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We present our current progress on the design and test of Ti/TiN Multilayer for use in Kinetic Inductance Detectors (KIDs). Sensors based on sub-stoichiometric TiN film are commonly used in several applications. However, it is difficult to control the targeted critical temperature $T_C$, to maintain precise control of the nitrogen incorporation process and to obtain a production uniformity. To avoid these problems we investigated multilayer Ti/TiN films that show a high uniformity coupled with high quality factor, kinetic inductance and inertness of TiN. These features are ideal to realize superconductive microresonator detectors for astronomical instruments application but also for the field of neutrino physics. Using pure Ti and stoichiometric TiN, we developed and tested different multilayer configuration, in term of number of Ti/TiN layers and in term of different interlayer thicknesses. The target was to reach a critical temperature $T_C$ around $(1\div 1.5)$ K in order to have a low energy gap and slower recombination time (i.e. low generation-recombination noise). The results prove that the superconductive transition can be tuned in the $(0.5\div 4.6)$ K temperature range properly choosing the Ti thickness in the $(0\div 15)$ nm range, and the TiN thickness in the $(5\div 100)$ nm range

The external shell of the CUORE cryostat is a large cryogen-free system designed to host the dilution refrigerator and the bolometers of the CUORE experiment in a low radioactivity environment. The three vessels that form the outer shell were produced and delivered to the Gran Sasso underground Laboratories in July 2012. In this paper, we describe the production techniques and the validation tests done at the production site in 2012., Comment: 11 pages, 13 figures; to appear in NIMA

In calorimetric neutrino mass experiments, where the shape of a beta decay spectrum has to be precisely measured, the understanding of the detector response function is a fundamental issue. In the MIBETA neutrino mass experiment, the X-ray lines measured with external sources did not have Gaussian shapes, but exhibited a pronounced shoulder towards lower energies. If this shoulder were a general feature of the detector response function, it would distort the beta decay spectrum and thus mimic a non-zero neutrino mass. An investigation was performed to understand the origin of the shoulder and its potential influence on the beta spectrum. First, the peaks were fitted with an analytic function in order to determine quantitatively the amount of events contributing to the shoulder, also depending on the energy of the calibration X-rays. In a second step, Montecarlo simulations were performed to reproduce the experimental spectrum and to understand the origin of its shape. We conclude that at least part of the observed shoulder can be attributed to a surface effect.

In this article we describe the background challenges for the CUORE experiment posed by surface contamination of inert detector materials such as copper, and present three techniques explored to mitigate these backgrounds. Using data from a dedicated test apparatus constructed to validate and compare these techniques we demonstrate that copper surface contamination levels better than 10E-07 - 10E-08 Bq/cm2 are achieved for 238U and 232Th. If these levels are reproduced in the final CUORE apparatus the projected 90% C.L. upper limit on the number of background counts in the region of interest is 0.02-0.03 counts/keV/kg/y depending on the adopted mitigation technique., Comment: 10 pages, 6 figures, 6 tables

We report the results of a search for axions from the 14.4 keV M1 transition from Fe-57 in the core of the sun using the axio-electric effect in TeO2 bolometers. The detectors are 5x5x5 cm3 crystals operated at about 10 mK in a facility used to test bolometers for the CUORE experiment at the Laboratori Nazionali del Gran Sasso in Italy. An analysis of 43.65 kg d of data was made using a newly developed low energy trigger which was optimized to reduce the detectors energy threshold. An upper limit of 0.63 c kg-1 d-1 was established at 95% C.L.. From this value, a lower bound at 95% C.L. was placed on the Peccei-Quinn energy scale of fa >= 0.76 10**6 GeV for a value of S=0.55 for the flavor-singlet axial vector matrix element. Bounds are given for the interval 0.15 < S < 0.55., Comment: 14 pages, 6 figures, submitted to JCAP

We collected 19.4 days of data from four 750 g TeO2 bolometers, and in three of them we were able to set the energy threshold around 3 keV using a new analysis technique. We found a background rate ranging from 25 cpd/keV/kg at 3 keV to 2 cpd/keV/kg at 25 keV, and a peak at 4.7 keV. The origin of this peak is presently unknown, but its presence is confirmed by a reanalysis of 62.7 kg.days of data from the finished CUORICINO experiment. Finally, we report the expected sensitivities of the CUORE0 (52 bolometers) and CUORE (988 bolometers) experiments to a WIMP annual modulation signal., Comment: 9 pages, 10 figures

