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The current need to move towards more sustainable technologies in the construction sector has promoted the investigation of using alternative materials in asphalt mixtures for pavements. Biomaterials, used as biobinders, have shown their potential as partial replacement of bitumen in asphalt mixtures as solution to decreasing the demand for fossil-fuel-based binders as well as CO2 emissions. However, more research is needed to increase the replacement of bitumen in asphalt mixtures. In this investigation,biobinders are used as full replacement of virgin bitumen and as recycling agent within asphalt mixtures with high Reclaimed Asphalt (RA) content. Blends of biobinders and RA binders, and bio-recycled asphalt mixtures, were produced, subjected to ageing and rheologically characterised. The results show that the rheological properties of binders’ blends seem adequate for their use, while the bio-recycled asphalt mixtures seem to have a faster ageing than conventional ones, hence their full-scale application still remains a concern.

Part of this research was funded by the project RTI2018-096224-J-I00 that has been cofounded by the Spanish Ministry of Science and Innovation, inside the National Program for Fostering Excellence in Scientific and Technical Research, National Subprogram of Knowledge Generation, 2018 call, in the framework of the Spanish National Plan for Scientific and Technical Research and Innovation 2017-2020, and by the European Union, through the European Regional Development Fund, with the main objective of Promoting technological development, innovation and quality research. Part of this work was financially supported by the Italian Ministry of University and Research with the research Grant PRIN 2017 USR342 Urban Safety, Sustainability and Resilience., This paper describes the development of novel/state-of-art computational framework to accurately predict the degree of binder activity of a reclaimed asphalt pavement sample as a percentage of the indirect tensile strength (ITS) using a reduced number of input variables that are relatively easy to obtain, namely compaction temperature, air voids and ITS. Different machine learning (ML) techniques were applied to obtain the most accurate data representation model. Specifically, three ML techniques were applied: 6th-degree multivariate polynomial regression with regularization, artificial neural network and random forest regression. The three techniques produced models with very similar precision, reporting a mean absolute error ranging from 12.2 to 12.8% of maximum ITS on the test data set. The work presented in this paper is an evolution in terms of data analysis of the results obtained within the interlaboratory tests conducted by Task Group 5 of the RILEM Technical Committee 264 on Reclaimed Asphalt Pavement. Hence, despite it has strong bonds with this framework, this work was developed independently and can be considered as a natural follow-up, Spanish Government RTI2018-096224-J-I00, European Commission, Ministry of Education, Universities and Research (MIUR) PRIN 2017 USR342

The recent drive to find ways to increase sustainability and decrease costs in asphalt paving has led researchers to find innovative ways to incorporate more recycled materials and bio-derived binders into mixes with varying success. A new novel bio-derived binder made from refined pine chemistry stabilised with a polymer can increase the sustainability of asphalt mixes while maintaining pavement performance. Laboratory performance testing was conducted on asphalt mixes containing 50% Reclaimed Asphalt Pavement (RAP) by mix weight and the novel bio-derived binder. Results show that the bio-derived binder outperforms the conventional 50/70 pen grade binder mixes with respect to resistance to thermal cracking and adequately passes all requirements for pavements with 20-year design loadings of less than 30 million ESALs. This research shows that asphalt mixes containing 50% RAP and a bio-derived binder can be designed to pass performance criteria at low, intermediate, and high temperatures without the need of neat bitumen.

Due to emerging climate challenges, engineers are looking to replace the conventional asphalt pavements by utilizing bio-materials combined with Reclaimed Asphalt (RA). However, there is insufficient record in the literature assessing their environmental performance. This study addresses the analysis of the results obtained from a life cycle assessment exercise of asphalt pavements containing bio-materials and RA within their binder courses, developed within the BioRePavation project. The aim is to analyze the environmental benefits achieved, by means of hotspot mapping and sensitivity analysis of the most impactful factors of their lifecycles. Two alternatives are compared to a conventional asphalt pavement and recommendations on how to improve the current practices are provided. Results rank the raw material acquisition and replacement as the most impactful stages, while through sensitivity analysis, linear relationships between the impact category indicator values and the RA% used, are detected.

