Eugenio, Schambach, Johann Joachim, Scheid, Horst Sebastian, Schiaua, Claudiu Cornel, Behera, Nirbhay Kumar, Schicker, Rainer Martin, Schmah, Alexander, Schmidt, Christian Joachim, Schmidt, 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Mario, Skaali, Bernhard, Slupecki, Maciej, Smirnov, Nikolai, Snellings, Raimond, Soncco Meza, Carlos, Song, Jihye, Songmoolnak, Arnon, Soramel, Francesca, Bencedi, Gyula, Sorensen, Soren Pontoppidan, Sputowska, Iwona Anna, Stachel, Johanna, Stan, Ionel, Steffanic, Patrick John, Stenlund, Evert Anders, Stiefelmaier, Stephan Friedrich, Stocco, Diego, Storetvedt, Maksim Melnik, Dello Stritto, Luigi, Beole, Stefania, Alarcon Do Passo Suaide, Alexandre, Sugitate, Toru, Suire, Christophe Pierre, Suleymanov, Mais Kazim Oglu, Suljic, Miljenko, Sultanov, Rishat, Sumbera, Michal, Sumberia, Vikash, Sumowidagdo, Suharyo, Swain, Sagarika, Bercuci, Alexandru, Szabo, Alexander, Szarka, Imrich, Tabassam, Uzma, Taghavi, Seyed Farid, Taillepied, Guillaume, Takahashi, Jun, Tambave, Ganesh Jagannath, Tang, Siyu, Tarhini, Mohamad, Tarzila, Madalina-gabriela, Ahmad, Shakeel, Berdnikov, Yaroslav, Tauro, Arturo, Tejeda Munoz, Guillermo, Telesca, Adriana, Terlizzi, Livia, Terrevoli, Cristina, Thakur, Dhananjaya, Thakur, Sanchari, Thomas, Deepa, Thoresen, Freja, Tieulent, Raphael Noel, Berenyi, Daniel, Tikhonov, Anatoly, Timmins, Anthony Robert, Toia, Alberica, Topilskaya, Nataliya, Toppi, Marco, Torales Acosta, Fernando, Rojas Torres, Solangel, Trifiro, Antonio, Tripathy, Sushanta, Tripathy, Tulika, Bertens, Redmer Alexander, Trogolo, Stefano, Trombetta, Giuseppe, Tropp, Lukas, Trubnikov, Victor, Trzaska, Wladyslaw Henryk, Trzcinski, Tomasz Piotr, Trzeciak, Barbara Antonina, Tumkin, Alexandr, Turrisi, Rosario, Tveter, Trine Spedstad, Berzano, Dario, Ullaland, Kjetil, Umaka, Ejiro Naomi, Uras, Antonio, Usai, Gianluca, Vala, Martin, Valle, Nicolo', Vallero, Sara, Van Der Kolk, Naomi, Van Doremalen, Lennart, Van Leeuwen, Marco, Besoiu, Mihaela Gabriela, Vande Vyvre, Pierre, Varga, Dezso, Varga, Zoltan, Varga-kofarago, Monika, Diozcora Vargas Trevino, Aurora, Vasileiou, Maria, Vasiliev, Andrey, Vazquez Doce, Oton, Vechernin, Vladimir, Vercellin, Ermanno, Betev, Latchezar, Vergara 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N., Uras, A., Usai, G. L., Vala, M., Valle, N., Vallero, S., van der Kolk, N., van Doremalen, L. V. R., van Leeuwen, M., Vyvre, P. V., Varga, D., Varga, Z., Varga-Kofarago, M., Vargas, A., Vasileiou, M., Vasiliev, A., Doce, O. V., Vechernin, V., Vercellin, E., Limon, S. V., Vermunt, L., Vernet, R., Vertesi, R., Vickovic, L., Vilakazi, Z., Baillie, O. V., Vino, G., Vinogradov, A., Virgili, T., Vislavicius, V., Vodopyanov, A., Volkel, B., Volkl, M. A., Voloshin, K., Voloshin, S. A., Volpe, G., von Haller, B., Vorobyev, I., Voscek, D., Vrlakova, J., Wagner, B., Weber, M., Weber, S. G., Wegrzynek, A., Wenzel, S. C., Wessels, J. P., Wiechula, J., Wikne, J., Wilk, G., Wilkinson, J., Willems, G. A., Willsher, E., Windelband, B., Winn, M., Witt, W. E., Wright, J. R., Wu, Y., Xu, R., Yalcin, S., Yamaguchi, Y., Yamakawa, K., Yang, S., Yano, S., Yin, Z., Yokoyama, H., Yoo, I. -K., Yoon, J. H., Yuan, S., Yuncu, A., Yurchenko, V., Zaccolo, V., Zaman, A., Zampolli, C., Zanoli, H. J. C., Zardoshti, N., Zarochentsev, A., Zavada, P., Zaviyalov, N., Zbroszczyk, H., Zhalov, M., Zhang, S., Zhang, X., Zhang, Z., Zherebchevskii, V., Zhi, Y., Zhou, D., Zhou, Y., Zhou, Z., Zhu, J., Zhu, Y., Zichichi, A., Zinovjev, G., Zurlo, N., Laboratoire de physique subatomique et des technologies associées (SUBATECH), Université de Nantes - UFR des Sciences et des Techniques (UN UFR ST), Université de Nantes (UN)-Université de Nantes (UN)-Centre National de la Recherche Scientifique (CNRS)-Institut National de Physique Nucléaire et de Physique des Particules du CNRS (IN2P3)-IMT Atlantique Bretagne-Pays de la Loire (IMT Atlantique), Institut Mines-Télécom [Paris] (IMT)-Institut Mines-Télécom [Paris] (IMT), Laboratoire de Physique des 2 Infinis Irène Joliot-Curie (IJCLab), Institut National de Physique Nucléaire et de Physique des Particules du CNRS (IN2P3)-Université Paris-Saclay-Centre National de la Recherche Scientifique (CNRS), Département de Physique Nucléaire (ex SPhN) (DPHN), Institut de Recherches sur les lois Fondamentales de l'Univers (IRFU), Commissariat à l'énergie atomique et aux énergies alternatives (CEA)-Université Paris-Saclay-Commissariat à l'énergie atomique et aux énergies alternatives (CEA)-Université Paris-Saclay, Laboratoire de Physique de Clermont (LPC), Centre National de la Recherche Scientifique (CNRS)-Université