1. Analysis of the individual annual layers elemental composition in the Lake Kucherlinskoe (Altai) varves sediments with submicron spatial resolution by scanning μ_XRF-SR with x-ray optics (polycapillary lenses).
- Author
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Andrey, Darin, Guoqiang, Chu, Qing, Sun, Viacheslav, Novikov, Fedor, Daryin, Dmitriy, Sorokoletov, Iakov, Rakshun, Andrey, Gogin, Roman, Senin, Knyazev, Boris, and Vinokurov, Nikolay
- Subjects
X-ray optics ,FOCUS (Optics) ,SEDIMENTS ,OPTICAL images ,BOUNDARY layer (Aerodynamics) ,LAKES - Abstract
Samples for analysis (optical thin section) were prepared from several core intervals of Lake Kucherlinskoe bottom sediments with well visually distinguished separate annual layers (varves). The annual nature of the layers was previously confirmed by the coincidence of varvechronology (layer counting) with isotopic dating (Cs-137, Pb-210, C-14). The thickness of the annual layers ranged from <1 to 3-4 mm. To study the internal structure of annual layers, we used the scanning μ_XRF-SR with focusing x-ray optics (polycapillary lenses). The experiments were carried out at the Siberian Center for Synchrotron and Terahertz Research (INP SB RAS, Novosibirsk) and the Kurchatov Complex of Synchrotron-Neutron Research (KISI, Moscow) using a confocal X-ray microscope, as well as at the Shanghai Synchrotron Center at the μ_XRF-SR station. The monochromatic excitation energy of 17 and 22 keV was used. The size of the scanning spot was determined by the used focusing polycapillary lenses and amounted to 15-25 microns. The scanning step was 50 or 100 µm. The measurement time was determined by the counting rate and ranged from 10 to 100 seconds per point. Scanning profiles were superimposed on the optical images of the thin section obtained with a high-resolution scanner. Given that the thickness of the thin section is less than 20 µm, a change in elemental composition reflects visual changes in the structure of the bottom sediment. Thus, while tracking visual changes in the structure and elemental composition of individual annual layers, seasonal geochemical features and boundaries between the layers can be distinguished. The obtained changes in the elemental composition made it possible to calculate the annual layers by the found lithological and geochemical indicators of the layer boundaries (Rb / Sr ratio). A geochemical trace of a catastrophic seismic event, the Mongolian earthquake of 1761, was found in the section of bottom sediments. [ABSTRACT FROM AUTHOR]
- Published
- 2020
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