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Aluminium matrix composites have been developed to replace other conventional engineering materials in specific industries where enhanced properties are required. The corrosion susceptibility of sintered unreinforced aluminium and composites in chloride medium (AMCs) were studied. The powders of pure as-received aluminium (matrix) and particles of ferrotitanium and silicon carbide particles were homogeneously dispersed using ball milling technique. Powder metallurgy route was utilised for consolidating the milled powders into a sintered compact. Microstructural examination of the compacted pure aluminium and composites confirmed an even distribution of the reinforcements in the aluminium matrix. The produced composites also recorded an improved corrosion resistance in a corrosive medium of 3.5 wt.% laboratory prepared sodium chloride, from the potentiodynamic polarization and chronoamperometry (potentiostatic) tests. The corroded specimens were further assessed for pitting using a field emission scanning electron microscope (FE-SEM). The resistance of the fabricated samples to corrosion was improved upon the addition of TiFe and SiC reinforcements.

The densification process and grain analysis of consolidated NiAl-CNT composites at 1000 °C, and at varied heating rates from 50 °C/min to 150 °C/min was investigated. The results revealed the effect of heating rate on the densification behaviour of the samples. The displacement of the composites decreased from 3.39 mm to 2.63 mm with increasing heating rate, while the porosity increased by 69% at rapid heating rate. The grain analysis of the sintered samples through the electron backscattered (EBSD) technique indicates the evolution of bigger grains as the heating rate proceeds higher. Furthermore, the mean grain size of the consolidated composites increased from 3.93 μm, to 8.05 μm due to the concentration of defects. Interestingly, there was no texture or predominance of any color evolution in the sintered materials.

The nanohardness, elastic modulus, anti-wear, and deformability characteristics of TiAl(100−x)-xTaN composites containing 0, 2, 4, 6, 8, and 10 wt.% of TaN were investigated via nanoindentation technique in the present study. The TiAl(100−x)-xTaN composites were successfully fabricated via the spark plasma sintering technique (SPS). The microstructure and phase formation of the TiAl sample constitute a duplex structure of γ and lamellar colonies, and TiAl2, α-Ti, and TiAl phases, respectively. The addition of TaN results in a complex phase formation and pseudo duplex structure. The depth-sensing indentation evaluation of properties was carried out at an ambient temperature through a Berkovich indenter at a prescribed load of 100 mN and a holding time of 10 s. The nanoindentation result showed that the nanohardness and elastic modulus characteristics increased as the TaN addition increased but exhibited a slight drop when the reinforcement was beyond 8 wt.%. At increasing TaN addition, the yield strain ( H E r ), yield pressure ( H 3 E r 2 ), and elastic recovery index ( W e W t ) increased, while the plasticity index ( W p W t ) and the ratio of plastic and elastic work (RPE) reduced. The best mechanical properties were attained at the 8 wt.%TaN addition. [ABSTRACT FROM AUTHOR]