We have investigated the possibility of measuring the electron neutrino mass with sub-eV sensitivity by studying the electron capture decay of 163-Ho with cryogenic microcalorimeters. In this paper we will introduce an experiment's concept, discuss the technical requirements, and identify a roadmap to reach a sensitivity of 0.1 eV and beyond., Comment: 9 pages, 6 figures

$^{209}$Bi alpha decay to the ground and to the first excited state have been contemporary observed for the first time with a large BGO scintillating bolometer. The half-life of $^{209}$Bi is determined to be $\tau_{1/2}$=(2.01$\pm$0.08)$\cdot10^{19}$ years while the branching ratio for the ground-state to ground-state transition is (98.8$\pm$0.3)%., Comment: 5 pages, 4 figures

We present a study of the sensitivity and discovery potential of CUORE, a bolometric double-beta decay experiment under construction at the Laboratori Nazionali del Gran Sasso in Italy. Two approaches to the computation of experimental sensitivity for various background scenarios are presented, and an extension of the sensitivity formulation to the discovery potential case is also discussed. Assuming a background rate of 10^-2 cts/(keV kg y), we find that, after 5 years of live time, CUORE has a 1 sigma sensitivity to the neutrinoless double-beta decay half-life of T_1/2(1 sigma) = 1.6 \times 10^26 y and thus a potential to probe the effective Majorana neutrino mass down to 40-100 meV; the sensitivity at 1.64 sigma, which corresponds to 90% C.L., will be T_1/2(1.64 sigma) = 9.5 \times 10^25 y. This range is compared with the claim of observation of neutrinoless double-beta decay in 76Ge and the preferred range of the neutrino mass parameter space from oscillation results., Comment: 14 pages, 6 figures, revision for new submission to Astroparticle Physics

The CUORE Crystal Validation Runs (CCVRs) have been carried out since the end of 2008 at the Gran Sasso National Laboratories, in order to test the performances and the radiopurity of the TeO$_2$ crystals produced at SICCAS (Shanghai Institute of Ceramics, Chinese Academy of Sciences) for the CUORE experiment. In this work the results of the first 5 validation runs are presented. Results have been obtained for bulk contaminations and surface contaminations from several nuclides. An extrapolation to the CUORE background has been performed., Comment: 11 pages, 8 figures

The CUORICINO experiment was an array of 62 TeO$_{2}$ single-crystal bolometers with a total $^{130}$Te mass of $11.3\,$kg. The experiment finished in 2008 after more than 3 years of active operating time. Searches for both $0\nu$ and $2\nu$ double-beta decay to the first excited $0^{+}$ state in $^{130}$Xe were performed by studying different coincidence scenarios. The analysis was based on data representing a total exposure of N($^{130}$Te)$\cdot$t=$9.5\times10^{25}\,$y. No evidence for a signal was found. The resulting lower limits on the half lives are $T^{2\nu}_{1/2}(^{130} Te\rightarrow^{130} Xe^{*})>1.3\times10^{23}\,$y (90% C.L.), and $T^{0\nu}_{1/2}(^{130} Te\rightarrow^{130} Xe^{*})>9.4\times10^{23}\,$y (90% C.L.)., Comment: 6 pages, 4 figures

We report the final result of the CUORICINO experiment. Operated between 2003 and 2008, with a total exposure of 19.75 kg y of 130Te, CUORICINO was able to set a lower bound on the 130Te 0nDBD half-life of 2.8 10^{24} years at 90% C.L. The limit here reported includes the effects of systematic uncertainties that are examined in detail in the paper. The corresponding upper bound on the neutrino Majorana mass is in the range 300--710 meV, depending on the adopted nuclear matrix element evaluation., Comment: 12 pages, 10 figures