The pavement engineering industry, having realized the significance of the impacts that it imposes on the environment through the production, construction and management of its products and assets, has been driven towards a more sustainable and circular way of operating. This has partly been through asphalt recycling, which is an area that many road authorities have prioritized. However, not all the National Road Authorities (NRAs) and/or sector stakeholders seem to be adequately familiar with the Circular Economy (CE) concept. This paper attempts to assist the transition of NRAs to a more circular way of doing business, by analyzing the current situation of CE within national/regional authorities and NRAs. To do so, a questionnaire was sent to di erent NRAs and an online search was conducted to identify the ways that NRAs communicate their CE practices. Findings indicate that, although the majority of the NRAs are familiar with CE as a concept, not many actions have been taken so far towards its holistic implementation. Finally, there is a significant lack of CE expertise and communication within these bodies., European Union's Horizon 2020 Program under the Marie Curie-Sklodowska actions for research, technological development, and demonstration 721493, CEDR Transnational Research Programme

As part of an effort by agencies and industry to move towards performance-based design to evaluate mixtures in the laboratory at a smaller scale before moving to full scale operation, laboratory protocols exist to simulate the aging that occurs as a material is produced. However, recent research has shown that these existing protocols may not accurately represent the changes a material experiences in a plant. Moreover, due to the focus of previous studies on the ability of the current method to replicate mixture characteristics and performance in an undamaged state, there is a lack of information as it relates to the damaged state. This paper presents a concise description of a study undertaken on a particular mixture to evaluate the differences in the behaviour of a standard asphalt concrete mixture produced in the laboratory and in the plant to assess the anticipated field performance at the mixture design stage. The results, in terms of the rheological properties of binders extracted and recovered from laboratory and plant produced mixtures as well as rheological, repeated cyclic fatigue, and cracking performance evaluation of the asphalt mixtures, have shown the ability of a short-term oven aging protocol to replicate plant produced material in the laboratory.

Polymer Modified Bitumens (PMBs) are largely used for pavement and roofing membranes applications with Styrene-Butadiene-Styrene Block copolymer (SBS) playing a major role in both markets despite its constantly increasing price due to the rising demand for quality bitumen modifiers. On the other hand, there is an increasing trend of recycling end of life tyres generating Recycled Tyre Rubber (RTR) at affordable price. This investigation aims at engineering a modified bitumen with a combination of Liquid Rubber (LR), a homogeneous blend of 50–70% RTR pre-processed in combination with heavy oils, and a wax denominated Ethylene Bis Stearamide (EBS). In the first phase, the effect of LR and EBS was independently characterised and compared to PMBs. Next, the Response Surface Methodology (RSM) was used to predict the response of different combinations of LR and EBS in terms of low and high temperature properties and cost, to then be optimised targeting conventional and rheological properties of PMBs currently used in asphalt mixtures and roofing membranes in UK. As a result, an optimum combination of LR and EBS was found leading to a cost-effective modified bitumen comparable to PMBs. The work provided also analytical functions that could be of use in further design exercises.

In this paper, a new and simple approach to estimate the rheological properties of Reclaimed Asphalt Pavement (RAP) binder is proposed to overcome the limitations of the conventional extraction procedure. This method is based on Dynamic Shear Rheometer tests performed on mortars composed of RAP fine fraction and virgin binder, together with a new back-calculation solution. The properties of the bituminous blends of virgin and RAP binders are obtained with a modified Nielsen model. The Voigt model is then successfully used to estimate complex modulus and phase angle of the RAP binder from the properties of the back-calculated binder blend. This procedure would prevent the need of RAP binder extractions to determine its properties, which is time-consuming and might modify the actual binder characteristics.

