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• The Nulliak supracrustal assemblage confirmed to be Eoarchean. • Zircon Hf isotope results indicate the presence of depleted mantle domains underneath the Saglek Block during the Eoarchean. • O-isotope signatures of Eoarchean metamorphic zircon indicate the reworking of material that experienced alteration at low temperature. The Archean Saglek Block, North Atlantic craton, is one of the oldest crustal segments preserved on Earth. This area records two granulite facies metamorphic events: one in the late-Eoarchean at ca. 3.7 Ga and one in the Neoarchean, at ca. 2.75 Ga. Here, we report the results of combined U–Pb/Hf/O in-situ isotope analyses of detrital and metamorphic zircon domains from two meta -sedimentary samples, one psammitic, and one pelitic. Both samples are components of the oldest supracrustal assemblage of the Saglek Block: the Eoarchean Nulliak supracrustal assemblage. The isotopic data presented in this study: (i) confirm deposition age of the Nulliak supracrustal assemblage before ca. 3.65 Ga, (ii) indicate local provenance of the detrital zircon, (iii) suggest deposition of the sedimentary protoliths in a convergent setting, such as an arc, (iv) crystallization of the oldest zircon during the early Eoarchean in a protolith derived from a depleted mantle component, (v) involvement of material that experienced prolonged low temperature alteration during the late Eoarchean granulite facies metamorphism and (vi) selective metamorphic overprinting during the Neoarchean granulite facies metamorphism. The new zircon U–Pb/Hf/O isotope data presented here in conjunction with previously published analyses suggest that a depleted mantle domain existed in the early Archean, as reflected in the positive εHf signature of zircon from the Saglek Block. Yet, such positive Hf isotope deviations are not the norm, but rather the exception in the preserved early Earth zircon record. In addition, mildly elevated zircon δ18O values, i.e. those ≥ 5.9 ‰, are as common in the early Archean as they are in the late-Archean zircon record, implying that crustal reworking was an active and efficient process all through the Archean. Hence, no significant variation in the nature of the reworking and broader geodynamic processes occurred during this period of time. [ABSTRACT FROM AUTHOR]

In metamorphic rocks, mineral species react over a range of pressure–temperature conditions that do not necessarily overlap. Mineral equilibration can occur at varied points along the metamorphic pressure–temperature (PT) path, and thus at different times. The sole or dominant use of zircon isotopic compositions to constrain the evolution of metamorphic rocks might then inadvertently skew geological interpretations towards one aspect or one moment of a rock's history. Here, we present in-situ U–Pb/Sm–Nd isotope analyses of the apatite crystals extracted from two meta-igneous rocks exposed in the Saglek Block (North Atlantic craton, Canada), an Archean metamorphic terrane, with the aim of examining the various signatures and events that they record. The data are combined with published U–Pb/Hf/O isotope compositions of zircon extracted from the same hand-specimens. We found an offset of nearly ca. 1.5 Gyr between U-Pb ages derived from the oldest zircon cores and apatite U–Pb/Sm–Nd isotopic ages, and an offset of ca. 200 Ma between the youngest zircon metamorphic overgrowths and apatite. These differences in metamorphic ages recorded by zircon and apatite mean that the redistribution of Hf isotopes (largely hosted in zircon) and Nd isotopes (largely hosted in apatite within these rocks), were not synchronous at the hand-specimen scale (≤~0.001 m3). We propose that the diachronous redistribution of Hf and Nd isotopes and their parent isotopes was caused by the different PT conditions of growth equilibration between zircon and apatite during metamorphism. These findings document the latest metamorphic evolution of the Saglek Block, highlighting the role played by intra-crustal reworking during the late-Archean regional metamorphic event. [ABSTRACT FROM AUTHOR]

When and how Earth's ancient crust – the cratons – became underpinned by cool, thick lithospheric mantle roots capable of hosting diamonds are among the most controversial aspects of Archean geology. Alluvial diamonds in cratonic sedimentary cover rocks, whose minimum age is determined by detrital-zircon geochronology, provide a unique perspective on this topic. A new discovery of a diamond-bearing quartz-pebble conglomerate from the northern Slave craton, Canada contains detrital zircon with a restricted U-Pb age distribution that has a dominant peak at ∼2.94 Ga and depositional age of ∼2.83 Ga. Pressure-temperature constraints derived from an olivine-diamond host pair lie on a conductive Mesoarchean geotherm of ∼36–38 mW/m2, comparable to the coolest modern lithospheric geotherms. This result is at odds with a hotter geothermal gradient related to nearby Mesoarchean komatiites. We propose a model whereby early building blocks for cratons were small but with deep cool roots that formed by slab-stacking, and were subsequently juxtaposed with regions of thinner, hotter lithosphere. This heterogeneous initial architecture later amalgamated and thickened through lateral accretion forming the more uniformly thick cratonic lithosphere observed today. Thermal modelling indicates that stacking/thickening of cool initial lithosphere into a lithospheric keel thick enough to stabilise diamonds is the most likely way of generating the observed geotherm by Mesoarchean times. • Detrital zircon in host sedimentary rock has a Mesoarchean U-Pb age of >2.83 Ga. • Oxidizing diamond-forming fluids had crustal component (non-mantle δ 13 C- δ 15 N). • PT constraints show cool conductive Mesoarchean mantle geotherm of ∼36–38 mW/m2. • Early cratonic building blocks were small with deep cool roots. • These blocks likely formed through slab-stacking. [ABSTRACT FROM AUTHOR]