The international project ``Microcalorimeter Arrays for a Rhenium Experiment'' (MARE) aims at the direct and calorimetric measurement of the electron neutrino mass with sub-electronvolt sensitivity. Calorimetric neutrino mass experiments measure all the energy released in a beta decay except for the energy carried away by the neutrino, therefore removing the most severe systematic uncertainties which have plagued the traditional and, so far, more sensitive spectrometers. Calorimetric measurements are best realized exploiting the thermal detection technique. This approach uses thermal microcalorimeters whose absorbers contain a low transition energy Q beta decaying isotope. To date the two best options are 187Re and 163Ho. While the first beta decays, the latter decays via electron capture, but both have a Q value around 2.5 keV. The potential of using 187Re for a calorimetric neutrino mass experiment has been already demonstrated. On the contrary, no calorimetric spectrum of 163Ho has been so far measured with the precision required to set a useful limit on the neutrino mass. In this talk we present the status and the perspectives of the MARE project activities for the active isotope selection and the single channel development. We also discuss the neutrino mass statistical sensitivity achievable with both isotopes., Comment: Plenary Talk presented at the XXIV International Conference on Neutrino Physics and Astrophysics (Neutrino 2010), Athens, Greece, June 14-19, 2010

We present a search for beta plus/EC double beta decay of 120Te performed with the CUORICINO experiment, an array of TeO2 cryogenic bolometers. After collecting 0.0573 kg y of 120Te, we see no evidence of a signal and therefore set the following limits on the half-life: T1/2 (0nu) > 1.9 10^{21} y at 90% C.L. for the 0 neutrino mode and T1/2 (2nu) > 7.6 10^{19} y at 90% C.L. for the two neutrino mode. These results improve the existing limits by almost three orders of magnitude (four in the case of 0 neutrino mode)., Comment: 6 pages, 10 figures, version accepted for publication by Astroparticle Physics

High purity TeO2 crystals are produced to be used for the search for the neutrinoless double beta decay of 130Te. Dedicated production lines for raw material synthesis, crystal growth and surface processing were built compliant with radio-purity constraints specific to rare event physics experiments. High sensitivity measurements of radio-isotope concentrations in raw materials, reactants, consumables, ancillaries and intermediary products used for TeO2 crystals production are reported. Production and certification protocols are presented and resulting ready-to-use TeO2 crystals are described., Comment: 11 pages, 5 figures, 3 tables

A large calorimetric neutrino mass experiment using thermal detectors is expected to play a crucial role in the challenge for directly assessing the neutrino mass. We discuss and compare here two approaches to the estimation of the experimental sensitivity of such an experiment. The first method uses an analytic formulation and allows to readily obtain a sensible estimate over a wide range of experimental configurations. The second method is based on a frequentist Montecarlo technique and is more precise and reliable. The Montecarlo approach is then exploited to study the main sources of systematic uncertainties peculiar to calorimetric experiments. Finally, the tools are applied to investigate the optimal experimental configuration for a calorimetric experiment with Rhenium based thermal detectors., Comment: 25 pagers, 16 figures

To better understand the contribution of cosmic ray muons to the CUORICINO background, 10 plastic scintillator detectors were installed at the CUORICINO site and operated during the final 3 months of the experiment. From these measurements, an upper limit of 0.0021 counts/(keV kg yr) (95% CL) was obtained on the cosmic ray-induced background in the neutrinoless double beta decay region of interest. The measurements were also compared to Geant4 simulations., Comment: 16 pages, 7 figures

The CUORE experiment will search for neutrinoless double beta decay (0nDBD) of 130Te using an array of 988 TeO_2 bolometers operated at 10 mK in the Laboratori Nazionali del Gran Sasso (Italy). The detector is housed in a large cryogen-free cryostat cooled by pulse tubes and a high-power dilution refrigerator. The TeO_2 bolometers measure the event energies, and a precise and reliable energy calibration is critical for the successful identification of candidate 0nDBD and background events. The detector calibration system under development is based on the insertion of 12 gamma-sources that are able to move under their own weight through a set of guide tubes that route them from deployment boxes on the 300K flange down into position in the detector region inside the cryostat. The CUORE experiment poses stringent requirements on the maximum heat load on the cryostat, material radiopurity, contamination risk and the ability to fully retract the sources during normal data taking. Together with the integration into a unique cryostat, this requires careful design and unconventional solutions. We present the design, challenges, and expected performance of this low-temperature energy calibration system., Comment: To be published in the proceedings of the 13th International Workshop on Low Temperature Detectors (LTD), Stanford, CA, July 20-24, 2009

