Search

Welding or brazing of metals to ceramics often leads to failures under aggressive conditions due to abrupt changes in physical, chemical, and thermal properties at the metal-ceramic interface. Metal-ceramic Functional Graded Materials (FGMs) replace the strict interface with a gradual transition of composition and properties, which protects the material from failures. The powder-blown Laser-Directed Energy Deposition (DED-LB) is one of the widely known Additive Manufacturing (AM) processes that offer unique features like developing FGMs and multi-material structures. Various studies have been conducted to process metalceramic FGMs using the DED-LB process but significant differences in thermal properties, varying laser-material interactions, and the possibility of formation of complex reaction products make the processing of metal-ceramic FGMs challenging. This study aims to understand the effect of laser power on a ceramic substrate, and its interaction with a metal powder introduced in the melt pool. A single track of nickel-based superalloy Alloy 718 powder was deposited on an Alumina substrate with different laser powers. The deposition was performed with and without substrate pre-heat to understand the effect of pre-treatment on deposition. Metallographic analysis was performed to reveal the microstructure of the resolidified metal mixed ceramic region, CC BY NC 4.0

Collaboration between those working in product development and production is essential for successful product realization. The Swedish Production Academy (SPA) was founded in 2006 with the aim of driving and developing production research and higher education in Sweden, and increasing national cooperation in research and education within the area of production. This book presents the proceedings of SPS2024, the 11th Swedish Production Symposium, held from 23 to 26 April 2024 in Trollhättan, Sweden. The conference provided a platform for SPA members, as well as for professionals from industry and academia interested in production research and education from around the world, to share insights and ideas. The title and overarching theme of SPS2024 was Sustainable Production through Advanced Manufacturing, Intelligent Automation and Work Integrated Learning, and the conference emphasized stakeholder value, the societal role of industry, worker wellbeing, and environmental sustainability, in alignment with the European Commission's vision for the future of manufacturing. The 59 papers included here were accepted for publication and presentation at the symposium after a thorough review process. They are divided into 6 sections reflecting the thematic areas of the conference, which were: sustainable manufacturing, smart production and automation, digitalization for efficient product realization, circular production, industrial transformation for sustainability, and the integration of education and research. Highlighting the latest developments and advances in automation and sustainable production, the book will be of interest to all those working in the field., CC BY NC

Forging on an industrial scale often involves slow, size-limited cooling rates or high temperature hold times between, or after, deformation. This enables the dynamic recrystallization (DRX) initiated during forging to further progress under static conditions, a phenomenon called meta-dynamic recrystallization (mDRX). As mDRX will influence the final grain size, and thus properties, it is critical to understand and control it during processing. Here, we study the mDRX evolution in Ni-based superalloy Haynes 282 during post-deformation hold times of up to 120 s at 1080 °C after partial DRX. We find that mDRX is the dominating mechanisms responsible for the microstructure evolution the hold time. The very rapid mDRX kinetics in the initial stages suggest that quench delays (the time between the end of the deformation and the onset of the quenching intended to arrest the microstructure evolution) must be kept well below 1 s in order to allow reliable conclusions to be drawn from post-deformation microstructure investigations. A larger prior strain (larger DRX fraction) leads to faster mDRX kinetics and a larger final grain size. Larger strains leads to earlier impingement of the growing grains, which, in combination with smaller remaining deformed regions into which the grains can grow, limits the maximum size of the mDRX grains. We also note a close correlation between static recovery and stress relaxation during the hold time, whereas no such correlation between mDRX and stress relaxation can be observed., CC BY 4.0