Clermont Auvergne [2017-2020] (UCA [2017-2020])-Institut National de Physique Nucléaire et de Physique des Particules du CNRS (IN2P3), Institut Pluridisciplinaire Hubert Curien (IPHC), Institut National de Physique Nucléaire et de Physique des Particules du CNRS (IN2P3)-Université de Strasbourg (UNISTRA)-Centre National de la Recherche Scientifique (CNRS), Institut de Physique Nucléaire de Lyon (IPNL), Centre National de la Recherche Scientifique (CNRS)-Université Claude Bernard Lyon 1 (UCBL), Université de Lyon-Université de Lyon-Institut National de Physique Nucléaire et de Physique des Particules du CNRS (IN2P3), Laboratoire de Physique Subatomique et de Cosmologie (LPSC), Institut National de Physique Nucléaire et de Physique des Particules du CNRS (IN2P3)-Centre National de la Recherche Scientifique (CNRS)-Université Grenoble Alpes (UGA)-Institut polytechnique de Grenoble - Grenoble Institute of Technology (Grenoble INP ), Université Grenoble Alpes (UGA), Centre de Calcul de l'IN2P3 (CC-IN2P3), Institut National de Physique Nucléaire et de Physique des Particules du CNRS (IN2P3)-Centre National de la Recherche Scientifique (CNRS), ALICE, Université de Nantes (UN)-Université de Nantes (UN)-Institut National de Physique Nucléaire et de Physique des Particules du CNRS (IN2P3)-Centre National de la Recherche Scientifique (CNRS)-IMT Atlantique (IMT Atlantique), Institut National de Physique Nucléaire et de Physique des Particules du CNRS (IN2P3)-Université Clermont Auvergne [2017-2020] (UCA [2017-2020])-Centre National de la Recherche Scientifique (CNRS), Université de Strasbourg (UNISTRA)-Institut National de Physique Nucléaire et de Physique des Particules du CNRS (IN2P3)-Centre National de la Recherche Scientifique (CNRS), Université Claude Bernard Lyon 1 (UCBL), Université de Lyon-Université de Lyon-Institut National de Physique Nucléaire et de Physique des Particules du CNRS (IN2P3)-Centre National de la Recherche Scientifique (CNRS), S. 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Husova, N. Hussain, S. A. Hussain, D. Hutter, J. P. Iddon, R. Ilkaev, H. Ilyas, M. Inaba, G. M. Innocenti, M. Ippolitov, A. Isakov, M. S. Islam, M. Ivanov, V. Ivanov, V. Izucheev, B. Jacak, N. Jacazio, P. M. Jacobs, S. Jadlovska, J. Jadlovsky, S. Jaelani, C. Jahnke, M. J. Jakubowska, M. A. Janik, T. Janson, M. Jercic, O. Jevons, M. Jin, F. Jonas, P. G. Jones, J. Jung, M. Jung, A. Jusko, P. Kalinak, A. Kalweit, V. Kaplin, S. Kar, A. Karasu Uysal, D. Karatovic, O. Karavichev, T. Karavicheva, P. Karczmarczyk, E. Karpechev, A. Kazantsev, U. Kebschull, R. Keidel, M. Keil, B. Ketzer, Z. Khabanova, A. M. Khan, S. Khan, A. Khanzadeev, Y. Kharlov, A. Khatun, A. Khuntia, B. Kileng, B. Kim, B. Kim, D. Kim, D. J. Kim, E. J. Kim, H. Kim, J. Kim, J. S. Kim, J. Kim, J. Kim, J. Kim, M. Kim, S. Kim, T. Kim, T. Kim, S. Kirsch, I. Kisel, S. Kiselev, A. Kisiel, J. L. Klay, C. Klein, J. Klein, S. Klein, C. Klein-Bösing, M. Kleiner, A. Kluge, M. L. Knichel, A. G. Knospe, C. Kobdaj, M. K. Köhler, T. 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G. Ma, A. Maevskaya, M. Mager, S. M. Mahmood, T. Mahmoud, A. Maire, R. D. Majka, M. Malaev, Q. W. Malik, L. Malinina, D. Mal’Kevich, P. Malzacher, G. Mandaglio, V. Manko, F. Manso, V. Manzari, Y. Mao, M. Marchisone, J. Mareš, G. V. Margagliotti, A. Margotti, A. Marín, C. Markert, M. Marquard, C. D. Martin, N. A. Martin, P. Martinengo, J. L. Martinez, M. I. Martínez, G. Martínez García, S. Masciocchi, M. Masera, A. Masoni, L. Massacrier, E. Masson, A. Mastroserio, A. M. Mathis, O. Matonoha, P. F. T. Matuoka, A. Matyja, C. Mayer, F. Mazzaschi, M. Mazzilli, M. A. Mazzoni, A. F. Mechler, F. Meddi, Y. Melikyan, A. Menchaca-Rocha, C. Mengke, E. Meninno, A. S. Menon, M. Meres, S. Mhlanga, Y. Miake, L. Micheletti, L. C. Migliorin, D. L. Mihaylov, K. Mikhaylov, A. N. Mishra, D. Miśkowiec, A. Modak, N. Mohammadi, A. P. Mohanty, B. Mohanty, M. Mohisin Khan, Z. Moravcova, C. Mordasini, D. A. Moreira De Godoy, L. A. P. Moreno, I. Morozov, A. Morsch, T. Mrnjavac, V. Muccifora, E. Mudnic, D. Mühlheim, S. Muhuri, J. D. Mulligan, A. Mulliri, M. G. Munhoz, R. H. Munzer, H. Murakami, S. Murray, L. Musa, J. Musinsky, C. J. Myers, J. W. Myrcha, B. Naik, R. Nair, B. K. Nandi, R. Nania, E. Nappi, M. U. Naru, A. F. Nassirpour, C. Nattrass, R. Nayak, T. K. Nayak, S. Nazarenko, A. Neagu, R. A. Negrao De Oliveira, L. Nellen, S. V. Nesbo, G. Neskovic, D. Nesterov, L. T. Neumann, B. S. Nielsen, S. Nikolaev, S. Nikulin, V. Nikulin, F. Noferini, P. Nomokonov, J. Norman, N. Novitzky, P. Nowakowski, A. Nyanin, J. Nystrand, M. Ogino, A. Ohlson, J. Oleniacz, A. C. Oliveira