A detailed description of the CUORICINO $^{130}Te$ neutrinoless double-beta ($\nbb$) decay experiment is given and recent results are reported. CUORICINO is an array of 62 tellurium oxide ($TeO_{2}$) bolometers with an active mass of 40.7 kg. It is cooled to $\sim 8-10$ mK by a dilution refrigerator shielded from environmental radioactivity and energetic neutrons. It is running in the Laboratori Nazionali del Gran Sasso (LNGS) in Assergi, Italy. These data represent an exposure of $11.83\textrm{kg}...\textrm{y}$ or 91 mole-years of $^{130}Te$. No evidence for $\nbb$-decay was observed and a limit of $T^{0\nu}_{1/2}(^{130}Te)\geq3.0\times10^{24}$ y (90% C.L.) is set. This corresponds to an upper limit on the effective mass, $< m_{\nu}>$, between 0.19 and 0.68 eV when analyzed with the many published nuclear structure calculations. In the context of these nuclear models, the values fall within the range corresponding to the claim of evidence of $\nbb$-decay by H.V. Klapdor-Kleingrothaus, \textit{et al.} The experiment continues to acquire data., Comment: 30 pages, 7 figures

Neutrinoless double beta decay is one of the most powerful tools to set the neutrino mass absolute scale and establish whether the neutrino is a Majorana particle. After a summary of the neutrinoless double beta decay phenomenology, the present status of the experimental search for this rare decay is reported and the prospects for next generation experiments are reviewed., Comment: Talk presented at Flavor Physics & CP Violation Conference, Bled, 2007; 7 pages

AgReO4 microcalorimeters are planned to be used again in the next generation of calorimetric neutrino mass experiments with sensitivity down to 0.2 eV. The understanding and characterization of all possible sources of systematic uncertainties is crucial. In this work we focus on two of these sources, which have been studied in the 10 detectors of the Milano AgReO4 array experiment (MIBETA): a) the solid-state Beta Environmental Fine Structure (BEFS) observed for the first time in AgReO4; b) the detector energy response for internal beta events, which has been investigated with a dedicated measurement using a 44Ti gamma source. The possible effects on neutrino mass experiments due to the incomplete understanding of these two aspects are discussed., Comment: 3 pages, 2 figures Accepted, Nucl. Instr. Meth. Phys. A, proc. LTD11 Workshop, Tokyo, 2005

Neutrino oscillation experiments have proved that neutrinos are massive particles, but can't determine their absolute mass scale. Therefore the neutrino mass is still an open question in elementary particle physics. An international collaboration is growing around the project of Microcalorimeter Arrays for a Rhenium Experiment (MARE) for directly measuring the neutrino mass with a sensitivity of about 0.2eV/c2. Many groups are joining their experiences and technical expertise in a common effort towards this challenging experiment. We discuss the different scenarios and the impact of MARE as a complement of KATRIN., Comment: 3 pages, 1 figure Nucl. Instr. Meth. A, proceedings of LTD11 workshop, Tokyo 2005

We report the present results of CUORICINO a cryogenic experiment on neutrinoless double beta decay (DBD) of 130Te consisting of an array of 62 crystals of TeO2 with a total active mass of 40.7 kg. The array is framed inside of a dilution refrigerator, heavily shielded against environmental radioactivity and high-energy neutrons, and operated at a temperature of ~8 mK in the Gran Sasso Underground Laboratory. Temperature pulses induced by particle interacting in the crystals are recorded and measured by means of Neutron Transmutation Doped thermistors. The gain of each bolometer is stabilized with voltage pulses developed by a high stability pulse generator across heater resistors put in thermal contact with the absorber. The calibration is performed by means of two thoriated wires routinely inserted in the set-up. No evidence for a peak indicating neutrinoless DBD of 130Te is detected and a 90% C.L. lower limit of 1.8E24 years is set for the lifetime of this process. Taking largely into account the uncertainties in the theoretical values of nuclear matrix elements, this implies an upper boud on the effective mass of the electron neutrino ranging from 0.2 to 1.1 eV. This sensitivity is similar to those of the 76Ge experiments., Comment: 4 pages, 2 figures