The equiaxed Ni-based superalloy René 108 was subjected to short-term annealing at five temperatures between 900 °C and 1100 °C. The phase composition, phase lattice parameters, microstructure, stereological parameters, and chemical composition of γ′ precipitates were investigated by thermodynamic simulations, X-ray diffraction, scanning and transmission electron microscopy, and energy-dispersive X-ray spectroscopy. Analysis of the γ and γ′ lattice parameters using the Nelson-Riley extrapolation function showed that the misfit parameter for temperatures 900 °C to 1050 °C is positive (decreasing from 0.32 to 0.11 pct). At 1100 °C, the parameter becomes negative, δ = − 0.18 pct. During the short-term annealing, γ′ precipitates dissolution occurred progressing more rapidly with increasing temperatures. The surface fraction of γ′ precipitates decreased with increasing temperature from 0.52 to 0.34. The dissolution of γ′ precipitates did not only proceed through uninterrupted thinning of each individual precipitate, but also included more complex mechanisms, including splitting. Based on transmission electron microscopy, it was shown that after γ′ precipitates dissolution, the matrix close to the γ/γ′ interface is strongly enriched in Co and Cr and depleted in Al.

Haynes 282 is a Ni-based gamma prime (gamma’) strengthening alloy with a balanced combination of high temperature properties and fabricability. This paper aims to study the evolution of the microstructure and hardness using a novel physical simulation method called arc heat treatment, followed by thermodynamic modeling of gamma’ precipitation. For the arc heat treatment, a steady state temperature gradient was generated using a stationary tungsten inert gas arc on a sample mounted onto a water-cooled chamber. The steady state condition ranged from room temperature to the liquidus and was achieved within the first few sec-onds. Aged and solutionized samples were arc heat treated for 1.5 min, 30 min, and 4 h. The experiments were complemented with temperature modeling, equilibrium calculations, and gamma’ precipitation simulations. A unique graded microstructure formed in the arc heat-treated samples. It consisted of a fusion zone with a dendritic microstructure; a region with the dissolution of all secondary phases (MC carbides, grain boundary carbides, and gamma’); a region with MC and grain boundary carbides; a gamma’ precipitation zone; and the base metal. The temperature range of the dissolution area extended to lower temperatures with increasing arc heat treatment dwell time. The gamma’ precipitation zone showed a distinct etching response coupled with high hardness. The hardness and the temperature range of the gamma’ precipitation zone increased with increasing arc heat treatment time. The gamma’ radii increased with increasing time and temperature. The gamma’ precipitation model, simulated with TC Prisma, showed very good agreement with the experimental results. Finally, the results were used to develop time-temperature precipitation and hardness diagrams. (c) 2021 The Authors. Published by Elsevier B.V. CC_BY_4.0

homogenisation heat treatments. The hot ductility deteriorated significantly after long-dwell homogenisation heat treatments for 24 h at temperatures of 1120 and 1190 °C as compared with those treated at a short dwell time of 4 h at the same temperatures. The observed ductility deterioration was related to more extensive liquation along the grain boundaries caused by different mechanisms, e.g., liquation by solute segregation mechanism, Laves melting, constitutional liquation of MC carbides and supersolidus grain boundary melting, with the effect and extent depending on the solute changes after the homogenisation heat treatments. Furthermore, the role of Nb as the solute element and as the precipitate former, as well as the effect of minor alloying elements segregating along the grain boundaries, is discussed in connection to grain boundary liquation, which contributes to a better understanding of heat-affected zone liquation cracking susceptibility of cast ATI® 718Plus®. © 2020 The Authors

The effect of grain size on the suceptibility towards strain age cracking (SAC) has been investigated for Haynes® 282® in the tempeature range of 750 to 950°C after isothermal exposure up to 1800s. Grain growth was induced by heattreating the material at 1150°C for 2h, resulting in a fourfold increase in grain size. Hardness was significanlty reduced after heat treatment as compared to millannealed material. Large grain size resulted in intergranular fracture over a widertemperature range than small grain size material. Ductility was lowest at 850°C, while lower values were observed to be correlated to increased grain size. The rapid formation of grain boundary carbide networks in Haynes® 282® is found to be notable to compensate for higher local stresses on grain boundaries due to incresedgrain size.