The massive exploitation of non-renewable natural resources which has taken place in the last decade has led to significant global environmental concerns. In such a context, the use of non-petroleum-based binders for the construction of bound layers of flexible pavements can represent an effective solution to limit crude oil depletion. The research work presented in this paper focused on the effects of ageing on the rheological and chemical characteristics of a non-bituminous binder, indicated in the study as a “biobinder”, and a traditional neat bitumen selected as a reference material. Binders were analyzed in four ageing conditions obtained by making use of the Rolling Thin Film Oven and of the Pressure Ageing Vessel. Rheological behaviour of binders was investigated by means of oscillatory tests carried out in a wide range of temperatures and frequencies with a dynamic shear rheometer. Chemical structure was explored via Thin Layer Chromatographic analyses and Fourier Transform Infrared Spectroscopy. The experimental work demonstrated that mechanisms of ageing which are involved in biobinders completely differ from those experienced by petroleum-based binders. Concerns were expressed with respect to the applicability to non-conventional binders of currently available ageing techniques and of chemical characterization methods.

The aged properties of Reclaimed Asphalt (RA) binders are one of the main factors working against their utilisation in high-RA content (&gt, 30%) mixes for surface courses. Fatigue cracking is the main distress of surface courses that are manufactured with a high percentage of RA. This investigation presents results of the rheological and fatigue results of different asphalt mixtures and their recovered binders. The binders were recovered from asphalt mixtures that had been manufactured in asphalt plants using different amounts of RA with contents up to 60% with and without rejuvenators. Two different sources of RA were used, representing a moderately aged RA and an extremely aged RA. The Dynamic Shear Rheometer (DSR) was used to assess the fatigue-characteristics of the binders using time sweep tests while the fatigue characteristics of their mixtures were assessed using the Indirect Tensile Fatigue Test (ITFT). The fatigue data was analysed based on the cumulative dissipated energy approach in addition to traditional fatigue analysis. Results have shown that the ageing condition of RA significantly affects the fatigue properties of recovered binders. Binder and asphalt mixture fatigue results showed that RA contents up to 60% can produce comparable fatigue performance compared to lower percentages of RA in road surface course if the aged RA binder is sufficiently rejuvenated.

The construction and maintenance of road pavements need to be undertaken to ensure proper economic and social growth. Considering the high environmental impact that the production of asphalt mixtures for road pavements entails, in terms of energy consumption and greenhouse gas (GHG) emissions, these operations must follow the global transition towards more sustainable development practices. In response to this, previous research has been focused on the development of manufacturing low temperature asphalt mixtures and the use of recycled modifiers such as tire crumb rubber to improve their durability. However, the use of high dosages of the latter reduces mixture workability, thus requiring high manufacturing temperatures to reduce the viscosity of the binder, and therefore limiting the advancement towards more sustainable mixtures. In this regard, further knowledge is needed on this topic to promote the combination of such techniques to maximise their advantages. This study aims to check the viability of producing asphalt mixtures with high crumb rubber contents at reduced temperatures, testing their workability, stiffness, cohesion, resistance to permanent deformations and resistance to moisture damage. Results show that it is possible to manufacture viable, warm, rubberised asphalt mixtures at 150 °C using a high penetration bitumen and reduce this temperature to 130 °C (45 °C less than conventional rubberised asphalt mixtures) by including warm additives, without compromising their mechanical performance.