High statistics calorimetric measurements of the beta spectrum of 187Re are being performed with arrays of silver perrhenate crystals operated at low temperature. After a modification of the experimental set-up, which allowed to substantially reduce the background of spurious counts and therefore to increase the sensitivity on the electron antineutrino mass, a new measurement with 10 silver perrhenate microbolometers is running since July 2002. The crystals have masses between 250 and 350 micrograms and their average FWHM energy resolution, constantly monitored by means of fluorescence X-rays, is of 28.3 eV at the beta end-point. The Kurie plot collected during 4485 hours x mg effective running time has an end-point energy of 2466.1 +/- 0.8{stat} +/- 1.5 {syst} eV, while the half lifetime of the decay is found to be 43.2 +/- 0.2{stat} +/- 0.1{syst} Gy. These values are the most precise obtained so far for 187Re. From the fit of the Kurie plot we can deduce a value for the squared electron antineutrino mass m(nu)^2 of 147 +/- 237{stat} +/- 90{syst} eV^2. The corresponding 90% C.L. upper limit for m(nu) is 21.7 eV., Comment: 3 pages, 3 figures. Submitted to Phys. Rev. Lett

CUORE is a proposed tightly packed array of 1000 TeO2 bolometers, each being a cube 5 cm on a side with a mass of 760 g. The array consists of 25 vertical towers, arranged in a square of 5 towers by 5 towers, each containing 10 layers of 4 crystals. The design of the detector is optimized for ultralow-background searches: for neutrinoless double beta decay of 130Te (33.8% abundance), cold dark matter, solar axions, and rare nuclear decays. A preliminary experiment involving 20 crystals 3x3x6 cm3 of 340 g has been completed, and a single CUORE tower is being constructed as a smaller scale experiment called CUORICINO. The expected performance and sensitivity, based on Monte Carlo simulations and extrapolations of present results, are reported., Comment: 39 pages, 12 figures, submitted to NIM

We report on the final results of a series of experiments on double decay of 130Te carried out with an array of twenty cryogenic detectors. The set-up is made with crystals of TeO2 with a total mass of 6.8 kg, the largest operating one for a cryogenic experiment. Four crystals are made with isotopically enriched materials: two in 128Te and two others in 130Te. The remaining ones are made with natural tellurium, which contains 31.7 % and 33.8 % 128Te and 130Te, respectively. The array was run under a heavy shield in the Gran Sasso Underground Laboratory at a depth of about 3500 m.w.e. By recording the pulses of each detector in anticoincidence with the others a lower limit of 2.1E23 years has been obtained at the 90 % C.L. on the lifetime for neutrinoless double beta decay of 130Te. In terms of effective neutrino mass this is the most restrictive limit in direct experiments, after those obtained with Ge diodes. Limits on other lepton violating decays of 130Te and on the neutrinoless double beta decay of 128Te to the ground state of 128Xe are also reported and discussed. An indication is presented for the two neutrino double beta decay of 130Te. Some consequences of the present results in the interpretation of geochemical experiments are discussed., Comment: 14 pages, 3 figures, 2 tables; more analysis details. Accepted for publication on Physics Letters B

Electron capture of 123Te from the K shell has been investigated in a new underground search with an array of 340 g TeO_2 thermal detectors. We find that some previous indication of this decay could be attributed to E.C. of 121Te resulting from neutron activation of natural Tellurium. There is therefore so far no evidence for E.C. of 123Te from the K shell with a 90 % c.l. lower limit t_{1/2}^K > 5.E19 years on the half lifetime. Taking into account the predicted K E.C. branching ratio, the corresponding lower limit on the 123Te EC half lifetime is t_{1/2} > 9.2E16 y, which can be theoretically interpreted only on the basis of a strong suppression of the nuclear matrix elements. A complementary analysis based on the expected fraction of E.C. accompanied by internal bremsstrahlung is discussed., Comment: 4 pages, 3 figures, submitted to Physical Review C