The influence of base metal conditions on the weld cracking behaviour of cast ATI 718Plus® is investigated by comparing 4 h and 24 h dwell time pseudo-hip homogenisation heat treatments at 1120, 1160 and 1190 °C with the as-cast microstructure. Scanning electron microscopy (SEM), X-ray diffraction (XRD) on electrolytically extracted powder and transmission electron microscopy (TEM) were used to identify Nb-rich secondary phases in interdendritic areas as the C14 Laves phase and Nb(Ti) MC-type carbides. All homogenisation heat treatments but the 1120 °C 4-h condition dissolve the Laves phase. A repair welding operation was simulated by linear groove multi-pass manual gas tungsten arc welding (GTAW). The Laves phase containing microstructures resulted in lower total crack length for heat affected zone cracking. Constitutional liquation of Nb(Ti) MC-type carbides is observed as a liquation mechanism in Laves-free microstructure, while thick liquid film formation due to the Laves eutectic melting could reduce the formation of weld cracks in microstructures containing the Laves phase.

A Gleeble-based test method has been developed to study the change in the ductility signature of Haynes (R) 282 (R) during isothermal exposure from 5 s to 1800 s. A temperature range of 750 to 950 degrees C has been used to investigate the effect of age-hardening reactions. Microstructural constituents have been analyzed and quantified using scanning and transmission electron microscopy. Carbides present in the material are identified as primary MC-type TiC carbides, Mo-rich M6C secondary carbides, and Cr-rich M23C6 secondary carbides. Gamma prime (gamma’) precipitates are present in all the material conditions with particle sizes ranging from 2.5 nm to 58 nm. Isothermal exposure causes the growth of gamma’ and development of a grain boundary carbide network. A ductility minimum is observed at 800-850 degrees C. The fracture mode is found to be dependent on the stroke rate, where a transition toward intergranular fracture is observed for stroke rates below 0.055 mm/s. Intergranular fracture is characterized by microvoids present on grain facets, while ductility did not change during ongoing age-hardening reactions for intergranularly fractured Haynes (R) 282 (R)., Funding: Consortium Material Technology for Thermal Energy Processes (KME)

This paper presents a method to acquire thermal data in the base metal heat affected zone (HAZ) during manual multi-pass TIG welding of ATI ® 718Plus TM , representing conditions close to an actual repair welding operation. Thermocouples were mounted in different locations along side walls of linear grooves to record temperature data. The thermal cycling was found to be largely independent of location within the HAZ. The recorded temperatures were below the incipient laves melting temperature, indicating that the current test setup requires optimisation to study HAZ liquation. Based on the results of this study, a modified thermocouple mounting technique is proposed. © 2018 Elsevier B.V. All rights reserved.

The ability of the precipitation hardening superalloy Haynes® 282® to be repaired by multi-pass gas tungsten arc welding is investigated in this study. The repair welding has been carried out on forged discs having four pre weld heat treatments, resulting in different grain sizes and precipitate structures of the base material. Another set of discs has additionally been put through a post weld heat treatment. The tendency to form cracks in the heat-affected zone and the fusion zone has been investigated metallographically. No cracks in the base metal heat-affected zone were found,whereas solidification cracks were present in the weld fusion zone of all tested conditions. While high heat input during welding increased cracking by a factor of 1.5, none of the heat treatments had a measurable influence on the cracking behaviour. Voids with solid state crack-like appearance turned out tobe aluminium-rich oxides being present from the deposition of previous weld deposit layers., First Online: 19 August 2017Funders: GKN

This paper reviews the literature with emphasis on strain age cracking, a cracking phenomenon that can occur during welding or heat treatment of precipitation hardening superalloys. The influence of chemical composition in terms of e.g. hardening elements and impurities, microstructure of base material and weld zone, precipitation-induced stress development, welding heat input, restraint and post weld heat treatment (PWHT) conditions is discussed and related to the cracking susceptibility of different nickel based superalloys. Furthermore, an overview on available testing methods is presented and scrutinized. As of now, neither a standardized nor universally applicable procedure is available where the now existing tests generally can be divided into two groups; procedures representing actual welds usually providing qualitative comparisons under specified conditions, and simulative tests like those based on the Gleeble® system which can provide fundamental insight into the ongoing mechanisms.