An experimental study was conducted to evaluate the effectiveness of two bio-additives as rejuvenators on the properties of asphalt mixtures containing 50% RAP and their binder constituents containing 37% RAP binder. Before mixing, the rejuvenators were blended with fresh bitumen and the extracted and recovered RAP bitumen, and changes in the rheological properties of the binders were assessed using performance grading (PG) criteria. The results showed that both rejuvenators could improve the low-temperature performance of the aged RAP binder and restore its low-temperature properties. Master curves for the unaged, RTFO-aged, and PAV aged blends were constructed using both the Christensen-Anderson-Marasteanu (CAM) model and the Sigmoidal models. A comparative statistical analysis conducted on the models indicated no significant difference between the measured and predicted complex modulus values at any aging conditions. The pairwise statistical comparison between the two models showed that at unaged conditions, they can perfectly overlap as the p-values were greater than the level of significance. However, for the PAV-aged binders, this behaviour appears to weaken due to the brittle behaviour of the binders. Further statistical analyses revealed no significant differences between the two models at unaged conditions, however, as the binders where subjected to aging, significant differences between the two models began to appear. Mixing was performed in two locations: lab and plant, while compaction was performed only in the lab. After mixing and compaction, mixtures were evaluated for their stiffness characteristics through dynamic modulus testing. Compared to the control mixture, rejuvenated mixtures showed lower dynamic modulus values specially at high temperatures. A statistical comparison between the lab-produced, lab-compacted mixtures and plant-produced, lab compacted mixtures showed that both the rejuvenation and the location of mixing were significant factors in the stiffness measurements.

Alternative binders not derived from fossil fuels, known as biobinders, are opening new paths for multiple applications in road infrastructure. Biobinders, usually produced from bio-oils obtained from the processing of biomass and industry by-products, are tuneable materials whose properties can be adjusted to meet specific targets. For this reason, an interesting approach is to couple biobinders with Reclaimed Asphalt (RA) by taking advantage of their rejuvenating properties to design bio-asphalt mixtures with high-content RA and no additional virgin bitumen. Recent research has proven the feasibility of this approach through validation at full-scale (BioRePavation project). However certain aspects related to the durability of bio-asphalt mixtures still require further research, one of these being their resistance to moisture damage. This study aims at filling some of these current gaps by conducting an initial investigation of the moisture sensitivity of selected biobinders and bio-rejuvenated asphalt binders. In order to do this, the intrinsic adhesion and cohesion properties of an extracted RA binder, two biobinders, their blends and two types of aggregates were characterised by means of Surface Free Energy (SFE), individually and as a system. The binders/blends-aggregate systems were further tested by means of the Pneumatic Adhesion Tensile Test Instrument (PATTI) to determine their pull-off tensile strength (POTS). The results show that the bio-rejuvenated asphalt binders present equivalent cohesive and adhesive properties to a conventional bitumen and superior performance when compared to the RA binder. Hence, the combination of biobinders and RA has great potential to guarantee resistance to moisture damage of bio-recycled asphalt mixtures with high-content RA and no additional bitumen.

Three innovative environmentally friendly pavement materials, designed with 50% of Reclaimed Asphalt and three different biomaterials (2 bio-additivated bitumens and 1 bio-binder), were produced in an industrial plant. These mixes were tested in lab and also at full scale using an Accelerated Pavement Test facility. The asphalt mix viscoelastic properties were measured in lab and their intrinsic viscoelastic response were simulated. These rheological models are used to simulate the pavement mechanical response using both elastic and viscoelastic multilayer codes. Hence, full scale measurement performed during the full scale test at an early stage (without damages) can be compared with these simulations. The overall prediction accuracy, when all the signals are considered, is between 4% and 8% for all materials. It can be concluded that material characterisation in lab as well as the selected models are well adapted to simulate actual loading state under a moving load, even for these non-conventional mixes. For temperatures lower than 25°C, elastic modelling appears to be sufficient for pavement structural design with the innovative materials tested here.

This paper presents the results from a laboratory investigation on the effects of aging on the properties of two binders recovered from two different sources of Reclaimed Asphalt (RA) and additivated with a biorejuvenator derived from pine trees. It has been already proven that the rejuvenators are able to restore some of the properties of the aged binder present in the RA, but nowadays their effects into the long-term period are not well known. In this regard, the rejuvenated asphalt binders and a virgin binder, defined as a target, have been aged artificially to simulate short-and long-term aging. All binders have been studied conducting physical, chemical, rheological, and performance-related tests at three different aging levels. Results show that physical and rheological properties can be fully restored by the addition of the proper dose of rejuvenator, while the chemical composition should be investigated in more detail. Rejuvenated binders exhibit great long-term performance especially at high and low temperatures, but also show significant resistance against fatigue at intermediate temperatures.

