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4. Collection of NMR Scalar and Residual Dipolar Couplings Using a Single Experiment.

Author

Gil ‐ Silva, Leandro F., Santamaría ‐ Fernández, Raquel, Navarro ‐ Vázquez, Armando, and Gil, Roberto R.

Subjects
*NUCLEAR magnetic resonance, *MAGNETIC coupling, *ZWITTERIONS, *METHACRYLATES, *ISOTROPIC properties, *MENTHOL
Abstract

A new DMSO-compatible aligning gel based on cross-linked poly(2-hydroxylethyl methacrylate) (poly-HEMA) has been developed. Due to a significant difference in bulk magnetic susceptibility between the DMSO inside and outside the gel, it is possible to simultaneously collect isotropic and anisotropic NMR data, such as residual dipolar couplings (RDC), in the same NMR tube. RDC-assisted structural analysis of menthol and the alkaloid retrorsine is reported as proof of concept. [ABSTRACT FROM AUTHOR]

Published
2016
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