Different industries make use of encapsulated particles, from the pharmaceutical industry for target drug delivery to the agricultural industry for masking of odor and flavor of feedstock food. Current techniques that are used for producing encapsulated particles are costly, time consuming or energy inefficient, so new techniques are researched. This study focusses on one of these novel techniques, electrospray encapsulation, and compares this technique to the more conventional cooling crystallization to encapsulate particles. Focus of this comparison lays on the encapsulation properties, the particle morphology, the process limitations and controllability. Using different experimental set-ups, multiple experiments have been conducted with the model compounds isonicotinamide and caffeine., Intensified Reaction & Separation Technology, Process and Energy, Mechanical, Maritime and Materials Engineering