El interés en la utilización de bio-materiales en ingeniería de pavimentos ha crecido significantemente en las últimas décadas debido a la conciencia ambiental sobre el uso de recursos naturales no renovables. En este artículo, se utilizan bio-materiales para recuperar las propiedades iniciales del betún envejecido presente en mezclas con alto contenido de asfalto reciclado (RA). Para ello, se ha estudiado y comparado el comportamiento de dos bio-materiales con betunes convencionales y betunes modificados con polímeros. Con este objetivo, se fabricaron mezclas de bio-materiales y betún reciclado simulando mezclas asfálticas con 50% de contenido de reciclado. El efecto rejuvenecedor de los bio-materiales se ha evaluado y comparado con el efecto rejuvenecedor de ligantes convencionales mediante el cálculo de las distribuciones de peso molecular aparente y diferentes parámetro reológicos. Los resultados muestran el poder rejuvenecedor de los bio-materiales, poniendo de manifiesto su potencial para usarse como ligantes vírgenes en mezclas asfálticas con alto contenido de reciclado.

Fatigue cracking is one of the most important failure mechanisms occurring in asphalt pavements, especially when mixtures incorporate considerable amount of rReclaimed asphalt pavement (RAP). In fact, aged binders contained in RAP generally make asphalt more brittle and specifically reduce fatigue resistance of the resulting asphalt mixtures. Binders and mortars play a key role in this phenomenon, considering fatigue cracking usually starts within these asphalt components. However, performance-related tests and specifications commonly regard binders and there are no sound methodologies allowing the use of mortars to predicting fatigue performance of asphalts containing RAP. For this reason, in this paper, fatigue resistance of extracted binders from high-RAP content mixtures and of RAP mortars (passing sieve with an opening size of 0.15 mm) were assessed and compared. Binders were extracted from asphalt mixtures manufactured with 30%, 60% RAP and rejuvenators. Mixtures recipes were then reproduced to manufacture mortars accordingly. Time sweep tests in stress-controlled mode were carried out on both materials (binders and mortars) and the resulting fatigue laws were compared. As a result, a strict correlation was obtained, leading to affirm fatigue-related properties of RAP mixture could be assessed by directly testing RAP mortars. This makes the recovery of RAP binders unnecessary. Moreover, a relationship between the two fatigue laws versus the percentage of fine particles in the mortar was found. This latter relationship allows determining the fatigue law of mortars corresponding to any percentage of fine particles and therefore corresponding to any percentage of RAP.

Reclaimed Asphalt (RA) has shown great potential to be reused in new asphalt mixtures, however its incorporation in top asphalt pavement layers is still very limited (10e30%). In fact, despite the advan- tages that its use implies, RA content in road pavement surface courses is still restricted in most countries due to mainly legislation limitations, but also some technical issues. This paper aims at being a step further to improve the latter by providing a methodology that allows producing fundamental inputs for confidently performing mix design of asphalt mixtures incorporating up to 100% RA. The methodology consists in an advanced preliminary binder's blend design that can be used with any type of RA and also in presence of rejuvenators. This procedure includes in the production of blending charts and laws that considers the uncertainties on accounting the extent of final binder content, Degree of Blending and Replaced Virgin Binder. The description of the methodology is accompanied with results of two extreme case studies consisting in the preliminary design of binders for asphalt mixtures with high content of two types of RA corresponding to extreme cases: the short-term aged RA (STA-RA), having a very soft residual binder (Pen > 20 dmm) and the long-term aged RA, having a much harder residual binder (Pen < 10 dmm). As a result, the proposed methodology allowed assessing the feasibility of using up to 90% of RA and determining whether the use of rejuvenating agents was needed.