Da Silva, M. H. Oliver, C. Oppedisano, A. Ortiz Velasquez, A. Oskarsson, J. Otwinowski, K. Oyama, Y. Pachmayer, V. Pacik, S. Padhan, D. Pagano, G. Paić, J. Pan, S. Panebianco, P. Pareek, J. Park, J. E. Parkkila, S. Parmar, S. P. Pathak, B. Paul, J. Pazzini, H. Pei, T. Peitzmann, X. Peng, L. G. Pereira, H. Pereira Da Costa, D. Peresunko, G. M. Perez, S. Perrin, Y. Pestov, V. Petráček, M. Petrovici, R. P. Pezzi, S. Piano, M. Pikna, P. Pillot, O. Pinazza, L. Pinsky, C. Pinto, S. Pisano, D. Pistone, M. Płoskoń, M. Planinic, F. Pliquett, M. G. Poghosyan, B. Polichtchouk, N. Poljak, A. Pop, S. Porteboeuf-Houssais, V. Pozdniakov, S. K. Prasad, R. Preghenella, F. Prino, C. A. Pruneau, I. Pshenichnov, M. Puccio, J. Putschke, S. Qiu, L. Quaglia, R. E. Quishpe, S. Ragoni, S. Raha, S. Rajput, J. Rak, A. Rakotozafindrabe, L. Ramello, F. Rami, S. A. R. Ramirez, R. Raniwala, S. Raniwala, S. S. Räsänen, R. Rath, V. Ratza, I. Ravasenga, K. F. Read, A. R. Redelbach, K. Redlich, A. Rehman, P. Reichelt, F. Reidt, X. Ren, R. Renfordt, Z. Rescakova, K. Reygers, A. Riabov, V. Riabov, T. Richert, M. Richter, P. Riedler, W. Riegler, F. Riggi, C. Ristea, S. P. Rode, M. Rodríguez Cahuantzi, K. Røed, R. Rogalev, E. Rogochaya, D. Rohr, D. Röhrich, P. F. Rojas, P. S. Rokita, F. Ronchetti, A. Rosano, E. D. Rosas, K. Roslon, A. Rossi, A. Rotondi, A. Roy, P. Roy, O. V. Rueda, R. Rui, B. Rumyantsev, A. Rustamov, E. Ryabinkin, Y. Ryabov, A. Rybicki, H. Rytkonen, O. A. M. Saarimaki, R. Sadek, S. Sadhu, S. Sadovsky, K. Šafařík, S. K. Saha, B. Sahoo, P. Sahoo, R. Sahoo, S. Sahoo, P. K. Sahu, J. Saini, S. Sakai, S. Sambyal, V. Samsonov, D. Sarkar, N. Sarkar, P. Sarma, V. M. Sarti, M. H. P. Sas, E. Scapparone, J. Schambach, H. S. Scheid, C. Schiaua, R. Schicker, A. Schmah, C. Schmidt, H. R. Schmidt, M. O. Schmidt, M. Schmidt, N. V. Schmidt, A. R. Schmier, J. Schukraft, Y. Schutz, K. Schwarz, K. Schweda, G. Scioli, E. Scomparin, J. E. Seger, Y. Sekiguchi, D. Sekihata, I. Selyuzhenkov, S. Senyukov, D. Serebryakov, A. Sevcenco, A. Shabanov, A. Shabetai, R. Shahoyan, W. Shaikh, A. Shangaraev, A. Sharma, A. Sharma, H. Sharma, M. Sharma, N. Sharma, S. Sharma, O. Sheibani, K. Shigaki, M. Shimomura, S. Shirinkin, Q. Shou, Y. Sibiriak, S. Siddhanta, T. Siemiarczuk, D. Silvermyr, G. Simatovic, G. Simonetti, B. Singh, R. Singh, R. Singh, R. Singh, V. K. Singh, V. Singhal, T. Sinha, B. Sitar, M. Sitta, T. B. Skaali, M. Slupecki, N. Smirnov, R. J. M. Snellings, C. Soncco, J. Song, A. Songmoolnak, F. Soramel, S. Sorensen, I. Sputowska, J. Stachel, I. Stan, P. J. Steffanic, E. Stenlund, S. F. Stiefelmaier, D. Stocco, M. M. Storetvedt, L. D. Stritto, A. A. P. Suaide, T. Sugitate, C. Suire, M. Suleymanov, M. Suljic, R. Sultanov, M. Šumbera, V. Sumberia, S. Sumowidagdo, S. Swain, A. Szabo, I. Szarka, U. Tabassam, S. F. Taghavi, G. Taillepied, J. Takahashi, G. J. Tambave, S. Tang, M. Tarhini, M. G. Tarzila, A. Tauro, G. Tejeda Muñoz, A. Telesca, L. Terlizzi, C. Terrevoli, D. Thakur, S. Thakur, D. Thomas, F. Thoresen, R. Tieulent, A. Tikhonov, A. R. Timmins, A. Toia, N. Topilskaya, M. Toppi, F. Torales-Acosta, S. R. Torres, A. Trifiró, S. Tripathy, T. Tripathy, S. Trogolo, G. Trombetta, L. Tropp, V. Trubnikov, W. H. Trzaska, T. P. Trzcinski, B. A. Trzeciak, A. Tumkin, R. Turrisi, T. S. Tveter, K. Ullaland, E. N. Umaka, A. Uras, G. L. Usai, M. Vala, N. Valle, S. Vallero, N. van der Kolk, L. V. R. van Doremalen, M. van Leeuwen, P. Vande Vyvre, D. Varga, Z. Varga, M. Varga-Kofarago, A. Vargas, M. Vasileiou, A. Vasiliev, O. Vázquez Doce, V. Vechernin, E. Vercellin, S. Vergara Limón, L. Vermunt, R. Vernet, R. Vértesi, L. Vickovic, Z. Vilakazi, O. Villalobos Baillie, G. Vino, A. Vinogradov, T. Virgili, V. Vislavicius, A. Vodopyanov, B. Volkel, M. A. Völkl, K. Voloshin, S. A. Voloshin, G. Volpe, B. von Haller, I. Vorobyev, D. Voscek, J. Vrláková, B. Wagner, M. Weber, S. G. Weber, A. Wegrzynek, S. C. Wenzel, J. P. Wessels, J. Wiechula, J. Wikne, G. Wilk, J. Wilkinson, G. A. Willems, E. Willsher, B. Windelband, M. Winn, W. E. Witt, J. R. Wright, Y. Wu, R. Xu, S. Yalcin, Y. Yamaguchi, K. Yamakawa, S. Yang, S. Yano, Z. Yin, H. Yokoyama, I.-K. Yoo, J. H. Yoon, S. Yuan, A. Yuncu, V. Yurchenko, V. Zaccolo, A. Zaman, C. Zampolli, H. J. C. Zanoli, N. Zardoshti, A. Zarochentsev, P. Závada, N. Zaviyalov, H. Zbroszczyk, M. Zhalov, S. Zhang, X. Zhang, Z. Zhang, V. Zherebchevskii, Y. Zhi, D. Zhou, Y. Zhou, Z. Zhou, J. Zhu, Y. Zhu, A. Zichichi, G. Zinovjev & N. Zurlo, Helsinki Institute of Physics, Sub Subatomic Physics (SAP), Afd Subatomic Physics (SAP), Sub Algemeen Physics Education, and Subatomic Physics

