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The Southern Irumide Belt (SIB) of Zambia consists of predominantly Mesoproterozoic terranes that record a pervasive tectono-metamorphic overprint from collision between the Congo and Kalahari cratons in the final stages of Gondwana amalgamation. This study applies multi-method thermochronology to samples throughout southern Zambia to constrain the post-collisional, Phanerozoic thermo-tectonic evolution of the region. U-Pb apatite and 40Ar/39Ar muscovite data are used to constrain the cooling history of the region following Congo–Kalahari collision, and reveal ages of c. 550–450 Ma. Variations in the recorded cooling ages are interpreted to relate to localised post-tectonic magmatism and the proximity of analysed samples to the Congo–Kalahari suture. Apatite fission track data are used to constrain the low-temperature thermo-tectonic evolution of the region and identify mean central ages of c. 320–300, 210–200 and 120–110 Ma. Thermal modelling of these samples identifies a number of thermal events occurring in the region throughout the Phanerozoic. Carboniferous to Permian–Triassic heating is suggested to relate to the development of Karoo rift basins found throughout central Africa and constrain the timing of sedimentation in the basin. Permian to Jurassic cooling is identified in a number of samples, reflecting exhumation as a result of the Mauritanian–Variscan and Gondwanide orogenies. Subsequent cooling of the majority of samples occurs from the Cretaceous and persists until present, reflecting exhumation in response to larger scale rifting associated with the break-up of Gondwana. Each model reveals a later phase of enhanced cooling beginning at c. 30 Ma that, if not an artefact of modelling, corresponds to the development of the East African Rift System. The obtained thermochronological data elucidate the previously unconstrained thermal evolution of the SIB, and provides a refined regional framework for constraining the tectonic history of central Africa throughout the Phanerozoic. • First thermochronological data available for the Southern Irumide Belt of Zambia • Medium temperature thermochronology constrains Neoproterozoic to Ordovician cooling. • Thermal modelling identifies a number of thermal events during the Phanerozoic. • Carboniferous to Permian–Triassic heating relates to Karoo sedimentation. • Onset of cooling from the Cretaceous relates to Gondwana break-up. [ABSTRACT FROM AUTHOR]