Resumen.-La mayoría de las investigaciones sobre el diseño de firmes de mezclas bituminosas se basan en ensayos de laboratorio que determinan las propiedades mecánicas de las mismas intentando reproducir las condiciones de fabricación de la mezcla en planta, su puesta en obra y las acciones que sufrirá durante su vida de servicio. Son muchas las variables que intervienen en el diseño de una mezcla bituminosa: tipo de árido, tamaño, tipo de ligante, contenido de huecos, etc., por lo que la realización de ensayos de laboratorio que abarquen todas ellas supone un consumo de material y tiempo muy elevados. Además, los materiales que componen las mezclas, áridos (provenientes de cantera) y betún (subproducto del petróleo), son recursos agotables que conllevan el deterioro del medio ambiente y un alto gasto económico. La posibilidad de predecir propiedades fundamentales de las mezclas bituminosas mediante modelos micro-mecánicos es esencial para suplir o reducir la necesidad de realizar ensayos de laboratorio. Asimismo, la simulación de las mezclas mediante estos modelos proporciona un mejor conocimiento del funcionamiento de la estructura interna de la mezcla. El Trabajo Fin de Máster que se presenta ensaya teóricamente el Método de los Elementos Discretos para modelizar el comportamiento mecánico de mezclas bituminosas y relacionar las propiedades del modelo con las variables que intervienen en el diseño de mezclas. En particular, esta investigación se centra en el tamaño de árido, la naturaleza del mismo y el tiempo de aplicación de la carga. Con este propósito, se ha generado un modelo 3D en el que se reproducen las propiedades volumétricas de las mezclas y se simula un ensayo de compresión uniaxial. Mediante la variación de las propiedades del modelo se obtienen resultados que se correlacionan con los datos de laboratorio. Dentro del rango de estudio del presente trabajo, se ha encontrado que el aumento del tamaño de árido no influye significativamente en las propiedades de las mezclas, pero sí en la rigidez de los contactos del modelo. Por el contrario, la naturaleza del árido y el tiempo de aplicación de la carga afectan tanto al comportamiento de la mezcla en laboratorio como a la rigidez de los contactos del modelo., Universidad de Granada. Departamento de Mecánica de Estructuras e Ingeniería Hidráulica. Máster Universitario en Estructuras, curso 2012-2013

The interest in using bio-materials in pavement engineering has grown significantly over the last decades due to environmental concerns about the use of non-recoverable natural resources. In this paper, bio-materials are used together with Reclaimed Asphalt (RA) to restore some of the properties of the aged bitumen present in mixtures with high RA content. For this purpose, two bio-materials are studied and compared to conventional and polymer modified bitumens. Blends of these materials with RA bitumen were produced and studied to simulate a 50% RA mixture. The rejuvenating effect of the two bio-materials on RA has been assessed and compared with the effect of the conventional binders. Apparent Molecular Weight Distribution of the samples (obtained by the ?-method) and different rheological parameters were used for this purpose. Results revealed the power of bio-materials to rejuvenate RA bitumen, showing their capability to be used as fresh binders in high-RA content mixtures., El interés en la utilización de bio-materiales en ingeniería de pavimentos ha crecido significantemente en las últimas décadas debido a la conciencia ambiental sobre el uso de recursos naturales no renovables. En este artículo, se utilizan bio-materiales para recuperar las propiedades iniciales del betún envejecido presente en mezclas con alto contenido de asfalto reciclado (RA). Para ello, se ha estudiado y comparado el comportamiento de dos bio-materiales con betunes convencionales y betunes modificados con polímeros. Con este objetivo, se fabricaron mezclas de bio-materiales y betún reciclado simulando mezclas asfálticas con 50% de contenido de reciclado. El efecto rejuvenecedor de los bio-materiales se ha evaluado y comparado con el efecto rejuvenecedor de ligantes convencionales mediante el cálculo de las distribuciones de peso molecular aparente y diferentes parámetro reológicos. Los resultados muestran el poder rejuvenecedor de los bio-materiales, poniendo de manifiesto su potencial para usarse como ligantes vírgenes en mezclas asfálticas con alto contenido de reciclado.