Subjects
EXCHANGE-POTENTIAL APPROACH, Strange quark, ALICE Collaboration, Hadron, Nuclear Theory, Strong interaction, hadron collisions, Position and momentum space, hiukkasfysiikka, nucl-ex, 7. Clean energy, 01 natural sciences, VDP::Fysikk: 430, High Energy Physics - Experiment, High Energy Physics - Experiment (hep-ex), Hadron-Hadron scattering (experiments), scattering [hadron], p p scattering, [PHYS.HEXP]Physics [physics]/High Energy Physics - Experiment [hep-ex], scattering [p p], Nuclear Experiment (nucl-ex), Experimental nuclear physics, NUCLEON, Nuclear Experiment, VDP::Physics: 430, Physics, Multidisciplinary, Large Hadron Collider, strong interaction, lattice [space-time], Publisher Correction, PRIRODNE ZNANOSTI. Fizika, BARYON-BARYON SCATTERING, CERN LHC Coll, LHC, ddc:500, Nucleon, Particle Physics - Experiment, discrete [space-time], Quark, Particle physics, CERN Lab, General Science & Technology, FOS: Physical sciences, short-range, Hadron, strong interaction, LHC, 114 Physical sciences, Fysikk: 430 [VDP], Article, hadron scattering, quark, ultrarelativistic proton–proton collisions, LHC, ALICE, 0103 physical sciences, Nuclear Physics - Experiment, General, 010306 general physics, Physics: 430 [VDP], interaction [hadron hadron], hep-ex, 010308 nuclear & particles physics, High Energy Physics::Phenomenology, effect [strong interaction], hadron-hadron interaction, strong interaction: effect, space-time: discrete, space-time: lattice, correlation, NATURAL SCIENCES. Physics, Baryon, Hypernuclei, Neutron Stars, Strangeness, Physics::Accelerator Physics, High Energy Physics::Experiment, hadron, Experimental particle physics
Abstract

