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Research and Control Laboratory, Bharat Aluminium Co. Ltd., Korba-495 684 Chemistry Department, Government Tilak College, Katni-483 501 Manuscript received 12 August 1984, revised 8 March1985, accepted 3 June1985 The X-ray diffraction data or fifteen N-hydroxy-N-aryl-arylamides are described here, out of which 14 are reported for the first time. An attempt has been made to establishtheir diffraction patterns.