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Nanoparticles are one of the effective methodologies implemented in concrete technology. The main objective of this research is to study the influence of nano alumina with different percentage variations ranging from 1% to 3% along with the incorporation of PVA fibers. From the mechanical properties test, the optimum dosage was determined to further study the durability behavior. This research work also investigates the hybridization of two nanoparticles such as nano silica (NS) and nano alumina (NA). The results show that the increasing quantity of NA reduces the compressive strength of the mortar due to agglomeration (cluster of particles), which results in a greater molecular attraction force. From the test results, it is concluded that the optimum dosage has been attained with an addition of 2% NA with 0.3% PVA. The compression strength test results at 14 days and 28 days reveal that the addition of NA tends the mineral admixture to react at early ages in the hydration process, which produces a new chemical compound to fill the pores. The rapid chloride penetration (RCPT) test results at 28 days significantly improved with the incorporation of nanoparticles due to their effective size and chemical reaction towards the other compounds. The test results from the hybridization of nanoparticles showed that the compressive strength was significantly enhanced compared to that of the control mortar and mortar with NA. They are effective up to certain limits beyond that addition, and the workability was reduced. Amongst all mixtures, the maximum compression strength has been attained for the mix with the addition of NA 0.5% and NS 2.5% comparatively. The microstructural properties of mortar were also studied through scanning electron microscope (SEM) analysis. The results showed that the incorporation of nanoparticles in the mortar matrix turns homogeneous with fewer pores and greater amount of hydration compounds; thereby, pore refinement has improved the hydration compounds remarkably. [ABSTRACT FROM AUTHOR]