One of the key challenges for nuclear physics today is to understand from first principles the effective interaction between hadrons with different quark content. First successes have been achieved using techniques that solve the dynamics of quarks and gluons on discrete space-time lattices1,2. Experimentally, the dynamics of the strong interaction have been studied by scattering hadrons off each other. Such scattering experiments are difficult or impossible for unstable hadrons3–6 and so high-quality measurements exist only for hadrons containing up and down quarks7. Here we demonstrate that measuring correlations in the momentum space between hadron pairs8–12 produced in ultrarelativistic proton–proton collisions at the CERN Large Hadron Collider (LHC) provides a precise method with which to obtain the missing information on the interaction dynamics between any pair of unstable hadrons. Specifically, we discuss the case of the interaction of baryons containing strange quarks (hyperons). We demonstrate how, using precision measurements of proton–omega baryon correlations, the effect of the strong interaction for this hadron–hadron pair can be studied with precision similar to, and compared with, predictions from lattice calculations13,14. The large number of hyperons identified in proton–proton collisions at the LHC, together with accurate modelling15 of the small (approximately one femtometre) inter-particle distance and exact predictions for the correlation functions, enables a detailed determination of the short-range part of the nucleon-hyperon interaction., Correlations in momentum space between hadrons created by ultrarelativistic proton–proton collisions at the CERN Large Hadron Collider provide insights into the strong interaction, particularly the short-range dynamics of hyperons—baryons that contain strange quarks.

