301. A comparison of dilatometry and in-situ neutron diffraction in tracking bulk phase transformations in a martensitic stainless steel
- Author
-
Mark T. F. Telling, K. S. Knight, Frédéric Christien, Institut des Matériaux Jean Rouxel (IMN), Université de Nantes - UFR des Sciences et des Techniques (UN UFR ST), Université de Nantes (UN)-Université de Nantes (UN)-Centre National de la Recherche Scientifique (CNRS)-Institut de Chimie du CNRS (INC)-Ecole Polytechnique de l'Université de Nantes (EPUN), Université de Nantes (UN)-Université de Nantes (UN), ISIS Facility, STFC Rutherford Appleton Laboratory (RAL), Science and Technology Facilities Council (STFC)-Science and Technology Facilities Council (STFC), Department of Materials, University of Oxford [Oxford], Department of Earth Sciences [NHM London] (DES-NHM), and The Natural History Museum [London] (NHM)
- Subjects
010302 applied physics ,Austenite ,Materials science ,Rietveld refinement ,Mechanical Engineering ,Neutron diffraction ,Metallurgy ,Thermodynamics ,02 engineering and technology ,Martensitic stainless steel ,engineering.material ,Atmospheric temperature range ,021001 nanoscience & nanotechnology ,Condensed Matter Physics ,01 natural sciences ,Thermal expansion ,Mechanics of Materials ,Diffusionless transformation ,Martensite ,0103 physical sciences ,engineering ,[PHYS.COND.CM-MS]Physics [physics]/Condensed Matter [cond-mat]/Materials Science [cond-mat.mtrl-sci] ,Dilatometry High temperature neutron diffraction Phase transformation Steel Austenite Martensite ,General Materials Science ,0210 nano-technology - Abstract
International audience; Phase transformations in the 17-4PH martensitic stainless steel have been studied using different in-situ techniques, including dilatometry and high resolution neutron diffraction. Neutron diffraction patterns were quantitatively processed using the Rietveld refinement method, allowing the determination of the temperature-dependence of martensite (α′, bcc) and austenite (γ, fcc) phase fractions and lattice parameters on heating to 1000 °C and then cooling to room temperature. It is demonstrated in this work that dilatometry doesn't permit an accurate determination of the end temperature (Ac3) of the α′ → γ transformation which occurs upon heating to high temperature. The analysis of neutron diffraction data has shown that the respective volumes of the two phases become very close to each other at high temperature, thus making the dilatometric technique almost insensitive in that temperature range. However, there is a very good agreement between neutron diffraction and dilatometry at lower temperature. The martensitic transformation occurring upon cooling has been analysed using the Koistinen-Marburger equation. The thermal expansion coefficients of the two phases have been determined in addition. A comparison of the results obtained in this work with data from literature is presented.
- Published
- 2013