Published
2020

40. Synthesis, in vitro antitumor evaluation and structure activity relationship of heptacoordinated amino-bis(Phenolato) Ti(IV) complexes stabilized by 2,6-dipicolinic acid.

Author

Li S, Zhang X, Zhao T, Liu N, Zhang Y, Wang P, Yang Z, and Huhn T

Subjects
Humans, Structure-Activity Relationship, HeLa Cells, Apoptosis drug effects, Molecular Structure, Cell Proliferation drug effects, Antineoplastic Agents pharmacology, Antineoplastic Agents chemistry, Antineoplastic Agents chemical synthesis, Picolinic Acids chemistry, Picolinic Acids pharmacology, Picolinic Acids chemical synthesis, Coordination Complexes chemistry, Coordination Complexes pharmacology, Coordination Complexes chemical synthesis, Titanium chemistry, Titanium pharmacology, Drug Screening Assays, Antitumor
Abstract

Eighteen novel Ti(IV) complexes stabilized by different chelating amino-bis(phenolato) (ONNO, ONON, ONOO) ligands and 2,6-dipicolinic acid as a second chelator were synthesized with isolated yields ranging from 79 to 93%. Complexes were characterized by 1 H and 13 C-NMR spectroscopy, as well as by HRMS and X-Ray diffraction analysis. The good to excellent aqueous stability of these Ti(IV) complexes can be modulated by the substitutions on the 2-position of the phenolato ligands. Most of the synthesized Ti(IV) complexes demonstrated potent inhibitory activity against Hela S3 and Hep G2 tumor cells. Among them, the naphthalenyl based Salan type 2j, 2-picolylamine based [ONON] type 2n and N-(2-hydroxyethyl) based [ONOO] type 2p demonstrated up to 40 folds enhanced cytotoxicity compared to cisplatin together with a significantly reduced activity against healthy AML12 cells. The three Ti(IV) complexes exhibited fast cellular uptake by Hela S3 cells and induced almost exclusively apoptosis. 2j could trigger higher level of ROS generation than 2p and 2n., (© 2024. The Author(s), under exclusive licence to Society for Biological Inorganic Chemistry (SBIC).)

Published
2024
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41. Nonuniform STM Contrast of Self-Assembled Tri- n -octyl-triazatriangulenium Tetrafluoroborate on HOPG.

Author

Snegir S, Dappe YJ, Sysoiev D, Huhn T, and Scheer E

Abstract

We have assembled 4,8,12-tri- n -octyl-4,8,12-triazatrianguleniumtetrafluoroborate (TATA-BF 4 ) on highly oriented pyrolytic graphite (HOPG) and have studied the structure and tunneling properties of this self-assembled monolayer (SAM) using scanning tunneling microscopy (STM) under ambient conditions. We show that the triazatriangulenium cations TATA + form hexagonally packed structures driven by the interaction between the aromatic core and the HOPG lattice, as evidenced by density functional theory (DFT) modeling. According to the DFT results, the three alkyl chains of the platform tend to follow the main crystallographic directions of HOPG, leading to a different STM appearance. The STM contrast of the SAM shows that the monolayer is formed by two types of species, namely, TATA + with BF 4 - counterions on top and without them. The cationic TATA + platform gives rise to a seemingly higher appearance than neutral TATA-BF 4 , in contrast to observations made on metallic substrates. The variation of the STM tunneling parameters does not change the relative difference of contrast, revealing the stability of both species on HOPG. DFT calculations show that TATA-BF 4 on HOPG has sufficient binding energy to resist dissociation into TATA + and BF 4 - , which might occur under the action of the electric field in the tunneling gap during STM scanning., Competing Interests: The authors declare no competing financial interest., (© 2023 The Authors. Published by American Chemical Society.)

Published
2023
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42. Synthesis and X-ray structure analysis of cytotoxic heptacoordinated Salan hafnium (IV) complexes stabilized with 2,6-dipicolinic acid.

Author

Zhao T, Wang P, Liu N, Zhao W, Yang M, Li S, Yang Z, Sun B, and Huhn T

Subjects
Humans, X-Rays, Picolinic Acids pharmacology, Picolinic Acids chemistry, Hafnium, Antineoplastic Agents chemistry
Abstract

Four novel Salan Hf (IV) complexes stabilized by 2,6-dipicolinic acid (Dipic) were synthesized and characterized by 1 H, 13 C NMR and X-ray diffraction spectroscopy. These Hf (IV) bis-chelates could be obtained in good to excellent yields (88%-91%) and demonstrated rather good stability in aqueous media and on silica gel. [L 2 Hf (IV) Dipic 4-H,Cl ] containing steric bulk L 2 were stable in about 10% H 2 O (H 2 O/THF (v/v)), however, [L 1 Hf (IV) Dipic 4-H,Cl ] with non-steric L 1 could slowly dissociate and release nontoxic L 1 . [L 1 - 2 Hf (IV) Dipic 4-Cl ] showed excellent anti-tumoral activity in the range of cisplatin (Hela S3: IC 50  = 3.5 ± 0.4 μM, Hep G2: IC 50  = 11.2 ± 2.1 μM). In addition, the cellular uptake and apoptosis investigation of [L 1 Hf (IV) Dipic 4-Cl ] suggested a fast cellular uptake process against Hela S3 cells with an almost exclusive induced apoptosis cell death path., Competing Interests: Declaration of Competing Interest The authors declare that they have no known competing financial interests or personal relationships that could have appeared to influence the work reported in this paper., (Copyright © 2022. Published by Elsevier Inc.)

Published
2023
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43. Anti-tumoral Titanium (IV) Complexes Stabilized with Phenolato Ligands and Structure-Activity Relationship.

Author

Zhao T, Wang P, Zhang X, Liu N, Zhao W, Zhang Y, Yuan P, Li S, Yang M, Yang Z, and Huhn T

Subjects
Humans, Titanium pharmacology, Titanium chemistry, Titanium therapeutic use, Ligands, Structure-Activity Relationship, Neoplasms drug therapy, Organometallic Compounds chemistry, Organometallic Compounds pharmacology, Organometallic Compounds therapeutic use, Antineoplastic Agents chemistry, Coordination Complexes pharmacology
Abstract

Titanocene dichloride and budotitane have opened a new chapter in medicinal chemistry of titanium (IV) complexes being novel non-platinum antitumor metallic agents. Numerous efforts have led to the discovery of the diamino bis -phenolato titanium (IV) complexes. Among which, the [ONNO] and [ONON] type ligands namely Salan, Salen and Salalen coordinated titanium (IV) alkoxyl complexes have demonstrated significantly enhanced aqueous stability, their in vitro and in vivo antitumor efficacy, mechanism of action, structure-activity relationships and combined tumor therapy have been intensively investigated. Replacement of the labile alkoxyls with a second chelator resulted in structural rigid titanium (IV) complexes, which showed exceedingly good aqueous stability and potent antitumor activity both in vitro and in vivo . The unique ligand system successfully allowed the access of isotopic [ 45 Ti]Titanium (IV) complexes, post-synthetic modification, facile synthetic protocols and antitumor congeneric zirconium (IV) and hafnium (IV) complexes. This review presents recent research progress in the field of antitumor group 4 metal complexes stabilized with phenolato ligands; especially their structure-activity relationships are summarized., (Copyright© Bentham Science Publishers; For any queries, please email at epub@benthamscience.net.)

Published
2023
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44. Bowl-Shaped Symmetric and Non-symmetric Bis-functionalized Indacenopicenes.

Author

Bayer J and Huhn T

Subjects
Halogens, Polymers chemistry, Alkynes chemistry, Azides chemistry
Abstract

Regioselective arrangement of two groups of orthogonal reactivity in bowl-shaped as -indaceno[3,2,1,8,7,6- pqrstuv ]picene (Idpc) was key for the synthesis of hetero-bis-functionalized Idpc derivatives. Halogen and methyl groups were positioned at specific positions in the rim area of Idpc at an early stage during the synthesis by functionalization of suitable precursors. Regioselective functionalization of the bowl's rim was then finally achieved either via consecutive Cu(I)-catalyzed azide-alkyne coupling (CuAAC) and C-C cross-coupling reactions or by C-C cross-coupling alone, giving access to either symmetric or non-symmetric bis-functionalized Idpc derivatives. The self-aggregation behavior of 9c in solution was investigated by recording a series of concentration-dependent NMR spectra. The aggregation constant of 9c was determined by a nonlinear least-squares treatment of the 1 H NMR shift data to be 2.9 ± 0.2 M -1 , and the formation of dimers was found to be the prevailing process.

Published
2022
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45. Describing chain-like assembly of ethoxygroup-functionalized organic molecules on Au(111) using high-throughput simulations.

Author

Lokamani, Kelling J, Ohmann R, Meyer J, Kühne T, Cuniberti G, Wolf J, Juckeland G, Huhn T, Zahn P, Moresco F, and Gemming S

Abstract

Due to the low corrugation of the Au(111) surface, 1,4-bis(phenylethynyl)-2,5-bis(ethoxy)benzene (PEEB) molecules can form quasi interlocked lateral patterns, which are observed in scanning tunneling microscopy experiments at low temperatures. We demonstrate a multi-dimensional clustering approach to quantify the anisotropic pair-wise interaction of molecules and explain these patterns. We perform high-throughput calculations to evaluate an energy function, which incorporates the adsorption energy of single PEEB molecules on the metal surface and the intermolecular interaction energy of a pair of PEEB molecules. The analysis of the energy function reveals, that, depending on coverage density, specific types of pattern are preferred which can potentially be exploited to form one-dimensional molecular wires on Au(111)., (© 2021. The Author(s).)

Published
2021
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46. Efficient and Consumer-Centered Item Detection and Classification with a Multicamera Network at High Ranges.

Author

Mandischer N, Huhn T, Hüsing M, and Corves B

Subjects
Humans, Algorithms, Machine Learning
Abstract

In the EU project SHAREWORK, methods are developed that allow humans and robots to collaborate in an industrial environment. One of the major contributions is a framework for task planning coupled with automated item detection and localization. In this work, we present the methods used for detecting and classifying items on the shop floor. Important in the context of SHAREWORK is the user-friendliness of the methodology. Thus, we renounce heavy-learning-based methods in favor of unsupervised segmentation coupled with lenient machine learning methods for classification. Our algorithm is a combination of established methods adjusted for fast and reliable item detection at high ranges of up to eight meters. In this work, we present the full pipeline from calibration, over segmentation to item classification in the industrial context. The pipeline is validated on a shop floor of 40 sqm and with up to nine different items and assemblies, reaching a mean accuracy of 84% at 0.85 Hz.

Published
2021
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47. Geodesic-Planar Conjugates: Substituted Buckybowls-Synthesis, Photoluminescence and Electrochemistry.

Author

Bayer J, Herberger J, Holz L, Winter RF, and Huhn T

Abstract

C-C cross coupling products of bowl-shaped as-indaceno[3,2,1,8,7,6-pqrstuv]picene (Idpc) and different planar arenes and ethynyl-arenes were synthesized. Photoluminescence as well as electrochemical properties of all products were investigated and complemented by time-dependent quantum chemical calculations. UV/Vis spectroelectrochemistry investigations of the directly linked (Idpc) 2 indicated the absence of any intramolecular charge-transfer transition of intermittently formed (Idpc) 2 .- . All coupling products showed fluorescence. Ferrocene-1-yl-Idpc was structurally characterized by X-ray diffraction and is a rare example of a ferrocene-containing buckybowl exhibiting luminescence., (© 2020 The Authors. Published by Wiley-VCH GmbH.)

Published
2020
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48. Basic enemies of photochromism: irreversible transformation of fluorinated diarylethenes to polyenic enamines and enols.

Author

Sysoiev D and Huhn T

Abstract

Non-photochemical degradation of perfluorinated photochromic diarylethenes (DAE) under Knoevenagel, Sonogashira or Wittig conditions was discovered. This base promoted formation of strongly colored non-photochromic byproducts has an impact in the field of molecular electronics due to the basic conditions often employed during deacylation and desilylation of the protected thiol anchoring groups of functionalized DAE. The products were identified as seven-membered ring systems of the bicyclo[5.3.0]deca-1,7-diene type. Their formation was rationalized by a tentative two-step reaction mechanism.

Published
2020
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49. Desulfatiglans anilini Initiates Degradation of Aniline With the Production of Phenylphosphoamidate and 4-Aminobenzoate as Intermediates Through Synthases and Carboxylases From Different Gene Clusters.

Author

Xie X, Spiteller D, Huhn T, Schink B, and Müller N

Abstract

The anaerobic degradation of aniline was studied in the sulfate-reducing bacterium Desulfatiglans anilini . Our aim was to identify the genes and their proteins that are required for the initial activation of aniline as well as to characterize intermediates of this reaction. Aniline-induced genes were revealed by comparison of the proteomes of D. anilini grown with different substrates (aniline, 4-aminobenzoate, phenol, and benzoate). Most genes encoding proteins that were highly abundant in aniline- or 4-aminobenzoate-grown D. anilini cells but not in phenol- or benzoate-grown cells were located in the putative gene clusters ani (aniline degradation), hcr (4-hydroxybenzoyl-CoA reductase) and phe (phenol degradation). Of these putative gene clusters, only the phe gene cluster has been studied previously. Based on the differential proteome analysis, four candidate genes coding for kinase subunits and carboxylase subunits were suspected to be responsible for the initial conversion of aniline to 4-aminobenzoate. These genes were cloned and overproduced in E. coli . The recombinant proteins were obtained in inclusion bodies but could be refolded successfully. Two subunits of phenylphosphoamidate synthase and two carboxylase subunits converted aniline to 4-aminobenzoate with phenylphosphoamidate as intermediate under consumption of ATP. Only when both carboxylase subunits, one from gene cluster ani and the other from gene cluster phe , were combined, phenylphosphoamidate was converted to 4-aminobenzoate in vitro, with Mn 2+ , K + , and FMN as co-factors. Thus, aniline is degraded by the anaerobic bacterium D. anilini only by recruiting genes for the enzymatic machinery from different gene clusters. We conclude, that D. anilini carboxylates aniline to 4-aminobenzoate via phenylphosphoamidate as an energy rich intermediate analogous to the degradation of phenol to 4-hydroxybenzoate via phenylphosphate., (Copyright © 2020 Xie, Spiteller, Huhn, Schink and Müller.)

Published
2020
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50. Surface Plasmon-Enhanced Switching Kinetics of Molecular Photochromic Films on Gold Nanohole Arrays.

Author

Lenyk B, Schöps V, Boneberg J, Kabdulov M, Huhn T, Scheer E, Offenhäusser A, and Mayer D

Abstract

Diarylethene molecules are discussed as possible optical switches, which can reversibly transition between completely conjugated (closed) and nonconjugated (open) forms with different electrical conductance and optical absorbance, by exposure to UV and visible light. However, in general the opening reaction exhibits much lower quantum yield than the closing process, hindering their usage in optoelectronic devices. To enhance the opening process, which is supported by visible light, we employ the plasmonic field enhancement of gold films perforated with nanoholes. We show that gold nanohole arrays reveal strong optical transmission in the visible range (∼60%) and pronounced enhancement of field intensities, resulting in around 50% faster switching kinetics of the molecular species in comparison with quartz substrates. The experimental UV-vis measurements are verified with finite-difference time-domain simulation that confirm the obtained results. Thus, we propose gold nanohole arrays as transparent and conductive plasmonic material that accelerates visible-light-triggered chemical reactions including molecular switching.

Published
2020
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